[HTML version][PDF version][CIF][3d view][Structure Factors][CIF check Report][Issue contents]  [Buy article online]

[Contents scheme]

Acta Cryst. (2004). E60, o662-o663  [ doi:10.1107/S1600536804006634 ]

The Schiff base 3,4-methylenedioxybenzaldehyde semicarbazone

J.-L. Wang, Y.-J. Jia and M. Yu

Abstract: The synthesis of the title compound, C9H9N3O3, was achieved by the condensation of 3,4-methylenedioxybenzaldehyde with semicarbazide hydrochloride. The molecule is approximately planar: the dihedral angles of the 3,4-methylenedioxybenzene and amide moieties with the hydrazone moiety are 10.2  (2) and 8.9  (3)°, respectively. Intra- and intermolecular hydrogen bonds generate a two-dimensional network. Aromatic stacking interactions are also found in the crystal structure.

Online 27 March 2004


Copyright © International Union of Crystallography
IUCr Webmaster