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Acta Cryst. (2004). E60, m625-m627  [ doi:10.1107/S1600536804008980 ]

[mu]-1,2-Bis(dicyclohexylphosphino)ethane-[kappa]2P:P'-bis{[1,2-bis(dicyclohexylphosphino)ethane-[kappa]2P,P']palladium(0)}

R. C. Boyle, J. T. Mague and M. J. Fink

Abstract: The title compound, [Pd2(C26H48P2)3], crystallizes in an `extended' conformation with crystallographically imposed centrosymmetry. The crystal used was twinned via a 180° rotation about the reciprocal axis (0,0,1). The ratio of the two twin components is 54.16  (4):46.84  (4). The crystal packing involves significant interdigitation of the cyclohexyl groups with a considerable number of short H...H contacts.

Online 24 April 2004


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