Acta Cryst. (2004). E60, m362-m363  [ doi:10.1107/S1600536804004660 ]

Bis{5-methyl-4-[(Z)-(1-naphthylamino)phenylmethylene]-2-phenyl-3H-pyrazol-3-one-²N,N'}silver(I) hexafluorophosphate

X.-Q. Lü, F. Bao, Q. Wu, B.-S. Kang and S. W. Ng

Online 13 March 2004

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.004 Å
• R factor = 0.037
• wR factor = 0.097
• Data-to-parameter ratio = 15.8

checkCIF/PLATON results

No syntax errors found




Alert level C
ABSTM02_ALERT_3_C  The ratio of expected to reported Tmax/Tmin(RR') is < 0.90
            Tmin and Tmax reported:      0.693     0.837
            Tmin' and Tmax expected:      0.789     0.851
            RR' =      0.893
            Please check that your absorption correction is appropriate.
PLAT061_ALERT_3_C Tmax/Tmin Range Test RR' too Large .............       0.89       
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       1.02       
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.57 Ratio 
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C15     
PLAT244_ALERT_4_C Low Solvent  U(eq) as Compared to Neighbors ....         P1     
PLAT414_ALERT_2_C Short Intra D-H..H-X       H3N    ..  H26     ..       1.97 Ang.  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   7 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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