Acta Cryst. (2004). E60, m606-m608  [ doi:10.1107/S1600536804008839 ]

Ethanol(ethoxy)[3-methoxysalicylaldehyde (4-methoxybenzoyl)hydrazonato-³O,N,O']oxovanadium(V)

L.-H. Huo, S. Gao, J.-W. Liu, H. Zhao and S. W. Ng

Online 24 April 2004

Key indicators

• Single-crystal X-ray study
• T = 293 K
• R factor = 0.060
• wR factor = 0.148
• Data-to-parameter ratio = 17.8

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.09 Ratio 
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.38 Ratio 
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....         C6     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C20     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....       C20'     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....         O5     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....         O6     
PLAT301_ALERT_3_C Main Residue  Disorder .........................      12.00 Perc. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   6 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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