Acta Cryst. (2004). E60, m530-m531  [ doi:10.1107/S1600536804007482 ]

Tetracarbonyl{2-[1-(2,6-dimethylphenylimino)ethyl]pyridine-²N,N'}molybdenum(0)

A. Mentes and O. Büyükgüngör

Online 9 April 2004

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.004 Å
• R factor = 0.023
• wR factor = 0.060
• Data-to-parameter ratio = 15.6

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Mo1    -   C17     ..      11.08 su    
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Mo1    -   C19     ..      11.01 su    

Alert level C
PLAT230_ALERT_2_C Hirshfeld Test Diff for    O2     -   C17     ..       6.66 su    
PLAT230_ALERT_2_C Hirshfeld Test Diff for    O4     -   C19     ..       6.52 su    
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Mo1    -   C16     ..       8.58 su    
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Mo1    -   C18     ..       9.40 su    
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......         C7     
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......        C15     

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   6 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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