Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 60| Part 1

ISSN: 2056-9890

January 2004 issue

Highlighted illustration

Cover illustration: Olanzapine belongs to the newer generation, atypical antipsychotic agents. Compared to the older ones, these are more efficacious and have reduced side effects. The boat conformation of the central diazepine ring results in the butterfly-like shape of the molecule. See Wawrzycka-Gorczyca, Koziol, Glice & Cybulski [Acta Cryst. E60, o66-o68].

editorial

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Structure Reports Online: a continuing growth and success story

D. G. Watson and W. Clegg

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international union of crystallography

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Notes for authors 2004

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inorganic compounds

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Na₄Ni₅[(As_1−xP_x)O₄]₂[(As_2yP_2−2y)O₇]₂ (x = 0.27 and y = 0.295)

R. Ben Smail and T. Jouini

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Dipotassium nickel(II) bis(dihydrogendiphosphate) dihydrate, K₂Ni(H₂P₂O₇)₂·2H₂O

A. A. Tahiri, I. Messouri, M. Lachkar, P. Y. Zavalij, R. Glaum, B. El Bali and O. Rachid

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Na₃VOS₃

F. Q. Huang and J. A. Ibers

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metal-organic compounds

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A novel supramolecular organic–inorganic adduct containing α-Keggin-type [PW₁₂O₄₀]³⁻ anions and benzo-15-crown-5 molecules

F. A. Almeida Paz, F. L. Sousa, P. C. R. Soares-Santos, A. M. V. Cavaleiro, H. I. S. Nogueira, J. Klinowski and T. Trindade

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cis-Diaquabis[2-(hydroxymethyl)pyridine]nickel(II) dichloride

S. Hamamci, V. T. Yilmaz and C. Thöne

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Bis(μ-1,2,4-triazole-κ²N¹:N²)bis[diaqua(oxalato-κ²O,O′)copper(II)]

O. Castillo, U. García-Couceiro, A. Luque, J. P. García-Terán and P. Román

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trans-Diaquabis(1H-imidazole-4,5-dicarboxylato-κ²N³,O⁴)cadmium(II)

X.-M. Zhang, R.-Q. Fang, H.-S. Wu and S. W. Ng

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Triaqua-1κO,2κO,3κO-hexakis-μ-chloroacetato-1:2κ⁴O:O′;2:3κ⁴O:O′;1:3κ⁴O:O′-μ₃-oxo-triiron(III) nitrate trihydrate

X. M. Ren, H. Okudera and R. K. Kremer

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[Bis(3-diphenylphosphinopropyl)phenylphosphine-κ³P,P′,P′′]chloroplatinum(II) perchlorate

S. T. Klint, O. Simonsen, L. V. Andreasen, A. D. Bond and O. Wernberg

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(Ferrocenylmethyl)trimethylammonium triiodide

A. J. Blake, C. Caltagirone, V. Lippolis, M. Schröder and C. Wilson

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Tetraaqua[(3-carboxyphenoxy)acetato]nickel(II)

S. Gao, J.-R. Li, J.-W. Liu, C.-S. Gu and L.-H. Huo

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A coordination polymer of Co^II with 1,1′-(1,4-butanediyl)bis(imidazole)

J. Yang, J.-F. Ma and J.-F. Liu

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Diaquabis(imidazole-κN)bis(nitrobenzoato-κO)nickel(II)

T.-G. Xu and D.-J. Xu

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A one-dimensional coordination polymer: catena-poly[[triaquapyridinecobalt(II)]-μ-sulfato]

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Tetra-μ-L-isoleucine-bis[tetraaquasamarium(III)] hexaperchlorate

J. Wang, C. Niu, N. Hu and J. Ni

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Hexaaquacobalt(II) trans-bis(η³-pyridine-2,6-dicarboxylato-κ³O,N,O′)cobaltate(II) dihydrate

K.-B. Shiu, C.-H. Yen, F.-L. Liao and S.-L. Wang

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Bis(1-acetophenone-1H-benzotriazole-κN³)dichlorozinc(II)

F. Jian, H. Xiao and P. Sun

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cis-Dichloro(N,N,N′,N′-tetramethyl-1,2-diaminoethane)palladium(II)

R. C. Boyle, J. T. Mague and M. J. Fink

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Hydrogen bonding in coordinated thiosemicarbazones: ammine[2-hydroxy-1-naphthaldehyde 4-methylthiosemicarbazonato]nickel(II)

J. V. Martínez, S. Hernández-Ortega and V. Bautista Jimenez

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Diaqua(diethylenetriamine-κ³N)(perchlorato-κO)copper(II) hydrogenmaleate

J. Valdés-Martínez, R. A. Toscano and M. D. Río-Ramírez

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Dipotassium diaquabis(malonato-κ²O,O′)nickelate(II) dihydrate

X. Xiao, W. Xu, Y. Li, B. Zhang and D. Zhu

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catena-Poly[bis[(2,2′-bipyridine-κ²N,N′)manganese(II)]-di-μ-4-hydroxyisophthalato]

X.-M. Zhang, R.-Q. Fang, H.-S. Wu and S. W. Ng

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μ-Oxo-bis{diethoxy[salicylaldoximato(2–)]niobium(V)}

M. M. Amini, M. Mirzaee and S. W. Ng

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Quinolinium trichloro(quinoline-κN)cobaltate(II)

T.-T. Pan and D.-J. Xu

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Bis(piperidinium) tetrachlorozincate

A. Fowkes and W. T. A. Harrison

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A supramolecular ladder in diaqua(μ-8-hydroxy-7-iodoquinoline-5-sulfonato-κ⁴N,O,O′,O′′)cadmium(II) dihydrate

S. Francis, P. T. Muthiah and R. J. Butcher

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Bis{di-μ-isobutyrato-bis[cis-diammineplatinum(II)]} tetraperchlorate

K. Sakai and E. Ishigami

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{2,6-Bis[(diphenylphosphino)methyl]phenyl}chloroplatinum(II)

S. Fischer and O. F. Wendt

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Bis[bis(1,10-phenanthroline)chlorocopper(II)] benzene-1,2,4,5-tetracarboxylate(2–) dihydrate

H.-P. Xiao, M.-L. Hu and X.-H. Li

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trans-Dibromobis(phenazine)copper(II)

W. Maniukiewicz, M. Bukowska-Strzyżewska and M. Sadowska

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A copper(I) iodide chain with the 2-amino-4,6-dimethylpyridine cation

S. F. Haddad, M. A. AlDamen, R. D. Willett and B. Twamley

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trans-Diazidobis{2-[(3-cyclohexylaminopropylimino)methyl]phenolato}nickel(II)

Z.-L. You, Z.-D. Xiong, W.-S. Liu, M.-Y. Tan and H.-L. Zhu

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trans-Bis(methanol-κO)bis(2-quinolinecarboxylato-κ²N,O)zinc(II)

Z.-Y. Yue, C. Cheng, P. Gao and P.-F. Yan

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Low-temperature phase of diaqua(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate

J. W. Bats, A. Rivas Nass and A. S. K. Hashmi

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Bis(2-aminopyridine)(2,2′-bipyridine)platinum(II) tetracyanoplatinate(II) dihydrate

K. Sakai, M. Mizota and N. Akiyama

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P(C₆H₄CH₂NMe₂-2)₃-stabilized mononuclear pentafluoropropionatosilver(I)

Y. Shen, H. Pritzkow, B. Walfort, T. Rüffer and H. Lang

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Aqua(1H-imidazole-κN³)(triethanolamine-κ³O)copper(II) perchlorate hemi(benzene-1,4-dioxyacetate)

S. Gao, J.-W. Liu, J.-R. Li, L.-H. Huo and H. Zhao

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Bis(4-benzoyl-3-methyl-1-phenyl-1H-pyrazol-5-onato)diethanolcadmium(II)

H.-Z. Xu, Y.-Q. Zhu, X. Zhang and H.-L. Zhu

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Bis(o-chlorophenylbenzoylthiourea-κS)diiodomercury(II)

M. S. M. Yusof, B. M. Yamin and M. B. Kassim

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Tetraaquabis(4-carboxyphenoxyacetato)magnesium(II)

S. Gao, J.-R. Li, L.-H. Huo, J.-W. Liu and C.-S. Gu

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Tetra-μ-chloro-chloro(N,N,N′,N′-tetramethylethane-1,2-diamine)(1,1,3-trimethyl-2-imidazolium)dicopper(I)copper(II)

R. J. Butcher, C. George and A. P. Purdy

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cis-Diaquabis(4-cyanobenzoato)(1,10-phenanthroline)cobalt(II)

L.-M. Xie, H.-Y. He, Y.-L. Zhou and L.-G. Zhu

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Dichlorobis(2,2′-diamino-4,4′-bi-1,3-thiazole-κ²N,N′)nickel(II) dihydrate

J.-G. Liu and D.-J. Xu

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Hexaaquacobalt(II) 1,5-naphthalenedisulfonate

D.-L. An, S. Gao, Z.-B. Zhu, L.-H. Huo and H. Zhao

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Bis[aquachlorobis(1,10-phenanthroline)manganese(II)] benzene-1,4-dioxyacetate dihydrate

S. Gao, J.-W. Liu, L.-H. Huo, H. Zhao and J.-G. Zhao

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trans-Diaquabis(pyridine-4-carboxylato)cobalt(II) dihydrate

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Bis(triphenylsilyl)phenylarsenite, PhAs(OSiPh₃)₂

G. Ferguson, B. J. O'Leary and T. R. Spalding

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cis-Diaquabis(ethylenediamine)nickel(II) benzene-1,4-dicarboxylate monohydrate

K.-B. Shiu, C.-H. Yen, F.-L. Liao and S.-L. Wang

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Bis{μ-2′-[1-(4-chloro-2-oxidophenyl)ethylidene]thiophene-2-carbohydrazidato}bis[pyridinezinc(II)]

H. Ali, M. Mohammad, M. S. M. Yusof and B. M. Yamin

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Dichloromethyl[1-(2-pyridyl)ethanone benzoylhydrazonato]tin(IV)

M. A. Affan, M. B. Shamsuddin, M. S. M. Yusof and B. M. Yamin

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(N-Salicylidene-D,L-glutamato)(2-methylimidazole)copper(II)

V. Langer, E. Scholtzová, D. Gyepesová, M. Kohútová and A. Valent

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organic compounds

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4-Methylphenyl 3-nitrobenzenesulfonate

N. Vembu, M. Nallu, S. Durmus, M. Pazner, J. Garrison and W. J. Youngs

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Bis(quininium) (R,R)-tartrate monohydrate

C. Ryttersgaard and S. Larsen

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1,3,5-Tris(4-formylphenoxymethyl)-2,4,6-trimethylbenzene ethyl acetate solvate

D. J. Bray, L. F. Lindoy and J. C. McMurtrie

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5,5-Dimethyl-2,3-diphenyl-5,6-dihydroimidazo[1,2-c]quinazoline

H. Wu, D. Shi, C. Shi, J. Wang, X. Wang, H. Hu and K. Yu

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trans-(4-Phenyltetrahydro-2-furyl)methyl p-nitrobenzoate

J. Hartung, P. Schmidt, I. Svoboda and H. Fuess

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1-Methyl-1-phenyl-3-(phthalimidoacetyl)cyclobutane

N. Özdemir, M. Dinçer, I. Yılmaz and A. Çukurovalı

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(11S)-(+)-N,N′-Dimethylcinchoninium diiodide

N. Yoshikawa, K. Takemoto, J. Sakamoto, N. Kanehisa, Y. Kai, H. Takashima and K. Tsukahara

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5-(tert-Butylamino)-5-oxopentanoic acid

K. Takahashi, T. Okamura, H. Yamamoto and N. Ueyama

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rac-(1R,11S,12R)-Ethyl 12-hydroxy-15-oxobicyclo[9.3.1]pentadecane-1-carboxylate

S. Fresu, M. Schürmann, H. Preut and P. Eilbracht

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N-(2-Benzyloxyethyl)-4,7-dimethyl-6-(1,3-dithiolan-2-yl)-1,2,3,4,5,6-hexahydro-1,5-methano-2-azocino[4,3-b]indol-2-one

T. Hökelek, N. Uludağ and S. Patır

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1,3-Diethylbenzimidazolium iodide

R. T. Stibrany, H. J. Schugar and J. A. Potenza

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3-(4-Hydroxystyryl)-1,1-dimethylcyclohex-3-en-5-one

T. Kolev, T. Berends, H. Preut and M. Spiteller

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4,5-Bis(4-methylphenylsulfanyl)phthalonitrile

N. Ocak, U. Çoruh, N. Akdemir, C. Kantar, E. Aǧar and A. Erdönmez

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1-Methyl-N-(2-{[(1-methyl-4-nitro-1H-pyrrol-2-yl)carbonyl]amino}ethyl)-4-nitro-1H-pyrrole-2-carboxamide dimethylformamide disolvate

L.-P. Lu, M.-L. Zhu and P. Yang

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2-tert-Butyl-4-methyl-6-(1-piperidiniomethyl)phenol chloride

M. Du, X.-J. Zhao and Y. Wang

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(R,S)-Methyl 2-(2′-methylenecyclopropyl)hydroxyacetate

D. S. Yufit, V. Bagutski, J. A. K. Howard and A. Meijere

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1,2-Bis(di-4-pyridylphosphino)ethane (d4pype)

S. J. Berners-Price, R. J. Bowen and P. C. Healy

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1,5-Diaminonaphthalene

S. Bernès, M. R. Pastrana, E. H. Sánchez and R. G. Pérez

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Diethyl 7-oxo-3-(pyrrolidin-1-yl)cycloocta-2,8-diene-1,2-dicarboxylate

T. Hökelek, A. Uzgören, Y. Ergün, N. Tunoğlu and G. Okay

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4′-(3-Chlorophenyl)-1-methyl-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-2′′-indan-2,1′′,3′′-trione

P. R. Seshadri, S. Selvanayagam, D. Velmurugan, K. Ravikumar, A. R. Sureshbabu and R. Raghunathan

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1-(2-Chlorophenyl)-1H-indan-2-spiro-2′-pyrrolizidine-3′-spiro-3′′-1H-indole-1,3,2′′(2H,3′′H)-trione

M. M. Govind, S. Selvanayagam, D. Velmurugan, K. Ravikumar, A. R. Sureshbabu and R. Raghunathan

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1-Benzoylacenaphthylene-1-spiro-3′-pyrrolizidine-2′-spiro-3′′-1H-indole-2,2′′(1H,3′′H)-dione

M. M. Govind, S. Selvanayagam, D. Velmurugan, K. Ravikumar, A. R. Sureshbabu and R. Raghunathan

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Diethyl 2-(4-nitrophenyl)malonate forms a hydrogen-bonded chain of rings

C. Glidewell, J. N. Low, J. M. S. Skakle and J. L. Wardell

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4,5-Diiodo[1,2,5]thiadiazolotetrathiafulvalene

M. Tomura and Y. Yamashita

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Polymorphic form II of 2-methyl-4-(4-methyl-1-piperazinyl)-10H-thieno[2,3-b][1,5]benzodiazepine

I. Wawrzycka-Gorczyca, A. E. Koziol, M. Glice and J. Cybulski

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2-Methyl-4-(4-methyl-1-piperazinyl)-10H-thieno[2,3-b][1,5]benzodiazepine methanol solvate

I. Wawrzycka-Gorczyca, L. Mazur and A. E. Koziol

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6α-Hydroxy-17β-azavouacapane-17,7β-carbolactone

O. Abrahão-Júnior, S. Guilardi, C. R. A. Maltha and D. Piló-Veloso

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9-(p-Methylphenyl)fluorene

A. W. McLean, C. Y. Meyers and P. D. Robinson

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2-(2-Pyridyl)benzo[1,2-d;4,5-d′]diimidazole

X.-J. Lin, Y.-Z. Li, H.-J. Xu, S.-G. Liu, L. Xu, Z. Shen and X.-Z. You

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4-(Benzyloxy)phthalonitrile

M. Dinçer, A. Ağar, N. Akdemir, E. Ağar and N. Özdemir

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A second polymorph of (+)-pinoresinol–dioxane (1/1)

R. Stomberg, V. Langer and K. Lundquist

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A new polymorph of 2-bromo-5-hydroxybenzaldehyde

M. R. Silva, J. A. Paixão, A. M. Beja, A. J. F. N. Sobral and A. M. d'A. Rocha Gonsalves

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5-Hydroxy-3,3′,4′,5′,7-pentamethoxyflavone (combretol)

Dachriyanus, R. Fahmi, M. V. Sargent, B. W. Skelton and A. H. White

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1-Amino-3-ammonioguanidinium dichloride

A. van der Lee and M. Barboiu

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3-Methyl-1H-quinoxalin-2-one

I. V. Nikolaenko and O. Q. Munro

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2-Methoxy-2-phenylacetic acid

J. Hartung, K. Špehar, I. Svoboda and H. Fuess

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Unique hydrogen bonding in the acetone-mediated helical structure of (R,R)-3,3′-bisBINOL

T. Kawanami, K. Ishizuka, H. Furuno and J. Inanaga

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3-Chloromethyl-5-methoxy-4-methoxycarbonyl-3-oxo-2,3-dihydro-[1,3]oxaphosphole monohydrate

C. Ciptadi, H. J. Cristau, Y. A. Bekro, M. Tillard and D. Virieux

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Ethyl 3-{[(2-chlorophenyl)sulfonyl]imino}-2-{[(3,5-dimethoxyphenyl)amino]carbonyl}-3-(methylsulfanyl)propanoate

C. H. L. Kennard, H. G. McFadden and K. A. Byriel

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5,5′-Oxybis[2-(phthalimido)acetic acid] N,N-dimethylformamide disolvate

X. Lü, B. Kang and S. W. Ng

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Dimethyl(2-trimethylsilylethyl)[(2-trimethylsilylethyl)dimethylammonio]ammonium tetrakis[3,5-bis(trifluoromethyl)phenyl]borate at 130 K

K. Hassall and J. White

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N-Hydroxy-N′-(1-naphthyl)-2-phenylacetamidin-2-one

T. Hökelek, O. Büyükgüngör, M. Taş and H. Batı

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3-Hydroxy-6-methyl-2-[4-(3-trifluoromethylphenyl)piperazin-1-ylmethyl]-4H-pyran-4-one

Y. Köysal, Ş. Işık and M. D. Aytemir

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A sulfanilamide derivative containing a boronate ester group

S. A. Westcott, X.-F. He, C. M. Vogels and A. Decken

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A neo-clerodane diterpene from Teucrium tomentosum

S. S. Devi, R. Malathi, S. S. Rajan, S. Aravind, G. N. Krishnakumari and K. Ravikumar

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Ethyl (3-ethyl-1-oxo-1,2,3,4-tetrahydrocarbazol-2-yl)acetate

F. B. Kaynak, S. Özbey, N. Uludag and S. Patir

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Phenacyltriphenylphosphonium picrate: intra-and interionic C—H⋯O interactions

M. Baby Mariyatra, E. C. Spencer, K. Panchanatheswaran and J. A. K. Howard

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2′-(p-Chlorobenzoyl)-2,2′,3,3′,4′,5′,6′,6a′-octahydro-1H-indan-2-spiro-3′-(1H-pyrrolizine)-1′-spiro-3′′-indoline-1,2′′,3-trione

P. R. Seshadri, S. Selvanayagam, D. Velmurugan, K. Ravikumar, A. R. Sureshbabu and R. Raghunathan

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4-(Pyridin-2-yl)thiazol-2-ylamine

J. D. Crane and A. McLaughlin

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1,16-Dichlorohexadecane

N. Nakamura and H. Shimizu

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Low-temperature 4-thiacyclohexyl m-nitrobenzoate

L. Andrau and J. White

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Bis(2,4,6-trichlorophenyl) 2-ethylmalonate

C. Wentrup, J. Buchanan, K. A. Byriel and C. H. L. Kennard

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A furodysinin lactone derivative from the marine sponge Dysidea fragilis

K. Ravikumar, S. Selvanayagam, T. V. Goud, P. Krishnaiah and Y. Venkateswarlu

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1-[N-(p-Hydroxyphenyl)aminomethylidene]naphthalen-2(1H)-one propan-1-ol hemisolvate

M. Odabaşoǧlu, Ç. Albayrak and O. Büyükgüngör

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2-[2-Hydroxyimino-2-(3-methyl-3-phenylcyclobutyl)ethyl]isoindole-1,3-dione

N. Özdemir, M. Dinçer, İ. Yılmaz and A. Çukurovalı

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Research communications are designed to help authors bring out the science behind their structure determinations. Authors are encouraged to report more than one structure in the same communication and also to include the results of investigations with other techniques. The Research communications format makes Acta E the natural home for structure determinations with interesting science to report.

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