Acta Cryst. (2004). E60, m644-m646  [ doi:10.1107/S1600536804009389 ]

(Acetato-O)(diacetyl monoxime benzoylhydrazonato-³O,O',N)(quinoline-N)zinc(II) quinoline hemisolvate

S. Gao, L.-H. Huo, J.-W. Liu, C. Wang, J.-G. Zhao and S. W. Ng

Online 24 April 2004

Key indicators

• Single-crystal X-ray study
• T = 293 K
• R factor = 0.051
• wR factor = 0.135
• Data-to-parameter ratio = 18.0

checkCIF/PLATON results

No syntax errors found



Alert level A
PLAT241_ALERT_2_A Check High   U(eq) as Compared to Neighbors ....        C24     
PLAT241_ALERT_2_A Check High   U(eq) as Compared to Neighbors ....        C32     

Alert level B
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.57 Ratio 
PLAT241_ALERT_2_B Check High   U(eq) as Compared to Neighbors ....        C31     
PLAT242_ALERT_2_B Check Low    U(eq) as Compared to Neighbors ....        C38     
PLAT414_ALERT_2_B Short Intra D-H..H-X       H1     ..  H9C     ..       1.89 Ang.  

Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio 
PLAT165_ALERT_3_C Nr. of Status R Flagged Non-Hydrogen Atoms .....         20       
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.63 Ratio 
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....         N7     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C33     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C37     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C25     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C27     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C29     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C34     
PLAT301_ALERT_3_C Main Residue  Disorder .........................      14.00 Perc. 
PLAT414_ALERT_2_C Short Intra D-H..H-X       H1     ..  H7      ..       1.90 Ang.  
PLAT420_ALERT_2_C D-H Without Acceptor       N1     -   H1     ...          ?       

   2 ALERT level A = In general: serious problem
   4 ALERT level B = Potentially serious problem
  15 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  15 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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