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Acta Cryst. (2004). E60, m705-m707  [ doi:10.1107/S1600536804009791 ]

(Ethylenediamine-[kappa]2N)(triethylenetetramine-[kappa]4N)nickel hexafluorogermanate

G.-M. Wang, Y.-Q. Sun and G.-Y. Yang

Abstract: The title compound, [Ni(en)(TETA)][GeF6] or [Ni(C2H8N2)(C6H18N4)][GeF6], was synthesized under mild solvothermal conditions in the presence of triethylenetetramine (TETA) as a base. It is a new salt composed of [GeF6]2- anions and [Ni(en)(TETA)]2+ cations. The ions are linked together by hydrogen bonding between F atoms and N-H groups. The complex cation and anion lie on twofold axes of the space group Pccn.

Online 30 April 2004


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