Acta Cryst. (2004). E60, m509-m510  [ doi:10.1107/S1600536804007226 ]

Tri--chloro-bis[(⁵-pentamethylcyclopentadienyl)rhodium(III)] tetrafluoroborate

L. Liu, Q.-F. Zhang and W.-H. Leung

Online 31 March 2004

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.007 Å
• R factor = 0.042
• wR factor = 0.084
• Data-to-parameter ratio = 20.4

checkCIF/PLATON results

No syntax errors found



Alert level A
PLAT029_ALERT_3_A _diffrn_measured_fraction_theta_full Low .......       0.89       

Alert level B
REFLT03_ALERT_3_B  Reflection count < 90% complete (theta max?)
           From the CIF: _diffrn_reflns_theta_max           28.33
           From the CIF: _diffrn_reflns_theta_full           0.00
           From the CIF: _reflns_number_total               5533
           TEST2: Reflns within _diffrn_reflns_theta_max
           Count of symmetry unique reflns         6183
           Completeness (_total/calc)             89.49%

Alert level C
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......         C8     
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......        C20     

   1 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion

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