# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_or _shelx_title ' ORNITHINE CHLORIDE SULPHATE NITRATE' _shelx_refln_list_code 4 _shelx_F_calc_maximum 126.50 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.7845 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' _cell_length_a 13.8720 _cell_length_b 9.5780 _cell_length_c 9.1780 _cell_angle_alpha 90.000 _cell_angle_beta 125.350 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -1 0 2121.98 2158.13 22.12 o 3 -1 0 7413.77 7531.96 15.77 o 5 -1 0 875.10 1035.86 6.35 o 7 -1 0 1380.71 1412.95 8.46 o 9 -1 0 99.01 109.62 9.14 o 11 -1 0 484.92 467.08 8.75 o 13 -1 0 153.19 169.13 21.96 o 2 0 0 256.63 364.48 3.65 o 4 0 0 2987.55 3045.75 24.80 o 6 0 0 4578.07 4500.89 19.20 o 8 0 0 8.07 -2.14 6.00 o 10 0 0 1013.60 1013.51 9.95 o 12 0 0 88.63 64.22 7.24 o 14 0 0 98.29 95.00 8.65 o 1 1 0 2184.30 2190.52 56.45 o 3 1 0 7526.53 7617.31 10.73 o 5 1 0 845.46 1009.83 6.30 o 7 1 0 1402.87 1413.10 12.13 o 9 1 0 102.89 112.09 15.73 o 11 1 0 476.51 457.16 8.81 o 13 1 0 157.36 148.39 8.37 o 0 2 0 2431.02 2094.29 8.08 o 2 2 0 4161.59 4071.44 55.95 o 4 2 0 2420.84 2353.70 15.23 o 6 2 0 541.44 573.92 6.26 o 8 2 0 543.61 558.34 7.79 o 10 2 0 42.38 23.39 7.05 o 12 2 0 5.61 -6.56 10.68 o 14 2 0 8.49 -4.55 9.18 o 1 3 0 4521.68 4196.60 74.85 o 3 3 0 9549.49 9743.59 180.35 o 5 3 0 67.52 85.63 8.56 o 7 3 0 1596.68 1784.10 9.79 o 9 3 0 45.03 24.98 6.53 o 11 3 0 137.65 125.39 21.87 o 13 3 0 103.31 91.94 9.60 o 0 4 0 1957.51 2044.75 10.88 o 2 4 0 582.39 672.42 21.71 o 4 4 0 2751.20 2613.60 48.25 o 6 4 0 1039.54 1043.46 8.15 o 8 4 0 887.99 855.60 9.14 o 10 4 0 959.72 943.81 10.22 o 12 4 0 63.74 85.47 7.78 o 1 5 0 2942.68 3005.43 23.40 o 3 5 0 87.22 103.02 5.15 o 5 5 0 559.63 621.44 7.23 o 7 5 0 491.15 491.71 14.75 o 9 5 0 19.21 8.15 12.97 o 11 5 0 263.75 232.09 21.88 o 13 5 0 47.86 62.98 12.39 o 0 6 0 36.50 8.24 8.01 o 2 6 0 70.82 68.28 5.20 o 4 6 0 184.01 151.78 7.94 o 6 6 0 87.44 89.32 6.32 o 8 6 0 27.50 19.99 6.63 o 10 6 0 67.59 61.68 7.26 o 12 6 0 11.53 16.89 8.23 o 1 7 0 325.12 329.23 11.34 o 3 7 0 596.68 566.08 8.04 o 5 7 0 350.62 361.72 15.96 o 7 7 0 723.73 721.01 20.36 o 9 7 0 84.17 93.09 7.43 o 11 7 0 374.46 383.09 11.93 o 0 8 0 1059.85 1093.72 13.91 o 2 8 0 325.57 303.87 8.60 o 4 8 0 957.20 994.42 13.99 o 6 8 0 274.30 280.10 14.21 o 8 8 0 312.70 311.62 21.13 o 10 8 0 269.13 298.91 10.61 o 1 9 0 229.36 251.55 8.04 o 3 9 0 51.69 47.51 6.72 o 5 9 0 50.01 50.82 8.60 o 7 9 0 43.59 51.48 7.48 o 9 9 0 14.02 19.23 8.05 o 0 10 0 167.55 149.83 11.66 o 2 10 0 24.38 32.22 15.84 o 4 10 0 9.48 14.64 11.86 o 6 10 0 28.45 29.17 7.70 o 8 10 0 38.77 61.17 9.05 o 1 11 0 80.33 80.07 8.00 o 3 11 0 301.86 349.34 10.00 o 5 11 0 11.89 23.84 8.10 o 0 12 0 322.81 387.31 15.25 o 2 12 0 186.72 229.53 16.84 o -15 -1 1 91.40 93.97 8.75 o -13 -1 1 72.34 59.93 7.42 o -11 -1 1 21.83 9.44 7.25 o -9 -1 1 76.80 85.02 5.95 o -7 -1 1 2648.50 2705.53 51.21 o -5 -1 1 1259.65 1323.19 37.36 o -3 -1 1 8651.54 8567.58 209.29 o -1 -1 1 673.41 666.39 24.21 o 1 -1 1 3166.50 3381.08 33.79 o 3 -1 1 6422.12 6658.39 46.78 o 5 -1 1 5.30 -2.59 4.67 o 7 -1 1 466.14 486.81 7.29 o 9 -1 1 551.74 514.19 16.59 o 11 -1 1 34.30 32.73 10.61 o 13 -1 1 42.19 37.63 10.91 o -14 0 1 37.10 17.77 8.13 o -12 0 1 137.73 125.66 7.24 o -10 0 1 2.38 18.41 6.20 o -8 0 1 553.13 608.68 20.87 o -6 0 1 1.51 -4.39 4.39 o -4 0 1 458.95 558.40 8.24 o -2 0 1 3157.31 3037.33 14.58 o 0 0 1 161.71 100.16 2.80 o 2 0 1 1770.02 1878.34 8.71 o 4 0 1 465.07 468.23 17.00 o 6 0 1 1148.17 1244.66 18.70 o 8 0 1 138.24 181.05 26.50 o 10 0 1 107.88 94.10 6.87 o 12 0 1 39.63 14.85 7.88 o -15 1 1 90.76 100.15 8.73 o -13 1 1 66.51 60.35 7.39 o -11 1 1 19.92 1.76 7.25 o -9 1 1 70.18 84.57 5.93 o -7 1 1 2709.96 2725.24 13.47 o -5 1 1 1308.64 1355.62 17.51 o -3 1 1 8581.00 8442.66 180.73 o -1 1 1 667.80 640.35 51.90 o 1 1 1 3082.08 3272.04 6.83 o 3 1 1 6427.62 6626.24 41.35 o 5 1 1 6.47 4.03 4.62 o 7 1 1 448.04 468.34 7.25 o 9 1 1 529.93 496.68 11.16 o 11 1 1 29.80 30.98 7.10 o 13 1 1 44.93 66.25 10.04 o -14 2 1 253.79 238.25 13.33 o -12 2 1 233.60 240.78 8.33 o -10 2 1 988.40 1011.67 13.69 o -8 2 1 1688.61 1613.29 9.29 o -6 2 1 83.46 70.89 23.46 o -4 2 1 5671.36 5420.05 184.01 o -2 2 1 7498.60 7468.31 381.14 o 0 2 1 12833.50 12957.53 412.32 o 2 2 1 2708.98 2697.25 8.03 o 4 2 1 2581.06 2666.45 14.08 o 6 2 1 1465.67 1516.08 8.86 o 8 2 1 1134.33 1216.91 10.58 o 10 2 1 881.21 873.43 10.07 o 12 2 1 52.44 50.21 11.47 o -13 3 1 43.72 33.01 10.58 o -11 3 1 361.29 362.24 8.45 o -9 3 1 1324.63 1313.72 31.72 o -7 3 1 822.74 816.66 18.60 o -5 3 1 1461.89 1407.42 41.85 o -3 3 1 3938.99 3930.34 240.83 o -1 3 1 1308.84 1316.19 54.41 o 1 3 1 424.79 391.56 4.96 o 3 3 1 188.74 191.61 5.12 o 5 3 1 691.45 680.62 6.81 o 7 3 1 71.23 64.02 6.06 o 9 3 1 247.31 197.41 7.87 o 11 3 1 318.26 308.00 9.16 o 13 3 1 10.17 16.15 8.90 o -14 4 1 24.89 28.01 8.30 o -12 4 1 62.67 64.41 7.42 o -10 4 1 58.26 50.13 6.94 o -8 4 1 149.95 126.16 8.69 o -6 4 1 500.16 562.64 11.35 o -4 4 1 1137.65 1249.46 55.45 o -2 4 1 450.51 550.92 17.98 o 0 4 1 2470.98 2757.89 44.44 o 2 4 1 47.87 39.94 5.73 o 4 4 1 711.18 780.27 6.95 o 6 4 1 658.27 643.21 7.93 o 8 4 1 1181.01 1160.90 10.25 o 10 4 1 7.35 7.72 15.19 o 12 4 1 10.30 0.01 8.83 o -13 5 1 116.86 129.38 8.25 o -11 5 1 556.35 580.62 23.07 o -9 5 1 556.00 538.33 8.80 o -7 5 1 1066.95 1094.25 20.27 o -5 5 1 573.33 551.56 6.81 o -3 5 1 154.66 160.83 7.07 o -1 5 1 791.25 675.42 16.78 o 1 5 1 1181.32 1130.84 59.72 o 3 5 1 1257.99 1377.31 8.34 o 5 5 1 409.82 445.45 28.70 o 7 5 1 1434.07 1481.02 10.91 o 9 5 1 159.95 175.96 9.43 o 11 5 1 296.94 298.48 9.50 o -12 6 1 20.52 19.82 13.35 o -10 6 1 509.39 497.33 9.26 o -8 6 1 1546.98 1510.95 28.26 o -6 6 1 1718.05 1706.34 46.46 o -4 6 1 1581.39 1693.75 95.70 o -2 6 1 301.95 322.73 13.42 o 0 6 1 101.94 90.47 5.26 o 2 6 1 370.12 362.49 6.73 o 4 6 1 1057.78 1119.17 9.15 o 6 6 1 89.99 99.17 6.62 o 8 6 1 93.21 98.63 6.97 o 10 6 1 63.86 51.09 7.87 o -11 7 1 21.55 19.45 7.67 o -9 7 1 44.03 54.30 10.02 o -7 7 1 99.35 65.98 6.78 o -5 7 1 11.84 25.80 13.59 o -3 7 1 20.30 24.86 5.85 o -1 7 1 359.49 391.98 7.37 o 1 7 1 293.78 262.12 14.91 o 3 7 1 543.38 570.65 8.23 o 5 7 1 184.94 155.37 7.62 o 7 7 1 59.03 63.22 6.82 o 9 7 1 134.30 132.23 7.99 o -10 8 1 34.09 26.26 19.16 o -8 8 1 119.00 116.85 9.37 o -6 8 1 107.84 102.25 6.88 o -4 8 1 124.79 115.40 6.75 o -2 8 1 437.91 463.15 8.33 o 0 8 1 195.51 204.65 7.58 o 2 8 1 63.03 86.57 16.33 o 4 8 1 149.46 137.69 8.75 o 6 8 1 66.45 71.19 8.29 o 8 8 1 100.19 109.74 11.48 o -9 9 1 88.81 85.92 8.11 o -7 9 1 584.49 580.59 9.88 o -5 9 1 149.64 172.24 7.92 o -3 9 1 541.60 537.58 23.34 o -1 9 1 614.42 592.94 9.24 o 1 9 1 127.91 110.73 7.03 o 3 9 1 316.10 334.73 17.55 o 5 9 1 114.33 139.15 7.83 o 7 9 1 115.03 129.61 11.25 o -8 10 1 9.24 7.80 8.41 o -6 10 1 175.67 200.04 9.05 o -4 10 1 123.48 123.20 7.56 o -2 10 1 181.41 192.60 14.75 o 0 10 1 630.85 706.10 15.68 o 2 10 1 343.45 384.18 9.33 o 4 10 1 196.71 226.34 8.89 o 6 10 1 157.38 161.56 8.89 o -7 11 1 13.63 6.42 9.40 o -5 11 1 94.13 127.57 8.34 o -3 11 1 21.55 17.81 7.97 o -1 11 1 14.23 6.87 8.51 o 1 11 1 275.76 319.67 9.69 o 3 11 1 12.84 16.91 8.18 o 5 11 1 42.11 68.08 8.58 o -2 12 1 112.53 141.06 9.16 o 0 12 1 173.31 193.61 10.13 o -15 -1 2 30.61 30.39 11.54 o -13 -1 2 73.56 79.75 9.96 o -11 -1 2 106.19 118.20 9.23 o -9 -1 2 390.95 448.30 9.68 o -7 -1 2 685.00 675.09 8.62 o -5 -1 2 1053.93 1071.27 8.44 o -3 -1 2 327.61 370.95 6.21 o -1 -1 2 8749.92 8697.63 15.14 o 1 -1 2 1918.47 1949.50 9.98 o 3 -1 2 487.13 465.57 7.78 o 5 -1 2 2227.32 2156.35 14.09 o 7 -1 2 817.11 832.86 12.81 o 9 -1 2 53.54 36.93 10.01 o 11 -1 2 15.82 23.04 11.00 o -14 0 2 629.95 636.62 14.23 o -12 0 2 1320.21 1352.64 15.49 o -10 0 2 687.60 719.70 11.68 o -8 0 2 606.08 627.88 9.29 o -6 0 2 8.02 -6.06 6.06 o -4 0 2 16001.91 16100.69 21.49 o -2 0 2 4879.69 5199.76 11.46 o 0 0 2 4928.36 5163.60 12.71 o 2 0 2 4416.25 4394.57 14.17 o 4 0 2 87.56 116.60 7.15 o 6 0 2 2888.87 2998.21 17.26 o 8 0 2 1024.56 1114.56 14.51 o 10 0 2 239.04 222.31 12.42 o 12 0 2 183.86 152.12 12.54 o -15 1 2 30.15 17.80 11.46 o -13 1 2 79.23 81.15 10.00 o -11 1 2 113.99 112.47 9.46 o -9 1 2 375.62 450.14 9.82 o -7 1 2 691.49 641.75 8.66 o -5 1 2 1054.94 1043.98 8.61 o -3 1 2 336.25 392.28 6.59 o -1 1 2 8809.95 8437.20 15.04 o 1 1 2 1966.19 1923.78 10.00 o 3 1 2 488.45 462.25 7.72 o 5 1 2 2257.77 2197.59 14.13 o 7 1 2 827.91 806.20 12.76 o 9 1 2 54.91 51.80 9.80 o 11 1 2 17.64 11.25 11.97 o -14 2 2 19.08 27.80 10.27 o -12 2 2 266.61 241.01 11.64 o -10 2 2 222.14 216.84 10.39 o -8 2 2 782.91 734.60 10.22 o -6 2 2 132.31 164.46 6.97 o -4 2 2 824.44 857.15 8.36 o -2 2 2 105.97 90.12 6.34 o 0 2 2 708.13 672.52 7.82 o 2 2 2 4901.18 4959.56 15.81 o 4 2 2 1468.61 1515.47 11.78 o 6 2 2 241.09 259.99 10.07 o 8 2 2 50.37 35.40 9.70 o 10 2 2 147.80 144.02 10.76 o 12 2 2 3.96 -3.51 13.29 o -15 3 2 105.86 118.72 12.17 o -13 3 2 79.77 73.42 10.34 o -11 3 2 1114.85 1128.97 14.48 o -9 3 2 56.05 56.60 8.59 o -7 3 2 217.79 171.83 8.08 o -5 3 2 1258.20 1215.61 9.66 o -3 3 2 701.52 617.36 7.82 o -1 3 2 2533.69 2340.55 11.17 o 1 3 2 587.59 616.02 8.03 o 3 3 2 2713.25 2860.70 14.47 o 5 3 2 568.91 595.94 10.76 o 7 3 2 164.81 202.28 10.80 o 9 3 2 258.94 278.82 12.20 o 11 3 2 108.86 101.47 11.56 o -14 4 2 128.84 126.35 11.60 o -12 4 2 170.62 184.78 11.59 o -10 4 2 355.07 334.44 11.66 o -8 4 2 1892.08 1797.99 14.46 o -6 4 2 1269.73 1222.31 11.19 o -4 4 2 1155.62 1173.97 9.92 o -2 4 2 401.56 342.18 7.68 o 0 4 2 2410.14 2314.78 12.48 o 2 4 2 1596.28 1624.66 11.95 o 4 4 2 633.89 592.38 10.50 o 6 4 2 1711.24 1578.87 15.33 o 8 4 2 245.41 224.76 11.76 o 10 4 2 178.90 160.14 11.64 o -13 5 2 95.06 103.13 10.99 o -11 5 2 359.51 419.09 12.31 o -9 5 2 180.55 195.42 10.78 o -7 5 2 862.18 817.06 11.68 o -5 5 2 543.84 608.15 9.68 o -3 5 2 498.42 401.43 8.53 o -1 5 2 628.19 519.63 8.98 o 1 5 2 773.35 837.98 10.48 o 3 5 2 50.65 71.17 8.11 o 5 5 2 165.26 200.40 10.50 o 7 5 2 93.05 60.75 10.07 o 9 5 2 161.50 154.70 11.12 o 11 5 2 91.86 90.38 12.46 o -14 6 2 30.72 13.62 12.28 o -12 6 2 33.16 40.70 10.59 o -10 6 2 430.17 426.12 12.70 o -8 6 2 129.44 155.86 10.58 o -6 6 2 565.30 554.13 11.18 o -4 6 2 20.43 19.45 7.61 o -2 6 2 276.96 305.83 9.53 o 0 6 2 417.80 399.38 10.06 o 2 6 2 219.86 245.19 10.10 o 4 6 2 36.32 53.30 9.09 o 6 6 2 451.10 443.23 12.37 o 8 6 2 29.40 20.73 10.29 o 10 6 2 41.43 32.57 11.81 o -13 7 2 64.42 84.00 12.05 o -11 7 2 153.13 153.04 10.87 o -9 7 2 722.51 731.16 13.67 o -7 7 2 759.77 761.93 12.98 o -5 7 2 511.98 452.52 11.24 o -3 7 2 1000.66 968.94 12.61 o -1 7 2 531.41 521.83 11.71 o 1 7 2 260.83 306.36 10.92 o 3 7 2 1095.48 1101.74 14.47 o 5 7 2 178.73 150.08 11.25 o 7 7 2 116.45 123.95 10.77 o 9 7 2 249.09 241.92 13.99 o -12 8 2 98.27 116.67 12.30 o -10 8 2 183.04 214.64 12.40 o -8 8 2 189.63 205.49 11.33 o -6 8 2 932.55 907.69 13.88 o -4 8 2 409.86 372.12 11.48 o -2 8 2 517.16 516.09 12.61 o 0 8 2 1156.91 1245.24 14.93 o 2 8 2 581.72 563.02 13.01 o 4 8 2 556.37 578.96 13.33 o 6 8 2 337.10 381.09 13.52 o 8 8 2 72.31 53.77 11.93 o -11 9 2 73.17 97.81 12.08 o -9 9 2 125.80 114.77 11.32 o -7 9 2 5.32 -2.80 10.90 o -5 9 2 65.04 98.63 10.20 o -3 9 2 798.38 773.75 13.87 o -1 9 2 303.75 291.97 12.04 o 1 9 2 26.29 8.44 10.81 o 3 9 2 81.10 85.87 10.47 o 5 9 2 87.60 67.49 11.32 o 7 9 2 10.12 -11.57 12.94 o -8 10 2 45.65 41.28 11.17 o -6 10 2 57.51 51.23 10.68 o -4 10 2 55.01 62.58 10.50 o -2 10 2 24.29 39.61 10.52 o 0 10 2 29.04 50.99 10.83 o 2 10 2 21.68 4.11 11.79 o 4 10 2 67.69 70.44 11.44 o 6 10 2 12.99 31.28 12.33 o -7 11 2 22.25 8.84 13.21 o -5 11 2 84.19 73.74 11.89 o -3 11 2 320.93 320.77 14.72 o -1 11 2 222.32 216.26 13.59 o 1 11 2 112.99 112.69 12.17 o 3 11 2 187.50 213.40 14.11 o -2 12 2 139.80 176.59 13.66 o -15 -1 3 108.98 107.97 11.57 o -13 -1 3 296.95 277.16 11.69 o -11 -1 3 58.17 29.83 9.37 o -9 -1 3 135.77 141.60 8.56 o -7 -1 3 175.83 164.25 7.14 o -5 -1 3 279.13 261.38 6.77 o -3 -1 3 12878.36 13130.45 20.99 o -1 -1 3 433.64 424.29 7.08 o 1 -1 3 245.75 259.88 7.09 o 3 -1 3 417.50 420.51 8.85 o 5 -1 3 1630.78 1635.41 14.51 o 7 -1 3 30.11 11.93 9.44 o 9 -1 3 327.03 335.55 12.80 o 11 -1 3 102.25 104.10 12.34 o -16 0 3 48.17 46.17 11.99 o -14 0 3 49.07 37.87 10.37 o -12 0 3 172.70 152.28 10.98 o -10 0 3 0.48 -2.90 8.93 o -8 0 3 1574.30 1599.87 11.76 o -6 0 3 524.12 521.13 7.83 o -4 0 3 4237.13 4155.74 12.96 o -2 0 3 4195.70 4582.08 13.48 o 0 0 3 2437.90 2588.04 11.62 o 2 0 3 360.86 376.66 7.83 o 4 0 3 697.63 690.96 10.49 o 6 0 3 0.10 -9.90 9.90 o 8 0 3 385.08 378.53 12.54 o 10 0 3 43.27 26.53 11.05 o -15 1 3 107.58 116.92 11.69 o -13 1 3 291.92 263.87 12.03 o -11 1 3 65.29 74.10 9.20 o -9 1 3 130.88 144.45 8.72 o -7 1 3 184.05 159.02 7.33 o -5 1 3 257.72 253.57 7.04 o -3 1 3 12730.62 12818.54 20.90 o -1 1 3 435.96 427.04 7.28 o 1 1 3 256.45 277.27 7.17 o 3 1 3 406.22 412.84 8.92 o 5 1 3 1616.03 1639.33 14.56 o 7 1 3 29.87 18.15 9.39 o 9 1 3 328.66 331.57 12.85 o 11 1 3 100.02 103.16 12.23 o -16 2 3 320.63 310.05 15.27 o -14 2 3 213.66 213.37 12.13 o -12 2 3 418.64 379.72 12.11 o -10 2 3 594.35 570.43 11.56 o -8 2 3 1203.95 1199.08 11.51 o -6 2 3 1947.14 2002.95 11.69 o -4 2 3 3259.28 2935.71 12.26 o -2 2 3 14305.58 13642.12 23.34 o 0 2 3 228.51 261.16 7.34 o 2 2 3 3282.49 3210.96 15.05 o 4 2 3 1979.03 1980.70 14.49 o 6 2 3 329.55 401.24 11.45 o 8 2 3 747.10 701.59 13.91 o 10 2 3 129.46 121.52 11.79 o -15 3 3 48.70 49.49 11.28 o -13 3 3 204.69 212.71 11.83 o -11 3 3 28.46 10.44 10.36 o -9 3 3 696.16 716.51 11.73 o -7 3 3 464.19 513.12 9.42 o -5 3 3 2121.11 2041.53 12.03 o -3 3 3 2368.28 2367.13 11.91 o -1 3 3 585.07 572.70 8.24 o 1 3 3 1366.39 1458.47 11.30 o 3 3 3 97.60 85.57 7.70 o 5 3 3 247.74 259.80 10.66 o 7 3 3 327.91 318.14 12.04 o 9 3 3 43.75 22.95 10.80 o -14 4 3 1.07 -11.57 11.57 o -12 4 3 221.00 206.85 11.83 o -10 4 3 175.29 185.68 11.00 o -8 4 3 101.77 72.44 8.75 o -6 4 3 257.62 261.56 9.34 o -4 4 3 1573.74 1281.33 10.88 o -2 4 3 1952.22 1925.15 12.32 o 0 4 3 49.21 49.11 7.10 o 2 4 3 1774.08 1848.78 13.83 o 4 4 3 503.75 503.02 11.41 o 6 4 3 821.60 802.31 13.73 o 8 4 3 176.24 161.40 12.18 o 10 4 3 34.83 36.19 11.90 o -15 5 3 28.29 24.47 12.08 o -13 5 3 35.98 28.82 10.53 o -11 5 3 245.44 230.85 11.63 o -9 5 3 1303.69 1227.61 14.47 o -7 5 3 200.90 191.46 9.63 o -5 5 3 2784.59 2551.13 15.26 o -3 5 3 1943.02 1697.60 12.76 o -1 5 3 2330.90 2137.67 14.20 o 1 5 3 1619.27 1724.42 14.03 o 3 5 3 123.26 117.40 9.08 o 5 5 3 412.52 406.40 12.15 o 7 5 3 48.20 49.14 10.07 o 9 5 3 94.54 109.29 11.69 o -14 6 3 30.97 39.53 11.54 o -12 6 3 344.75 308.37 13.07 o -10 6 3 341.91 339.11 12.00 o -8 6 3 737.57 689.35 12.83 o -6 6 3 1426.91 1365.25 14.17 o -4 6 3 54.83 50.88 8.44 o -2 6 3 380.77 380.95 10.61 o 0 6 3 930.44 922.30 12.84 o 2 6 3 396.42 430.45 11.63 o 4 6 3 299.45 280.74 11.73 o 6 6 3 95.68 60.53 10.75 o 8 6 3 214.89 209.12 13.22 o -13 7 3 13.09 12.28 11.42 o -11 7 3 23.61 2.02 11.18 o -9 7 3 217.79 195.84 11.48 o -7 7 3 88.71 63.22 9.50 o -5 7 3 158.59 195.53 10.58 o -3 7 3 1301.76 1243.83 14.08 o -1 7 3 135.80 180.13 10.79 o 1 7 3 292.14 282.56 11.46 o 3 7 3 506.96 448.88 12.47 o 5 7 3 146.56 149.61 10.90 o 7 7 3 37.70 18.45 11.32 o -12 8 3 28.28 48.17 11.57 o -10 8 3 116.59 106.73 10.85 o -8 8 3 123.80 107.46 10.23 o -6 8 3 210.91 183.27 11.30 o -4 8 3 135.14 140.19 10.05 o -2 8 3 461.51 400.07 12.51 o 0 8 3 188.94 156.60 11.42 o 2 8 3 72.13 96.55 10.09 o 4 8 3 50.38 41.98 10.58 o 6 8 3 12.20 29.47 11.19 o -11 9 3 23.64 50.16 11.59 o -9 9 3 123.55 116.84 11.31 o -7 9 3 121.65 126.90 10.68 o -5 9 3 355.38 372.34 12.45 o -3 9 3 31.65 36.67 10.32 o -1 9 3 78.25 78.95 10.31 o 1 9 3 297.63 284.86 12.72 o 3 9 3 103.31 115.10 11.25 o 5 9 3 158.49 147.16 12.20 o -10 10 3 94.84 106.19 12.58 o -8 10 3 71.21 53.86 11.35 o -6 10 3 365.63 359.90 13.62 o -4 10 3 248.84 239.92 12.47 o -2 10 3 277.82 270.54 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