[HTML version][PDF version] [Open access]

[Contents scheme]

Acta Cryst. (2004). E60, o1034-o1037  [ doi:10.1107/S1600536804011511 ]

Bis(5-amino-3-methyl-1-phenyl-1H-pyrazol-4-yl)-3,4,5-trimethoxyphenylmethane: sheets built from N-H...N and N-H...O hydrogen bonds

J. N. Low, J. Cobo, J. Portilla, J. Quiroga and C. Glidewell

Abstract: In molecules of the title compound, C30H32N6O3, there is an intramolecular N-H...N hydrogen bond [H...N = 2.28 Å, N...N = 3.194 (3) Å and N-H...N = 167°]. The molecules are linked by an N-H...O hydrogen bond [H...O = 2.37 Å, N...O = 3.255 (3) Å and N-H...O = 154°] into C(10) chains along [100], and by an intermolecular N-H...N hydrogen bond [H...N = 2.06 Å, N...N = 2.958 (3) Å and N-H...N = 155°] into C(8) chains along [001]; these chains combine to generate (010) sheets.

Online 22 May 2004


Copyright © International Union of Crystallography
IUCr Webmaster