Acta Cryst. (2004). E60, m91-m93  [ doi:10.1107/S1600536803028320 ]

P(C₆H₄CH₂NMe₂-2)₃-stabilized mononuclear pentafluoropropionatosilver(I)

Y. Shen, H. Pritzkow, B. Walfort, T. Rüffer and H. Lang

Online 19 December 2003

Key indicators

• Single-crystal X-ray study
• T = 173 K
• R factor = 0.033
• wR factor = 0.080
• Data-to-parameter ratio = 20.3

checkCIF/PLATON results

No syntax errors found



Alert level A
GEOM005_ALERT_1_A  _geom_angle_atom_site_label_1 is missing
            Label identifying the atom site 1.
PLAT027_ALERT_3_A _diffrn_reflns_theta_full (too) Low ............       0.00 Deg.  
PLAT029_ALERT_3_A _diffrn_measured_fraction_theta_full Low .......       0.00       
PLAT037_ALERT_1_A _diffrn_reflns_theta_full .......... Not Given .          ?
PLAT038_ALERT_1_A _diffrn_measured_fraction_theta_max  Not Given .          ?
PLAT039_ALERT_1_A _diffrn_measured_fraction_theta_full Not Given .          ?
PLAT761_ALERT_1_A CIF Contains no X-H Bonds ......................          ?
PLAT762_ALERT_1_A CIF Contains no X-Y-H or H-Y-H Angles ..........          ?

Alert level B
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.79 Ratio 
PLAT222_ALERT_3_B Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       4.87 Ratio 

Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.69       
PLAT164_ALERT_4_C Nr. of Refined C-H H-Atoms in Heavy-At Struct...         72       
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.77 Ratio 
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C29     
PLAT301_ALERT_3_C Main Residue  Disorder .........................       2.00 Perc. 

   8 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   6 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   4 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion

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