# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' di-\m~2~-Chloro-dichloro-di-\m~3~-oxo- octaphenyl-tetratin' _shelx_refln_list_code 4 _shelx_F_calc_maximum 901.64 _exptl_crystal_F_000 2616.00 _reflns_d_resolution_high 0.8400 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 11.6940 _cell_length_b 23.2560 _cell_length_c 18.8050 _cell_angle_alpha 90.000 _cell_angle_beta 100.565 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14719.62 15751.53 344.20 o 4 0 0 6017.23 7043.64 273.47 o 6 0 0 22461.53 22118.28 579.33 o 8 0 0 79409.87 84246.05 2294.30 o 10 0 0 11298.75 11394.59 875.72 o 12 0 0 6122.67 6045.78 735.79 o 1 1 0 50087.41 54843.04 1197.71 o 2 1 0 148215.83 163930.08 2887.19 o 3 1 0 5975.85 6013.11 177.32 o 4 1 0 638.67 592.23 83.51 o 5 1 0 5449.20 4990.29 189.36 o 6 1 0 45576.84 46117.74 770.12 o 7 1 0 729.83 829.25 134.66 o 8 1 0 20407.30 20887.82 602.60 o 9 1 0 3071.92 2904.55 368.43 o 10 1 0 3951.49 3848.63 390.70 o 11 1 0 4141.02 3812.52 402.24 o 12 1 0 6199.87 5857.73 509.78 o 13 1 0 2146.11 2506.48 423.46 o 0 2 0 43290.46 40983.53 2603.02 o 1 2 0 4680.80 5168.05 106.34 o 2 2 0 23839.78 24162.07 433.04 o 3 2 0 696.27 856.56 83.08 o 4 2 0 3038.62 2815.13 135.09 o 5 2 0 12646.73 13072.36 295.27 o 6 2 0 11718.83 11201.18 301.01 o 7 2 0 8971.03 8635.67 288.78 o 8 2 0 8853.58 9127.46 315.81 o 9 2 0 1425.84 1383.17 285.21 o 10 2 0 1124.67 1219.66 285.36 o 11 2 0 6341.68 6250.09 496.06 o 12 2 0 49.03 314.95 225.43 o 13 2 0 66.71 -63.55 185.96 o 1 3 0 54.12 88.16 30.73 o 2 3 0 243.04 280.62 57.55 o 3 3 0 3686.94 3532.18 141.24 o 4 3 0 25.40 3.20 48.87 o 5 3 0 3551.74 3688.59 172.91 o 6 3 0 2438.79 2245.74 156.17 o 7 3 0 4025.76 3856.18 207.12 o 8 3 0 2857.32 2661.85 199.60 o 9 3 0 802.65 783.68 193.20 o 10 3 0 1.99 -88.53 148.46 o 11 3 0 254.82 112.55 188.84 o 12 3 0 830.39 1015.21 294.46 o 13 3 0 1481.15 1287.53 331.09 o 0 4 0 382.49 493.87 77.63 o 1 4 0 9300.63 9529.76 367.22 o 2 4 0 119905.65 132496.22 3950.59 o 3 4 0 10733.73 10772.15 337.89 o 4 4 0 859.70 862.43 106.05 o 5 4 0 766.09 822.38 115.89 o 6 4 0 7382.20 7307.70 262.12 o 7 4 0 2947.82 2936.97 196.30 o 8 4 0 11464.16 11352.92 363.64 o 9 4 0 80.90 169.23 135.88 o 10 4 0 2766.56 2729.62 399.68 o 11 4 0 5000.19 4837.31 445.93 o 12 4 0 189.34 280.88 214.60 o 13 4 0 173.11 299.91 223.08 o 1 5 0 6461.41 5954.97 332.75 o 2 5 0 47.53 71.12 58.56 o 3 5 0 4078.27 3772.77 161.30 o 4 5 0 87929.93 90614.66 1630.24 o 5 5 0 4129.70 4090.39 196.97 o 6 5 0 6.01 56.48 78.40 o 7 5 0 3606.78 3583.24 215.19 o 8 5 0 33972.00 34083.38 788.58 o 9 5 0 297.68 330.06 169.13 o 10 5 0 9732.71 9210.99 564.29 o 11 5 0 5770.31 5885.78 494.03 o 12 5 0 3024.92 3080.67 449.03 o 13 5 0 95.06 196.77 319.14 o 0 6 0 8284.05 8766.80 503.17 o 1 6 0 1708.93 1514.26 112.47 o 2 6 0 52573.98 53038.90 1803.54 o 3 6 0 57439.82 59229.41 1647.31 o 4 6 0 7635.80 7599.00 266.26 o 5 6 0 72383.39 74211.37 1449.98 o 6 6 0 14109.47 14005.13 377.99 o 7 6 0 5601.44 5769.30 272.89 o 8 6 0 14862.16 15240.79 440.36 o 9 6 0 23477.42 22221.73 858.99 o 10 6 0 4707.80 4613.10 420.37 o 11 6 0 49.27 51.60 166.64 o 12 6 0 2687.79 2976.69 440.77 o 13 6 0 1877.06 1843.15 388.23 o 1 7 0 47239.38 46630.61 1588.35 o 2 7 0 50707.57 48768.97 1654.81 o 3 7 0 142314.63 146490.11 5198.62 o 4 7 0 26287.07 26403.12 696.86 o 5 7 0 3580.36 3340.01 197.89 o 6 7 0 36209.11 36895.68 933.65 o 7 7 0 56.33 -36.67 95.43 o 8 7 0 4345.62 4114.39 258.28 o 9 7 0 2541.14 2696.48 298.07 o 10 7 0 1180.31 1099.14 281.92 o 11 7 0 17519.50 16960.93 798.01 o 12 7 0 1948.13 2087.14 396.28 o 13 7 0 1276.54 1410.15 367.62 o 0 8 0 31789.28 30834.32 1523.48 o 1 8 0 16310.10 16036.20 660.91 o 2 8 0 5146.69 4626.77 189.30 o 3 8 0 13253.08 13001.57 384.65 o 4 8 0 9907.46 9769.51 340.32 o 5 8 0 38141.71 36500.63 1064.38 o 6 8 0 7364.66 7048.87 295.65 o 7 8 0 69.43 66.03 113.60 o 8 8 0 8219.88 8390.22 357.01 o 9 8 0 8633.12 9098.98 456.27 o 10 8 0 16.93 8.43 168.38 o 11 8 0 0.76 65.01 172.07 o 12 8 0 389.89 307.42 227.31 o 13 8 0 458.03 580.43 253.76 o 1 9 0 2744.87 2657.75 154.97 o 2 9 0 1921.74 1794.34 136.05 o 3 9 0 3536.32 3371.72 185.33 o 4 9 0 13.03 80.82 84.08 o 5 9 0 7500.30 7481.92 293.18 o 6 9 0 6284.28 6335.23 336.00 o 7 9 0 7310.96 7267.02 327.55 o 8 9 0 4973.57 4903.61 293.65 o 9 9 0 193.01 199.43 161.84 o 10 9 0 523.61 494.88 216.50 o 11 9 0 285.39 244.70 200.49 o 12 9 0 104.31 30.84 194.62 o 0 10 0 38885.43 38092.82 1690.55 o 1 10 0 20940.87 20648.59 627.12 o 2 10 0 3.57 32.74 67.32 o 3 10 0 5950.48 6342.25 405.84 o 4 10 0 2.55 -19.61 75.85 o 5 10 0 3373.99 3144.74 213.08 o 6 10 0 4933.71 5205.55 276.48 o 7 10 0 471.38 524.63 146.67 o 8 10 0 2960.53 3338.93 270.16 o 9 10 0 794.77 1041.59 231.41 o 10 10 0 10.44 2.11 165.18 o 11 10 0 152.07 95.91 192.32 o 12 10 0 1107.66 1362.21 334.31 o 1 11 0 43936.54 43306.35 2235.33 o 2 11 0 226.34 219.17 93.29 o 3 11 0 3910.98 4000.29 215.75 o 4 11 0 11.35 -32.55 75.40 o 5 11 0 6206.99 6241.60 289.63 o 6 11 0 1604.24 1608.53 207.31 o 7 11 0 9.53 94.68 118.01 o 8 11 0 802.90 861.97 187.36 o 9 11 0 8435.28 8436.34 460.98 o 10 11 0 23.16 68.27 152.31 o 11 11 0 0.51 150.98 195.70 o 12 11 0 396.63 515.27 244.35 o 0 12 0 3394.56 3341.64 281.69 o 1 12 0 40453.42 38191.06 1055.02 o 2 12 0 54971.45 53804.16 2246.55 o 3 12 0 28.53 122.25 93.42 o 4 12 0 2863.27 2854.42 211.95 o 5 12 0 1925.22 1990.18 210.15 o 6 12 0 2478.26 2507.18 237.88 o 7 12 0 32865.36 34601.88 1147.20 o 8 12 0 9.72 -35.58 122.23 o 9 12 0 468.55 359.41 177.42 o 10 12 0 4184.83 4527.54 386.98 o 11 12 0 2583.80 3037.88 432.87 o 12 12 0 1076.80 1160.22 389.30 o 1 13 0 14196.42 13052.38 377.62 o 2 13 0 217.88 164.50 106.53 o 3 13 0 36189.54 35408.46 1481.84 o 4 13 0 50813.96 51214.00 2124.23 o 5 13 0 12766.69 11966.88 582.52 o 6 13 0 19537.58 19794.59 637.93 o 7 13 0 169.11 246.61 151.65 o 8 13 0 4216.83 4349.53 308.03 o 9 13 0 5222.16 5106.59 389.94 o 10 13 0 4206.93 4681.61 436.08 o 11 13 0 3499.76 3757.05 540.19 o 12 13 0 39.33 -9.81 246.59 o 0 14 0 13242.37 12636.81 541.10 o 1 14 0 14371.92 12847.73 492.24 o 2 14 0 28133.18 26643.46 607.39 o 3 14 0 26962.85 27352.47 932.48 o 4 14 0 6179.86 5858.28 297.48 o 5 14 0 20792.65 21603.87 923.65 o 6 14 0 945.62 878.16 186.96 o 7 14 0 3481.39 3601.47 282.02 o 8 14 0 2491.32 2406.33 271.99 o 9 14 0 6321.82 6795.38 511.84 o 10 14 0 2463.32 2666.29 423.86 o 11 14 0 12.09 -42.32 218.57 o 1 15 0 4343.88 3934.51 239.71 o 2 15 0 756.16 682.12 183.16 o 3 15 0 24567.24 24664.57 739.30 o 4 15 0 2.22 6.35 107.01 o 5 15 0 2027.40 2149.62 239.70 o 6 15 0 1398.76 1173.40 209.79 o 7 15 0 1032.09 1057.02 207.27 o 8 15 0 61.06 86.58 175.23 o 9 15 0 13.64 22.59 169.08 o 10 15 0 841.02 1007.21 292.20 o 11 15 0 2564.52 2639.22 512.65 o 0 16 0 0.13 -89.81 125.01 o 1 16 0 1092.94 1058.66 176.54 o 2 16 0 203.36 407.16 134.30 o 3 16 0 54.08 11.94 106.55 o 4 16 0 304.53 331.99 143.47 o 5 16 0 480.38 509.32 164.92 o 6 16 0 2.45 44.50 138.07 o 7 16 0 41.38 26.60 143.06 o 8 16 0 0.22 -22.22 167.69 o 9 16 0 1071.51 1174.33 299.95 o 10 16 0 806.99 712.09 268.73 o 11 16 0 28.76 197.47 282.54 o 1 17 0 516.01 485.72 142.78 o 2 17 0 83.13 119.14 113.43 o 3 17 0 5415.61 5053.59 298.91 o 4 17 0 5534.23 5756.54 353.03 o 5 17 0 2859.59 2800.41 302.03 o 6 17 0 2412.07 2709.82 309.56 o 7 17 0 307.95 377.07 178.50 o 8 17 0 7.17 19.97 168.13 o 9 17 0 376.86 283.38 213.53 o 10 17 0 974.53 1039.20 295.49 o 0 18 0 376.27 417.43 204.79 o 1 18 0 2559.05 2332.74 235.24 o 2 18 0 7198.45 6983.55 344.58 o 3 18 0 1728.22 2052.38 274.25 o 4 18 0 6652.75 6399.56 409.34 o 5 18 0 149.42 210.34 171.92 o 6 18 0 264.73 202.42 169.21 o 7 18 0 5217.21 5233.27 398.73 o 8 18 0 112.41 149.73 193.14 o 9 18 0 1084.47 810.23 278.09 o 10 18 0 487.07 586.19 264.97 o 1 19 0 10318.70 10280.23 496.02 o 2 19 0 85.24 25.89 127.00 o 3 19 0 593.02 723.23 207.30 o 4 19 0 5270.92 5027.85 380.36 o 5 19 0 17502.47 17104.10 847.79 o 6 19 0 1101.13 1230.12 264.14 o 7 19 0 1485.49 1491.96 292.24 o 8 19 0 1201.07 1246.97 315.79 o 9 19 0 3007.97 3051.55 436.29 o 0 20 0 2450.43 2298.58 361.77 o 1 20 0 10755.86 11300.00 578.47 o 2 20 0 1.16 -6.38 142.33 o 3 20 0 2759.13 2731.28 306.04 o 4 20 0 389.47 452.19 188.57 o 5 20 0 1932.06 1780.68 299.29 o 6 20 0 157.55 201.99 183.82 o 7 20 0 17622.38 19395.97 754.76 o 8 20 0 1459.99 1666.84 370.16 o 9 20 0 44.60 -17.57 199.12 o 1 21 0 5440.39 5330.64 375.65 o 2 21 0 5997.34 6252.82 410.56 o 3 21 0 379.37 479.67 193.98 o 4 21 0 19.41 68.18 184.69 o 5 21 0 5076.17 4756.06 398.30 o 6 21 0 5807.14 6200.90 451.82 o 7 21 0 250.59 169.21 195.86 o 8 21 0 604.23 600.08 278.77 o 0 22 0 744.78 924.44 353.11 o 1 22 0 187.19 374.84 174.59 o 2 22 0 81.51 165.01 159.86 o 3 22 0 23.28 203.23 162.91 o 4 22 0 564.29 752.80 227.28 o 5 22 0 35.14 18.47 160.24 o 6 22 0 430.65 358.50 198.10 o 7 22 0 235.18 368.88 201.51 o 8 22 0 163.84 150.54 238.30 o 1 23 0 21.77 168.78 179.41 o 2 23 0 772.37 774.98 222.19 o 3 23 0 520.70 686.80 223.77 o 4 23 0 20.87 74.50 151.07 o 5 23 0 25.27 98.79 185.64 o 6 23 0 11.27 99.90 179.19 o 7 23 0 181.29 47.74 213.42 o 0 24 0 4782.85 4866.20 626.71 o 1 24 0 277.44 292.98 193.14 o 2 24 0 141.35 435.28 209.11 o 3 24 0 1890.03 2121.04 327.86 o 4 24 0 30.21 237.66 179.33 o 5 24 0 1092.46 1176.61 278.26 o 6 24 0 1038.13 1141.84 314.60 o 1 25 0 1467.22 1649.37 335.74 o 2 25 0 260.89 520.95 232.60 o 3 25 0 3795.92 4289.12 444.69 o 4 25 0 2429.04 2658.37 358.43 o 5 25 0 154.24 308.70 228.72 o 0 26 0 37.55 120.85 296.90 o 1 26 0 835.67 1135.72 296.95 o 2 26 0 7460.69 8578.51 608.26 o 3 26 0 145.37 207.81 256.84 o 4 26 0 418.63 642.60 317.89 o 1 27 0 1236.02 2002.44 382.93 o 2 27 0 203.23 569.94 292.28 o -13 0 1 1395.60 2044.01 569.53 o -11 0 1 5031.42 3675.83 541.84 o -9 0 1 6130.79 5582.49 415.00 o -7 0 1 122116.10 128743.63 4302.88 o -5 0 1 610.45 572.09 136.99 o -3 0 1 185077.36 203471.95 5554.82 o -1 0 1 196974.95 182872.19 12107.41 o 1 0 1 143423.56 161104.41 4522.37 o 3 0 1 1285.85 1142.90 106.06 o 5 0 1 58988.79 60135.51 1617.09 o 7 0 1 116102.90 121395.85 4556.70 o 9 0 1 34.09 208.32 252.58 o 11 0 1 19789.95 19465.89 1203.96 o 13 0 1 2.34 160.02 307.66 o -13 1 1 5564.16 6002.04 540.94 o -12 1 1 74.71 211.31 189.62 o -11 1 1 17.52 31.26 176.51 o -10 1 1 314.16 260.93 204.66 o -9 1 1 47064.18 50152.21 1437.93 o -8 1 1 4304.38 4319.18 246.18 o -7 1 1 479.64 548.46 126.61 o -6 1 1 14673.87 14085.43 393.53 o -5 1 1 4562.59 4095.19 181.32 o -4 1 1 16809.58 17160.60 314.51 o -3 1 1 18844.91 18808.73 385.46 o -2 1 1 13680.48 13823.00 207.21 o -1 1 1 353155.25 331322.47 14194.00 o 0 1 1 52.33 5.66 11.01 o 1 1 1 27291.77 29955.53 475.47 o 2 1 1 13439.47 14838.21 367.92 o 3 1 1 2803.96 2686.23 135.04 o 4 1 1 61.25 84.20 62.33 o 5 1 1 46630.56 47773.34 776.62 o 6 1 1 11188.05 10971.43 343.79 o 7 1 1 20411.32 19916.56 498.72 o 8 1 1 10047.27 9676.64 296.87 o 9 1 1 276.23 177.99 171.81 o 10 1 1 2221.95 2254.83 363.84 o 11 1 1 25.21 17.47 176.89 o 12 1 1 302.65 407.24 243.38 o 13 1 1 7206.98 7331.13 593.29 o -13 2 1 2159.16 2195.50 419.55 o -12 2 1 4067.82 4195.58 444.96 o -11 2 1 266.97 193.50 183.60 o -10 2 1 1309.25 1002.46 268.29 o -9 2 1 2.83 12.83 110.46 o -8 2 1 8092.73 7805.95 308.86 o -7 2 1 5015.38 4763.37 232.90 o -6 2 1 17.84 29.09 84.08 o -5 2 1 669.16 717.18 125.05 o -4 2 1 4677.78 4154.66 193.52 o -3 2 1 7466.22 7862.99 197.65 o -2 2 1 30770.72 30921.94 951.27 o -1 2 1 4753.19 4808.36 161.80 o 0 2 1 56798.46 59741.22 2259.76 o 1 2 1 48965.25 53747.71 886.84 o 2 2 1 11667.68 12425.21 337.32 o 3 2 1 10899.36 10884.40 205.72 o 4 2 1 13003.21 13544.06 451.77 o 5 2 1 45.77 98.63 56.85 o 6 2 1 18.90 36.04 62.64 o 7 2 1 7694.30 7403.50 247.22 o 8 2 1 156.83 178.49 122.04 o 9 2 1 4671.00 4067.81 381.11 o 10 2 1 20.99 94.77 166.98 o 11 2 1 4368.48 4455.20 440.91 o 12 2 1 4992.74 4638.11 464.95 o 13 2 1 53.32 157.35 215.14 o -13 3 1 42.87 110.08 200.32 o -12 3 1 3547.21 3591.94 437.92 o -11 3 1 125.10 269.47 193.59 o -10 3 1 1.52 6.21 156.23 o -9 3 1 1.52 18.68 131.95 o -8 3 1 2602.60 2736.02 211.82 o -7 3 1 6582.95 6655.39 270.74 o -6 3 1 633.92 699.49 119.51 o -5 3 1 334.06 365.39 87.31 o -4 3 1 4298.87 4148.38 171.12 o -3 3 1 452.33 613.30 90.94 o -2 3 1 14203.01 14269.63 486.44 o -1 3 1 688.79 570.05 58.43 o 0 3 1 878.01 796.56 49.20 o 1 3 1 574.28 585.09 55.79 o 2 3 1 62834.94 67180.32 1166.39 o 3 3 1 3.75 26.16 48.10 o 4 3 1 1542.06 1469.04 104.50 o 5 3 1 276.26 277.53 71.62 o 6 3 1 3119.94 3264.70 168.85 o 7 3 1 1999.95 1899.07 153.60 o 8 3 1 2469.34 2449.57 235.72 o 9 3 1 99.44 126.57 172.76 o 10 3 1 9081.92 8770.28 553.34 o 11 3 1 47.10 95.52 170.74 o 12 3 1 248.86 157.79 202.70 o 13 3 1 9.07 47.34 190.10 o -13 4 1 986.94 1046.75 314.79 o -12 4 1 252.98 322.09 225.57 o -11 4 1 260.94 176.97 195.44 o -10 4 1 3086.35 2821.62 366.60 o -9 4 1 12785.14 11971.77 487.97 o -8 4 1 298.40 287.49 122.31 o -7 4 1 296.73 480.00 119.63 o -6 4 1 864.31 827.05 128.77 o -5 4 1 31012.95 31672.45 496.88 o -4 4 1 10240.20 10343.33 343.53 o -3 4 1 738.24 618.30 88.19 o -2 4 1 750.42 805.26 80.60 o -1 4 1 283.30 368.31 50.88 o 0 4 1 7920.26 7378.79 181.65 o 1 4 1 52414.08 54167.17 1260.50 o 2 4 1 410.37 574.32 82.26 o 3 4 1 11504.40 11253.25 368.47 o 4 4 1 1058.47 1123.53 112.29 o 5 4 1 6260.47 6795.07 227.29 o 6 4 1 1260.19 1420.25 141.46 o 7 4 1 7910.72 7755.04 275.62 o 8 4 1 5019.20 4741.84 307.70 o 9 4 1 1605.20 1441.50 300.67 o 10 4 1 890.41 978.53 265.59 o 11 4 1 727.64 878.86 275.01 o 12 4 1 428.95 490.99 249.31 o 13 4 1 635.91 642.28 271.65 o -13 5 1 735.79 840.33 298.95 o -12 5 1 57.65 72.45 201.06 o -11 5 1 14635.24 14051.76 713.73 o -10 5 1 3624.10 3458.47 373.62 o -9 5 1 61.31 0.98 131.78 o -8 5 1 841.86 929.53 166.42 o -7 5 1 739.55 824.61 144.55 o -6 5 1 6830.10 6883.45 269.72 o -5 5 1 3529.45 3320.36 183.11 o -4 5 1 6114.53 5712.89 209.05 o -3 5 1 3096.38 2704.39 137.96 o -2 5 1 513.19 717.33 83.77 o -1 5 1 378.63 438.96 65.29 o 0 5 1 39085.63 38535.76 1039.27 o 1 5 1 188115.31 194605.52 5715.41 o 2 5 1 1010.77 949.44 100.23 o 3 5 1 64543.97 67024.70 1550.45 o 4 5 1 25585.38 26657.24 835.80 o 5 5 1 6054.90 6649.79 239.33 o 6 5 1 127.04 61.74 77.94 o 7 5 1 36869.96 37491.09 778.39 o 8 5 1 8626.83 8251.42 394.68 o 9 5 1 3729.90 3202.11 439.70 o 10 5 1 4159.08 3671.67 392.93 o 11 5 1 14067.68 14112.04 734.14 o 12 5 1 629.09 706.51 268.51 o 13 5 1 48.42 193.99 217.35 o -13 6 1 2896.89 2914.80 441.11 o -12 6 1 14042.34 14135.70 822.35 o -11 6 1 2825.12 2630.72 370.18 o -10 6 1 6972.72 6395.81 479.63 o -9 6 1 8388.84 7559.10 415.89 o -8 6 1 118.02 99.00 113.40 o -7 6 1 6834.84 6325.70 283.94 o -6 6 1 15518.19 15391.00 457.14 o -5 6 1 77598.20 77391.23 1979.82 o -4 6 1 21796.59 22232.35 593.14 o -3 6 1 6420.53 6317.67 322.46 o -2 6 1 1631.11 1523.68 106.32 o -1 6 1 6744.89 6344.02 309.34 o 0 6 1 18040.99 17491.21 550.91 o 1 6 1 101284.05 101367.98 3272.92 o 2 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