# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Template texray.inf' _shelx_refln_list_code 4 _shelx_F_calc_maximum 562.38 _exptl_crystal_F_000 1656.00 _reflns_d_resolution_high 0.7091 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 13.8888 _cell_length_b 18.8359 _cell_length_c 13.9301 _cell_angle_alpha 90.000 _cell_angle_beta 116.545 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 66605.39 72227.66 2078.11 o 4 0 0 91192.56 99100.12 2875.68 o 6 0 0 4478.56 4983.60 263.83 o 8 0 0 51310.52 52833.09 1684.01 o 10 0 0 119.88 225.20 131.92 o 12 0 0 27590.06 27825.13 1087.90 o 14 0 0 7509.48 6962.35 480.20 o 16 0 0 120.23 6.34 145.44 o 1 1 0 268731.19 228424.34 3796.97 o 2 1 0 26.37 28.13 19.68 o 3 1 0 499.70 584.11 56.79 o 4 1 0 402.03 361.99 95.49 o 5 1 0 21833.18 22807.65 537.20 o 6 1 0 374.36 452.70 71.66 o 7 1 0 2.78 56.02 48.94 o 8 1 0 300.92 340.58 78.04 o 9 1 0 4884.78 4895.79 222.66 o 10 1 0 1394.11 1112.59 145.99 o 11 1 0 5785.49 5974.96 279.84 o 12 1 0 206.47 141.80 94.32 o 13 1 0 14555.46 13915.70 493.05 o 14 1 0 211.39 281.37 158.69 o 15 1 0 2921.15 3639.30 280.61 o 16 1 0 27.35 86.77 96.88 o 17 1 0 452.65 613.62 95.31 o 0 2 0 100498.66 109652.09 2144.46 o 1 2 0 334.68 348.13 17.05 o 2 2 0 13467.33 14562.69 267.85 o 3 2 0 10753.04 11649.20 253.09 o 4 2 0 4009.84 4407.64 151.83 o 5 2 0 3500.18 3658.25 150.41 o 6 2 0 2017.22 2066.98 121.85 o 7 2 0 1150.19 1161.68 106.13 o 8 2 0 522.22 497.49 88.43 o 9 2 0 2299.24 2079.67 155.08 o 10 2 0 1233.39 1199.10 142.23 o 11 2 0 905.98 795.97 129.17 o 12 2 0 8687.81 8580.65 354.61 o 13 2 0 2225.67 1945.38 201.68 o 14 2 0 4936.94 4777.20 524.91 o 15 2 0 51.31 224.90 84.86 o 16 2 0 123.70 179.82 67.92 o 17 2 0 676.45 980.62 142.16 o 1 3 0 13808.41 15723.63 209.26 o 2 3 0 5306.52 5835.15 96.91 o 3 3 0 40282.12 42563.30 728.86 o 4 3 0 10548.16 10894.19 303.71 o 5 3 0 42526.44 45025.36 981.03 o 6 3 0 4600.94 4874.99 184.72 o 7 3 0 174.52 234.96 64.74 o 8 3 0 1586.60 1617.16 131.70 o 9 3 0 4262.55 3899.56 276.53 o 10 3 0 1391.62 1470.04 151.00 o 11 3 0 6804.55 6834.04 298.96 o 12 3 0 4626.75 4579.12 489.31 o 13 3 0 408.70 377.45 295.30 o 14 3 0 1661.78 1771.33 227.68 o 15 3 0 444.16 495.30 104.47 o 16 3 0 217.85 112.29 89.59 o 17 3 0 381.67 397.41 185.91 o 0 4 0 31496.67 35791.95 718.20 o 1 4 0 1182.41 1308.71 40.04 o 2 4 0 2279.70 2471.14 67.75 o 3 4 0 1575.10 1579.85 67.48 o 4 4 0 94667.48 97202.54 1616.04 o 5 4 0 1395.47 1514.24 82.58 o 6 4 0 5260.56 5042.74 191.48 o 7 4 0 121.33 45.09 51.95 o 8 4 0 35173.23 34615.42 828.47 o 9 4 0 8.22 68.76 71.49 o 10 4 0 15719.48 15549.66 695.46 o 11 4 0 71.18 74.93 79.09 o 12 4 0 965.16 936.67 148.61 o 13 4 0 470.05 502.89 129.77 o 14 4 0 27.60 19.18 63.32 o 15 4 0 49.95 71.93 76.69 o 16 4 0 1841.46 1895.62 180.33 o 17 4 0 322.88 460.41 116.75 o 1 5 0 22261.12 24749.01 327.28 o 2 5 0 1541.52 1527.77 49.17 o 3 5 0 52819.61 55096.63 708.41 o 4 5 0 466.36 533.57 53.97 o 5 5 0 69145.55 72701.95 1243.38 o 6 5 0 1150.68 1105.91 109.98 o 7 5 0 18911.30 18463.69 487.64 o 8 5 0 2018.04 2055.45 144.99 o 9 5 0 25826.53 24665.70 651.04 o 10 5 0 26.00 67.61 80.40 o 11 5 0 770.98 697.52 147.37 o 12 5 0 71.67 74.31 95.32 o 13 5 0 2031.23 2169.97 292.77 o 14 5 0 20.07 95.48 71.97 o 15 5 0 571.92 750.64 119.71 o 16 5 0 6.04 81.12 81.90 o 17 5 0 1831.48 1939.31 188.18 o 0 6 0 7335.75 7893.25 164.06 o 1 6 0 6.68 -6.10 18.89 o 2 6 0 1114.06 993.48 40.24 o 3 6 0 105.14 133.10 21.04 o 4 6 0 39083.99 38881.93 695.21 o 5 6 0 404.50 444.57 56.65 o 6 6 0 3945.23 3526.71 133.92 o 7 6 0 9561.73 9229.72 248.24 o 8 6 0 11723.81 11362.52 359.93 o 9 6 0 987.52 989.66 122.43 o 10 6 0 11832.21 10583.05 1622.47 o 11 6 0 0.27 -27.38 76.23 o 12 6 0 204.29 210.27 77.42 o 13 6 0 475.36 625.89 129.58 o 14 6 0 73.05 127.75 124.30 o 15 6 0 0.19 38.89 92.57 o 16 6 0 1376.93 1529.35 168.01 o 17 6 0 120.79 304.42 124.00 o 1 7 0 1980.60 1849.06 53.17 o 2 7 0 2151.26 2232.77 61.60 o 3 7 0 234.11 599.18 100.43 o 4 7 0 1.44 -20.50 20.50 o 5 7 0 6397.58 6392.55 156.59 o 6 7 0 612.00 566.89 75.19 o 7 7 0 54.28 31.55 48.73 o 8 7 0 6272.16 6251.40 250.73 o 9 7 0 4277.44 4051.15 212.29 o 10 7 0 3578.87 3551.44 215.28 o 11 7 0 3232.71 3134.47 176.23 o 12 7 0 821.14 709.06 132.13 o 13 7 0 92.48 153.76 82.22 o 14 7 0 2211.29 2539.22 188.33 o 15 7 0 685.32 775.39 131.31 o 16 7 0 216.44 231.03 127.97 o 0 8 0 104124.54 108996.03 1756.17 o 1 8 0 321.12 364.78 30.19 o 2 8 0 1598.43 1309.79 50.33 o 3 8 0 1963.22 2037.08 65.65 o 4 8 0 3333.03 3693.55 80.91 o 5 8 0 148.85 153.08 48.76 o 6 8 0 2608.71 2491.00 130.58 o 7 8 0 4822.66 4433.19 144.40 o 8 8 0 2183.82 2364.49 117.60 o 9 8 0 3500.23 3287.57 160.89 o 10 8 0 2.31 -31.76 89.06 o 11 8 0 606.56 565.68 90.54 o 12 8 0 5329.36 5090.92 492.73 o 13 8 0 1271.86 1220.32 134.42 o 14 8 0 3382.68 3504.61 216.29 o 15 8 0 34.09 -94.76 94.76 o 16 8 0 52.39 303.15 117.21 o 1 9 0 98992.58 104615.41 1311.78 o 2 9 0 159.34 200.72 30.39 o 3 9 0 221.29 308.79 35.25 o 4 9 0 2418.41 2517.14 68.97 o 5 9 0 20184.71 21410.68 377.52 o 6 9 0 1966.71 1935.88 96.52 o 7 9 0 63.82 90.92 55.61 o 8 9 0 2558.56 2386.75 120.31 o 9 9 0 5145.79 4836.78 202.69 o 10 9 0 75.93 76.58 58.98 o 11 9 0 1595.94 1832.58 230.55 o 12 9 0 83.28 47.78 91.92 o 13 9 0 8675.09 9587.63 327.35 o 14 9 0 670.03 728.95 157.13 o 15 9 0 1274.01 1151.34 192.89 o 16 9 0 1.10 -62.62 98.83 o 0 10 0 190740.00 196090.63 3128.57 o 1 10 0 708.13 846.59 46.43 o 2 10 0 16473.18 16843.46 421.25 o 3 10 0 10203.90 10226.16 177.94 o 4 10 0 30638.54 30809.29 396.45 o 5 10 0 2.69 22.50 31.03 o 6 10 0 10377.55 9827.12 226.56 o 7 10 0 1198.21 1172.02 90.09 o 8 10 0 12510.69 12074.14 278.59 o 9 10 0 818.94 733.43 85.41 o 10 10 0 475.38 453.81 82.18 o 11 10 0 177.39 123.42 74.10 o 12 10 0 14352.74 14011.14 508.46 o 13 10 0 408.38 462.95 142.09 o 14 10 0 5138.51 4764.52 323.82 o 15 10 0 221.78 322.43 136.40 o 16 10 0 92.38 -99.99 99.99 o 1 11 0 47530.60 48603.50 645.31 o 2 11 0 414.42 457.54 40.90 o 3 11 0 17.76 54.97 31.91 o 4 11 0 6747.18 6557.68 124.17 o 5 11 0 10096.78 9891.50 167.62 o 6 11 0 4753.14 4320.54 143.93 o 7 11 0 184.38 252.85 66.60 o 8 11 0 1612.23 1675.39 110.28 o 9 11 0 2583.06 2669.22 175.67 o 10 11 0 417.92 519.23 116.17 o 11 11 0 3048.35 3241.21 244.58 o 12 11 0 587.13 660.24 141.77 o 13 11 0 9998.74 9729.98 431.62 o 14 11 0 99.15 153.72 125.18 o 15 11 0 827.53 990.28 189.23 o 0 12 0 18780.34 18418.21 369.64 o 1 12 0 214.31 196.16 33.82 o 2 12 0 13234.89 13466.96 223.86 o 3 12 0 4622.71 4416.14 111.05 o 4 12 0 2613.63 2678.71 124.92 o 5 12 0 4541.37 4240.37 117.39 o 6 12 0 431.65 474.27 80.94 o 7 12 0 2600.33 2591.55 123.57 o 8 12 0 9.26 -53.57 92.38 o 9 12 0 726.93 894.19 117.59 o 10 12 0 719.73 645.51 107.61 o 11 12 0 300.58 445.54 123.39 o 12 12 0 2931.13 3205.23 263.95 o 13 12 0 1646.72 1779.25 220.14 o 14 12 0 1739.05 1651.42 276.25 o 15 12 0 30.99 77.11 126.95 o 1 13 0 8761.33 8401.98 151.06 o 2 13 0 2004.37 1970.37 76.07 o 3 13 0 5372.19 5402.08 157.34 o 4 13 0 2428.22 2167.77 101.40 o 5 13 0 4742.63 4687.62 149.76 o 6 13 0 1302.08 1049.83 124.64 o 7 13 0 181.24 295.37 78.26 o 8 13 0 10.82 -51.90 77.79 o 9 13 0 3787.41 3785.50 204.68 o 10 13 0 144.32 131.11 83.10 o 11 13 0 3780.66 4151.67 280.23 o 12 13 0 1360.38 1535.75 319.86 o 13 13 0 123.42 202.03 113.39 o 14 13 0 121.60 144.63 130.54 o 15 13 0 30.02 105.34 163.93 o 0 14 0 5553.62 5412.57 169.52 o 1 14 0 198.30 245.39 40.00 o 2 14 0 4283.79 4147.96 132.25 o 3 14 0 1369.33 1449.45 136.47 o 4 14 0 20916.78 19693.75 436.76 o 5 14 0 1770.48 1577.90 124.75 o 6 14 0 1585.63 1461.36 126.05 o 7 14 0 2577.00 2473.30 159.17 o 8 14 0 13033.80 12343.34 356.32 o 9 14 0 9.34 176.38 80.05 o 10 14 0 6406.89 6606.18 341.07 o 11 14 0 113.24 113.83 261.07 o 12 14 0 247.23 404.86 128.97 o 13 14 0 282.07 339.98 139.33 o 14 14 0 86.23 189.46 122.39 o 1 15 0 2971.03 3034.63 92.19 o 2 15 0 137.40 133.94 68.28 o 3 15 0 20070.81 18859.55 418.87 o 4 15 0 1830.32 1857.98 126.75 o 5 15 0 22277.53 20964.59 474.30 o 6 15 0 1750.74 1681.30 207.39 o 7 15 0 3165.52 2911.29 173.14 o 8 15 0 1155.37 1180.69 128.37 o 9 15 0 12290.95 12320.67 406.28 o 10 15 0 587.67 716.67 123.74 o 11 15 0 92.13 -36.03 82.17 o 12 15 0 164.11 51.82 116.74 o 13 15 0 1257.86 1516.36 215.02 o 14 15 0 193.08 210.67 125.71 o 0 16 0 1712.57 1956.23 112.18 o 1 16 0 115.86 98.28 79.27 o 2 16 0 1200.74 1080.99 88.68 o 3 16 0 197.50 133.22 68.35 o 4 16 0 10772.92 10370.58 367.77 o 5 16 0 396.76 437.89 84.40 o 6 16 0 2555.46 2814.41 165.27 o 7 16 0 3244.50 3338.42 224.63 o 8 16 0 3165.85 3523.89 201.49 o 9 16 0 1144.67 1371.70 151.32 o 10 16 0 2608.33 2466.07 191.64 o 11 16 0 266.32 70.37 89.97 o 12 16 0 40.76 -89.03 104.78 o 13 16 0 466.14 892.75 174.78 o 1 17 0 85.60 82.93 65.63 o 2 17 0 1093.33 1103.30 89.31 o 3 17 0 4125.77 3513.73 145.98 o 4 17 0 1.43 -51.92 51.92 o 5 17 0 1476.37 1500.26 127.52 o 6 17 0 41.28 172.92 72.14 o 7 17 0 366.11 473.87 94.33 o 8 17 0 4925.51 5517.63 242.62 o 9 17 0 1268.43 1133.74 139.22 o 10 17 0 1190.69 1284.47 152.24 o 11 17 0 1.04 6.98 105.95 o 12 17 0 301.93 566.99 141.86 o 13 17 0 9.82 39.02 132.47 o 0 18 0 7405.45 7393.43 484.62 o 1 18 0 99.64 64.88 93.01 o 2 18 0 2516.24 2475.35 155.09 o 3 18 0 870.76 845.37 86.41 o 4 18 0 880.05 1020.84 105.77 o 5 18 0 57.20 89.05 67.74 o 6 18 0 1093.63 1200.34 126.57 o 7 18 0 1967.17 1916.94 167.30 o 8 18 0 392.45 598.95 111.21 o 9 18 0 2132.69 2164.20 180.14 o 10 18 0 489.21 648.73 123.94 o 11 18 0 212.78 491.81 113.18 o 12 18 0 850.86 1211.45 192.36 o 1 19 0 14703.66 13959.39 552.78 o 2 19 0 74.69 24.74 116.74 o 3 19 0 1238.22 1020.14 132.60 o 4 19 0 1258.70 1254.71 130.93 o 5 19 0 9416.29 9081.88 308.73 o 6 19 0 1638.53 1489.76 149.23 o 7 19 0 565.68 826.92 150.02 o 8 19 0 1854.79 2032.37 172.05 o 9 19 0 2271.44 2257.02 307.92 o 10 19 0 117.43 195.55 105.73 o 11 19 0 126.31 201.35 100.25 o 12 19 0 3.68 -26.66 120.64 o 0 20 0 20424.37 20198.22 919.00 o 1 20 0 743.26 779.31 195.39 o 2 20 0 1597.23 1840.97 341.94 o 3 20 0 2841.53 2729.70 245.99 o 4 20 0 10565.25 9631.21 880.64 o 5 20 0 683.89 938.03 150.67 o 6 20 0 481.47 375.19 126.60 o 7 20 0 1071.60 1315.03 179.71 o 8 20 0 3537.20 3645.33 219.56 o 9 20 0 820.77 1048.21 223.26 o 10 20 0 396.27 780.07 161.88 o 11 20 0 147.12 270.16 104.52 o 1 21 0 6406.08 6218.26 744.59 o 2 21 0 849.10 1037.25 176.85 o 3 21 0 369.51 265.40 130.53 o 4 21 0 2461.42 2358.34 247.39 o 5 21 0 2760.04 2903.23 265.62 o 6 21 0 1996.11 2342.52 324.00 o 7 21 0 1193.96 1324.96 216.09 o 8 21 0 314.98 67.40 151.79 o 9 21 0 1411.89 1669.76 445.70 o 10 21 0 29.63 90.65 107.83 o 0 22 0 802.47 680.01 229.61 o 1 22 0 14.83 124.32 147.37 o 2 22 0 1017.70 997.27 181.12 o 3 22 0 1044.56 1089.92 210.85 o 4 22 0 228.05 202.96 124.58 o 5 22 0 3380.44 3162.07 442.12 o 6 22 0 70.19 -64.27 101.02 o 7 22 0 624.27 501.73 247.83 o 8 22 0 50.42 176.16 118.11 o 9 22 0 39.03 91.83 119.37 o 1 23 0 3.41 58.20 160.07 o 2 23 0 707.22 562.38 166.14 o 3 23 0 534.71 750.90 174.95 o 4 23 0 1699.46 1159.73 202.58 o 5 23 0 514.81 527.45 362.36 o 6 23 0 1116.14 954.34 187.77 o 7 23 0 103.71 -65.68 194.84 o 8 23 0 104.00 329.52 204.22 o 0 24 0 2584.95 2944.68 425.01 o 1 24 0 27.80 -35.42 123.54 o 2 24 0 405.44 372.82 158.67 o 3 24 0 469.70 551.26 172.33 o 4 24 0 3588.30 3266.95 317.17 o 5 24 0 1531.57 1562.29 512.77 o 6 24 0 269.77 330.92 141.75 o 7 24 0 1441.94 1164.37 195.76 o 1 25 0 1658.95 1604.45 237.09 o 2 25 0 0.25 -56.44 134.22 o 3 25 0 3640.27 3838.28 337.95 o 4 25 0 456.49 586.55 279.56 o 5 25 0 3530.11 3917.34 415.90 o 0 26 0 1618.11 1924.11 341.66 o 1 26 0 46.11 281.36 145.38 o 2 26 0 8.63 280.04 138.57 o 3 26 0 85.08 -42.85 139.37 o -17 0 1 221.05 256.66 211.40 o -15 0 1 2527.94 2124.47 323.45 o -13 0 1 25848.88 25706.18 1052.03 o -11 0 1 348.58 259.42 128.05 o -9 0 1 32271.12 31484.04 1095.08 o -7 0 1 27741.27 27391.30 930.04 o -5 0 1 27920.02 29933.60 954.33 o -3 0 1 5.64 -19.87 40.29 o -1 0 1 222137.06 196986.55 3823.82 o 1 0 1 87766.30 96090.88 2562.17 o 3 0 1 1766.54 2263.01 142.40 o 5 0 1 158620.25 173480.97 4989.67 o 7 0 1 3128.07 3300.14 235.13 o 9 0 1 1387.53 1243.55 194.84 o 11 0 1 240.71 146.82 130.81 o 13 0 1 7362.23 7509.66 351.87 o 15 0 1 0.85 108.73 90.52 o 17 0 1 2341.23 2261.02 231.10 o -17 1 1 131.33 230.03 136.75 o -16 1 1 1.55 -29.98 161.17 o -15 1 1 148.05 290.09 124.46 o -14 1 1 6255.42 6276.88 863.53 o -13 1 1 205.57 439.14 113.45 o -12 1 1 12202.11 11259.78 414.68 o -11 1 1 411.82 359.08 104.78 o -10 1 1 6492.82 5409.71 349.39 o -9 1 1 123.82 176.14 88.31 o -8 1 1 51851.71 52546.24 1178.09 o -7 1 1 4991.42 5208.15 201.95 o -6 1 1 11054.00 10961.70 350.77 o -5 1 1 16.00 43.45 36.02 o -4 1 1 34763.43 35883.67 1100.05 o -3 1 1 2957.81 3255.60 114.32 o -2 1 1 25906.87 29398.90 379.61 o -1 1 1 325.62 340.64 12.76 o 0 1 1 197396.22 187494.31 3067.53 o 1 1 1 827.48 812.55 24.85 o 2 1 1 27175.90 30417.32 517.28 o 3 1 1 2974.30 2947.61 112.06 o 4 1 1 152454.89 155874.45 3161.54 o 5 1 1 6713.19 6850.61 219.12 o 6 1 1 41948.44 43153.50 965.91 o 7 1 1 37.21 46.01 50.23 o 8 1 1 2001.93 2041.33 149.79 o 9 1 1 2856.96 2606.69 267.15 o 10 1 1 202.29 207.06 94.60 o 11 1 1 14.62 -33.89 78.19 o 12 1 1 10560.85 10086.42 394.64 o 13 1 1 405.59 391.35 104.73 o 14 1 1 1592.09 1625.31 141.73 o 15 1 1 33.06 204.50 65.33 o 16 1 1 1564.06 1599.70 134.67 o 17 1 1 530.90 1200.50 208.09 o -17 2 1 243.09 289.73 101.07 o -16 2 1 115.53 239.55 129.75 o -15 2 1 906.56 910.31 170.10 o -14 2 1 3216.95 2926.09 275.15 o -13 2 1 5028.20 4618.38 287.57 o -12 2 1 1644.50 1446.39 169.17 o -11 2 1 163.65 130.41 86.99 o -10 2 1 432.61 579.82 106.90 o -9 2 1 4614.47 4114.86 232.65 o -8 2 1 874.35 854.64 148.48 o -7 2 1 26554.45 27221.47 656.43 o -6 2 1 3043.36 3111.28 143.86 o -5 2 1 2155.14 2175.63 110.64 o -4 2 1 143.95 137.37 34.12 o -3 2 1 127.74 151.55 26.74 o -2 2 1 3434.44 3716.42 77.46 o -1 2 1 24086.77 27163.87 389.55 o 0 2 1 958.51 1065.41 38.55 o 1 2 1 7948.87 8645.88 122.81 o 2 2 1 1457.42 1408.09 51.41 o 3 2 1 10831.33 11762.63 495.10 o 4 2 1 7187.94 7269.78 238.17 o 5 2 1 60864.57 63397.31 1349.34 o 6 2 1 7669.78 7334.33 301.64 o 7 2 1 1481.86 1669.54 126.22 o 8 2 1 3241.23 2935.72 171.41 o 9 2 1 812.09 936.74 126.88 o 10 2 1 1706.00 1536.11 157.63 o 11 2 1 2410.97 2324.29 194.80 o 12 2 1 874.54 705.70 104.21 o 13 2 1 2809.38 2403.12 169.57 o 14 2 1 667.78 660.81 87.10 o 15 2 1 184.20 164.33 72.34 o 16 2 1 495.28 758.49 125.49 o -17 3 1 581.95 818.20 129.86 o -16 3 1 1502.75 1598.50 352.15 o -15 3 1 221.97 259.43 120.60 o -14 3 1 455.01 257.68 178.01 o -13 3 1 3746.41 3779.25 368.98 o -12 3 1 47.37 48.72 88.45 o -11 3 1 681.02 537.45 113.89 o -10 3 1 791.06 698.42 113.95 o -9 3 1 10.85 42.18 64.00 o -8 3 1 407.30 501.10 83.22 o -7 3 1 725.58 749.71 90.06 o -6 3 1 16182.06 15721.26 571.00 o -5 3 1 461.74 441.69 51.46 o -4 3 1 63417.62 66691.58 854.30 o -3 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