[HTML version][PDF version] [Buy article online]

[Contents scheme]

Acta Cryst. (2004). E60, o464-o465  [ doi:10.1107/S1600536804004143 ]

Ethyl 5-(2,6-dichlorophenyl)-7-methyl-2-(1-naphthylmethylene)-3-oxo-2,3-dihydro-5H-thiazolo[3,2-a]pyrimidine-6-carboxylate

X.-G. Liu, Y.-Q. Feng, X.-F. Li and B. Gao

Abstract: The title compound, C27H20Cl2N2O3S, was synthesized by the reaction of ethyl 2-mercapto-4-methyl-6-(2,6-dichlorophenyl)-1,6-dihydro-pyrimidine-5-carboxylate, ethyl chloroacetate and aldehyde in acetic acid and acetic anhydride. In the molecule, the thiazolo[3,2-a]pyrimidine and naphthalene systems are essentially coplanar, with a dihedral angle between the combined plane and the mean plane of the benzene ring of the 2,6-dichlorophenyl substituent of 94.7 (4)°.

Online 28 February 2004


Copyright © International Union of Crystallography
IUCr Webmaster