# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' tik40m in P2(1)/n (-90 degrees Celcius)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 264.96 _exptl_crystal_F_000 1152.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 11.6505 _cell_length_b 10.4942 _cell_length_c 19.4752 _cell_angle_alpha 90.000 _cell_angle_beta 104.799 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 523.53 396.67 49.22 o 4 0 0 197.91 220.04 44.54 o 6 0 0 8.38 12.01 17.54 o 8 0 0 3367.85 4012.37 298.84 o 10 0 0 849.97 1005.01 154.74 o 12 0 0 26.68 20.80 57.62 o 1 1 0 475.14 507.80 56.27 o 2 1 0 3974.03 4401.96 227.86 o 3 1 0 50.61 61.14 13.31 o 4 1 0 17.34 29.77 10.05 o 5 1 0 778.68 803.23 56.65 o 6 1 0 40.57 23.88 14.86 o 7 1 0 477.42 467.05 37.81 o 8 1 0 2.03 13.39 25.05 o 9 1 0 4951.33 5723.07 340.74 o 10 1 0 532.40 467.27 94.43 o 11 1 0 3.84 -19.04 28.70 o 12 1 0 23.58 15.32 38.25 o 13 1 0 244.01 293.57 69.97 o 0 2 0 13299.91 12677.92 1198.03 o 1 2 0 3647.75 2992.35 330.36 o 2 2 0 2578.98 2618.30 139.63 o 3 2 0 1706.47 1812.99 101.38 o 4 2 0 3.47 0.41 9.89 o 5 2 0 7.91 19.37 10.32 o 6 2 0 62.88 50.75 14.64 o 7 2 0 1835.55 2281.36 178.35 o 8 2 0 58.94 83.08 30.23 o 9 2 0 15.31 19.49 24.40 o 10 2 0 515.89 368.51 178.77 o 11 2 0 248.47 251.04 60.17 o 12 2 0 0.33 28.52 40.09 o 13 2 0 2.14 7.17 40.66 o 1 3 0 32906.10 31764.87 1601.56 o 2 3 0 1840.96 1742.76 97.43 o 3 3 0 378.89 341.57 28.13 o 4 3 0 1633.22 1432.42 85.05 o 5 3 0 1316.50 1311.88 102.39 o 6 3 0 0.30 10.29 17.24 o 7 3 0 969.52 1147.88 79.66 o 8 3 0 1.40 -6.28 29.81 o 9 3 0 447.50 399.93 60.74 o 10 3 0 2487.60 2651.76 178.10 o 11 3 0 574.52 647.55 73.68 o 12 3 0 124.58 187.76 65.21 o 13 3 0 5.60 41.87 50.25 o 0 4 0 327.95 393.44 54.19 o 1 4 0 15130.66 16584.91 919.32 o 2 4 0 602.61 596.42 41.60 o 3 4 0 34.93 36.13 13.05 o 4 4 0 883.51 773.46 53.72 o 5 4 0 1962.71 2016.24 126.38 o 6 4 0 152.86 147.79 32.84 o 7 4 0 183.32 215.39 33.02 o 8 4 0 65.12 75.52 27.41 o 9 4 0 18.70 23.57 27.78 o 10 4 0 76.63 95.50 35.93 o 11 4 0 293.34 329.34 54.26 o 12 4 0 39.60 45.11 41.17 o 1 5 0 12.92 37.03 27.57 o 2 5 0 102.60 82.32 15.62 o 3 5 0 316.48 281.38 29.13 o 4 5 0 331.15 378.39 35.55 o 5 5 0 831.81 919.48 65.47 o 6 5 0 487.57 507.33 47.00 o 7 5 0 96.75 124.56 28.32 o 8 5 0 1531.86 1489.49 104.93 o 9 5 0 63.72 62.06 27.16 o 10 5 0 483.64 554.97 80.98 o 11 5 0 295.77 247.86 50.37 o 12 5 0 58.63 106.05 47.70 o 0 6 0 2898.85 3698.17 372.27 o 1 6 0 212.69 218.45 24.71 o 2 6 0 1163.39 1216.73 153.51 o 3 6 0 328.30 326.42 32.78 o 4 6 0 34.94 31.74 17.76 o 5 6 0 2533.52 2499.86 145.75 o 6 6 0 264.65 243.42 35.56 o 7 6 0 398.50 356.59 42.37 o 8 6 0 307.21 288.07 41.93 o 9 6 0 67.06 73.88 30.48 o 10 6 0 160.89 148.05 43.21 o 11 6 0 136.92 129.70 47.32 o 1 7 0 679.83 669.70 50.25 o 2 7 0 406.28 428.82 38.81 o 3 7 0 499.26 517.39 45.76 o 4 7 0 488.58 484.44 45.10 o 5 7 0 3.09 3.72 17.32 o 6 7 0 17.67 26.10 22.12 o 7 7 0 740.78 710.76 63.94 o 8 7 0 46.87 40.47 26.44 o 9 7 0 556.83 580.81 61.64 o 10 7 0 3.34 19.12 41.19 o 11 7 0 30.65 27.10 38.77 o 0 8 0 967.01 1047.89 127.84 o 1 8 0 0.03 11.25 15.06 o 2 8 0 35.86 42.33 19.40 o 3 8 0 21.64 10.35 18.17 o 4 8 0 10.51 10.64 19.73 o 5 8 0 258.19 306.69 39.03 o 6 8 0 56.35 56.80 26.90 o 7 8 0 28.65 17.41 24.56 o 8 8 0 898.87 908.62 92.41 o 9 8 0 4.91 9.70 32.56 o 10 8 0 3.42 4.75 26.53 o 1 9 0 88.36 87.90 23.64 o 2 9 0 2033.31 2007.71 121.93 o 3 9 0 20.20 29.25 22.84 o 4 9 0 30.42 24.77 23.00 o 5 9 0 379.50 398.53 56.41 o 6 9 0 291.40 311.37 43.36 o 7 9 0 890.57 906.63 76.17 o 8 9 0 104.06 92.16 36.08 o 9 9 0 156.41 163.04 39.73 o 0 10 0 162.91 133.98 51.60 o 1 10 0 244.53 209.82 39.66 o 2 10 0 245.95 195.39 40.09 o 3 10 0 0.49 38.63 44.34 o 4 10 0 103.32 70.03 33.17 o 5 10 0 18.55 38.76 35.78 o 6 10 0 120.46 109.29 40.41 o 7 10 0 67.27 24.21 46.55 o 8 10 0 2.42 15.97 39.00 o 1 11 0 65.48 65.80 32.25 o 2 11 0 5.94 -7.73 22.50 o 3 11 0 114.13 140.82 39.72 o 4 11 0 188.01 116.67 48.48 o 5 11 0 6.96 -1.29 37.10 o 6 11 0 24.15 25.55 47.50 o 2 12 0 29.11 35.52 41.46 o 3 12 0 145.31 143.46 64.54 o -13 0 1 356.35 373.18 101.42 o -11 0 1 741.59 747.53 134.59 o -9 0 1 7590.19 9268.22 922.07 o -7 0 1 1030.96 1254.70 155.95 o -5 0 1 442.27 385.44 60.84 o -3 0 1 181.01 106.94 27.95 o 3 0 1 74.36 6.46 11.85 o 5 0 1 61.14 64.08 19.58 o 7 0 1 84.00 67.14 26.88 o 9 0 1 4286.23 4416.62 462.79 o 11 0 1 4249.48 4004.40 434.55 o 13 0 1 1.24 15.15 61.97 o -13 1 1 41.80 19.74 42.00 o -12 1 1 123.76 117.22 52.89 o -11 1 1 337.59 395.02 67.15 o -10 1 1 1631.54 1741.60 154.51 o -9 1 1 866.35 877.25 72.62 o -8 1 1 340.35 369.73 56.42 o -7 1 1 995.51 1204.94 85.41 o -6 1 1 34.28 31.30 15.74 o -5 1 1 4199.75 3948.85 212.22 o -4 1 1 920.55 913.21 58.49 o -3 1 1 97.80 53.29 12.80 o -2 1 1 2187.19 1747.38 94.68 o -1 1 1 1389.12 1540.97 171.25 o 1 1 1 70.53 111.01 14.28 o 2 1 1 11.23 10.92 7.94 o 3 1 1 15.09 8.33 9.62 o 4 1 1 9448.08 8520.90 415.07 o 5 1 1 1086.47 1172.03 76.83 o 6 1 1 523.15 489.10 108.83 o 7 1 1 4063.65 3343.60 556.46 o 8 1 1 124.91 131.70 30.07 o 9 1 1 585.92 551.04 55.57 o 10 1 1 4085.59 4516.08 341.12 o 11 1 1 1.25 15.98 35.42 o 12 1 1 40.86 47.04 43.60 o 13 1 1 0.60 28.58 41.64 o -13 2 1 49.21 43.59 48.24 o -12 2 1 387.08 371.92 67.00 o -11 2 1 2074.21 2077.06 183.15 o -10 2 1 2399.59 953.47 1340.68 o -9 2 1 591.51 735.75 84.93 o -8 2 1 905.71 1066.88 100.94 o -7 2 1 355.44 412.76 41.42 o -6 2 1 68.49 68.40 14.98 o -5 2 1 151.74 184.00 21.22 o -4 2 1 1861.28 1631.12 93.96 o -3 2 1 178.64 119.61 16.46 o -2 2 1 6261.17 6258.02 321.95 o -1 2 1 5344.83 687.02 1980.67 o 0 2 1 182.59 199.79 21.03 o 1 2 1 5257.12 5568.99 285.58 o 2 2 1 374.31 414.35 29.52 o 3 2 1 1916.92 1832.32 102.24 o 4 2 1 2275.13 2360.71 115.35 o 5 2 1 1075.52 1082.81 60.32 o 6 2 1 693.90 687.02 46.73 o 7 2 1 368.73 387.48 42.23 o 8 2 1 331.77 351.95 42.98 o 9 2 1 29.31 32.90 27.03 o 10 2 1 386.73 364.59 80.41 o 11 2 1 402.70 393.42 68.01 o 12 2 1 11.71 20.05 41.94 o 13 2 1 284.98 247.33 65.31 o -13 3 1 306.59 260.99 98.33 o -12 3 1 583.08 526.60 81.67 o -11 3 1 913.68 951.23 87.60 o -10 3 1 1174.42 1345.61 107.08 o -9 3 1 87.21 119.99 42.69 o -8 3 1 363.52 387.34 57.03 o -7 3 1 5143.55 6037.75 324.11 o -6 3 1 34.13 46.06 18.40 o -5 3 1 105.78 126.49 21.43 o -4 3 1 59.06 45.87 15.48 o -3 3 1 11370.19 12915.95 659.46 o -2 3 1 6677.02 6115.09 316.09 o -1 3 1 31448.12 34126.57 2038.22 o 0 3 1 23442.28 21140.26 1410.10 o 1 3 1 9348.29 9041.46 460.45 o 2 3 1 6.95 10.75 7.62 o 3 3 1 999.97 921.58 58.17 o 4 3 1 269.17 274.35 28.48 o 5 3 1 3082.91 3066.67 158.98 o 6 3 1 109.20 109.21 22.67 o 7 3 1 10.17 10.19 19.94 o 8 3 1 290.89 334.12 43.74 o 9 3 1 2540.78 2861.17 186.51 o 10 3 1 3111.86 3564.38 231.47 o 11 3 1 103.07 67.45 36.19 o 12 3 1 4.20 -13.44 32.36 o -12 4 1 70.75 94.54 42.89 o -11 4 1 61.67 121.86 43.44 o -10 4 1 147.81 156.23 47.02 o -9 4 1 1648.19 1716.74 114.17 o -8 4 1 2.06 -7.82 18.83 o -7 4 1 73.93 83.90 24.69 o -6 4 1 102.55 113.45 28.14 o -5 4 1 1534.67 1672.31 102.11 o -4 4 1 817.84 749.15 51.73 o -3 4 1 1826.58 1812.83 104.27 o -2 4 1 51.38 65.49 14.26 o -1 4 1 5760.67 5561.93 592.98 o 0 4 1 1214.06 366.17 662.61 o 1 4 1 617.89 578.51 38.93 o 2 4 1 367.46 337.19 28.48 o 3 4 1 2817.64 2544.18 140.43 o 4 4 1 134.30 153.82 23.13 o 5 4 1 31.57 23.90 16.49 o 6 4 1 165.57 152.34 26.22 o 7 4 1 1261.20 1394.54 93.21 o 8 4 1 21.93 20.81 24.63 o 9 4 1 69.54 58.01 29.09 o 10 4 1 5.29 2.15 35.78 o 11 4 1 285.21 264.29 51.03 o 12 4 1 191.56 188.91 49.45 o -12 5 1 21.09 60.03 40.85 o -11 5 1 0.28 -1.87 26.94 o -10 5 1 233.54 216.00 43.09 o -9 5 1 1272.73 1375.28 99.58 o -8 5 1 907.53 898.82 93.25 o -7 5 1 604.67 687.87 58.22 o -6 5 1 803.33 938.11 67.97 o -5 5 1 6.98 6.12 13.82 o -4 5 1 90.38 111.02 21.33 o -3 5 1 204.89 192.20 23.74 o -2 5 1 228.33 253.90 25.53 o -1 5 1 10932.41 11460.60 679.91 o 0 5 1 485.93 205.78 250.60 o 1 5 1 276.34 171.62 84.77 o 2 5 1 101.12 100.24 17.15 o 3 5 1 952.31 902.36 60.45 o 4 5 1 458.37 520.87 42.22 o 5 5 1 1898.15 1982.86 118.60 o 6 5 1 831.69 789.04 60.04 o 7 5 1 48.52 53.19 24.21 o 8 5 1 17.79 18.73 21.20 o 9 5 1 24.98 16.74 25.06 o 10 5 1 121.05 137.12 38.34 o 11 5 1 34.09 57.34 35.82 o 12 5 1 46.67 22.45 38.72 o -11 6 1 436.19 439.81 62.92 o -10 6 1 1069.32 985.32 82.56 o -9 6 1 2.77 3.75 22.91 o -8 6 1 162.75 216.47 38.67 o -7 6 1 17.24 9.27 23.09 o -6 6 1 1120.21 1086.56 78.07 o -5 6 1 1100.74 961.18 68.53 o -4 6 1 1452.68 1485.55 142.68 o -3 6 1 20.94 22.39 14.95 o -2 6 1 3391.07 3862.55 246.36 o -1 6 1 24.33 23.54 13.35 o 0 6 1 77.52 44.25 45.38 o 1 6 1 2509.60 934.58 1071.26 o 2 6 1 170.10 102.96 67.60 o 3 6 1 3.17 10.14 14.12 o 4 6 1 2039.91 2037.41 120.72 o 5 6 1 2.48 8.96 17.50 o 6 6 1 519.21 504.30 60.00 o 7 6 1 0.25 6.94 26.59 o 8 6 1 1.16 14.15 20.22 o 9 6 1 125.22 103.48 28.26 o 10 6 1 303.96 289.31 51.51 o 11 6 1 77.03 68.33 38.54 o -11 7 1 68.09 73.49 33.29 o -10 7 1 6.47 -7.46 26.93 o -9 7 1 1.32 -6.18 24.48 o -8 7 1 50.45 40.16 27.23 o -7 7 1 51.31 38.87 23.77 o -6 7 1 216.45 223.78 35.41 o -5 7 1 94.03 80.72 24.14 o -4 7 1 781.35 681.98 54.21 o -3 7 1 274.72 266.43 33.60 o -2 7 1 5501.72 5466.69 292.29 o -1 7 1 98.44 82.32 19.61 o 0 7 1 92.86 89.93 23.29 o 1 7 1 500.09 333.18 193.04 o 2 7 1 11.17 24.48 15.52 o 3 7 1 16.56 25.56 17.31 o 4 7 1 27.94 28.14 20.31 o 5 7 1 877.79 806.12 74.46 o 6 7 1 490.84 464.03 47.79 o 7 7 1 114.79 112.67 30.93 o 8 7 1 275.79 272.13 38.63 o 9 7 1 367.36 412.77 47.94 o 10 7 1 19.94 45.16 41.73 o -10 8 1 12.33 23.51 32.83 o -9 8 1 130.92 150.17 37.80 o -8 8 1 876.72 1072.62 104.13 o -7 8 1 1744.24 1654.71 112.58 o -6 8 1 127.16 91.02 28.81 o -5 8 1 11.64 -3.19 20.88 o -4 8 1 72.31 75.55 24.45 o -3 8 1 0.43 17.76 19.04 o -2 8 1 116.62 102.40 23.08 o -1 8 1 372.04 373.35 37.33 o 0 8 1 36.57 47.73 18.64 o 1 8 1 47.85 40.79 17.50 o 2 8 1 1.02 -1.87 14.48 o 3 8 1 158.43 157.37 28.40 o 4 8 1 10.53 28.59 20.07 o 5 8 1 124.49 123.25 29.11 o 6 8 1 14.77 21.05 25.29 o 7 8 1 233.98 236.39 40.74 o 8 8 1 166.79 173.87 35.98 o 9 8 1 223.86 252.93 42.05 o 10 8 1 2.02 15.46 27.89 o -9 9 1 118.83 109.81 38.55 o -8 9 1 25.06 26.35 29.50 o -7 9 1 24.79 35.46 27.68 o -6 9 1 234.96 269.01 41.58 o -5 9 1 33.92 17.57 22.19 o -4 9 1 102.73 84.17 26.23 o -3 9 1 734.32 725.45 61.81 o -2 9 1 731.35 708.87 58.12 o -1 9 1 223.09 206.52 29.95 o 0 9 1 108.79 101.24 23.11 o 1 9 1 719.42 656.21 163.42 o 2 9 1 1144.69 701.93 419.57 o 3 9 1 33.30 40.70 24.56 o 4 9 1 143.50 143.46 30.42 o 5 9 1 130.04 141.98 33.43 o 6 9 1 29.63 20.56 31.97 o 7 9 1 207.02 203.05 44.20 o 8 9 1 382.24 396.97 74.28 o 9 9 1 271.32 256.13 65.90 o -8 10 1 14.09 42.06 40.26 o -7 10 1 333.95 318.72 49.72 o -6 10 1 34.26 10.99 25.83 o -5 10 1 0.01 -5.05 21.96 o -4 10 1 21.04 1.07 22.42 o -3 10 1 483.38 496.68 50.71 o -2 10 1 0.46 16.39 21.23 o -1 10 1 9.17 10.06 17.95 o 0 10 1 95.35 88.66 25.25 o 1 10 1 54.35 30.39 26.29 o 2 10 1 48.40 22.18 24.20 o 3 10 1 1.77 20.04 27.50 o 4 10 1 0.05 2.97 32.74 o 5 10 1 447.88 395.08 84.70 o 6 10 1 26.92 25.79 36.40 o 7 10 1 587.35 554.66 84.87 o -6 11 1 357.67 332.98 62.34 o -5 11 1 30.40 5.40 30.13 o -4 11 1 12.06 17.28 27.98 o -3 11 1 35.42 46.80 32.95 o -2 11 1 0.37 27.73 27.34 o -1 11 1 212.50 172.46 37.72 o 0 11 1 347.64 275.47 66.30 o 1 11 1 0.63 2.59 37.29 o 2 11 1 2.97 36.14 41.80 o 3 11 1 15.06 -3.31 31.30 o 4 11 1 27.63 22.73 31.70 o 5 11 1 429.10 441.56 87.64 o 6 11 1 123.28 103.68 50.59 o -3 12 1 325.02 248.62 80.97 o -1 12 1 1.42 20.04 41.12 o 0 12 1 218.87 196.10 61.00 o 1 12 1 73.02 65.77 46.02 o 2 12 1 50.96 62.56 48.18 o 3 12 1 14.91 17.55 38.73 o -12 0 2 433.06 361.43 96.79 o -10 0 2 3426.79 3926.92 429.09 o -8 0 2 1002.53 1107.90 144.88 o -6 0 2 3416.82 3092.92 318.83 o -4 0 2 6193.90 5857.73 747.98 o -2 0 2 160.26 152.82 17.08 o 2 0 2 70206.45 17473.11 44399.04 o 4 0 2 2273.31 2022.02 150.64 o 6 0 2 438.99 409.58 48.97 o 8 0 2 27.74 33.45 26.71 o 10 0 2 1183.21 1232.95 167.73 o 12 0 2 35.40 40.70 59.10 o -13 1 2 446.24 444.25 81.97 o -12 1 2 23.23 10.31 56.85 o -11 1 2 300.50 347.93 64.46 o -10 1 2 3501.28 3543.97 272.01 o -9 1 2 28.04 23.51 30.51 o -8 1 2 451.43 460.76 60.53 o -7 1 2 620.17 694.89 71.59 o -6 1 2 38.89 39.40 18.04 o -5 1 2 198.60 315.83 30.33 o -4 1 2 1536.51 1546.51 89.20 o -3 1 2 4306.46 4003.97 210.23 o -2 1 2 54.12 3.46 6.80 o -1 1 2 203.61 201.14 15.84 o 0 1 2 582.36 678.42 43.32 o 1 1 2 4874.95 4230.17 240.96 o 2 1 2 5003.29 4627.51 245.33 o 3 1 2 25.98 45.90 11.14 o 4 1 2 2890.90 3048.48 155.63 o 5 1 2 1662.17 1851.34 140.06 o 6 1 2 1054.12 1213.07 122.33 o 7 1 2 0.47 -0.78 14.10 o 8 1 2 281.00 284.38 57.36 o 9 1 2 718.12 737.82 67.75 o 10 1 2 101.41 64.29 40.15 o 11 1 2 534.96 569.05 80.75 o 12 1 2 113.37 104.91 47.51 o -13 2 2 90.82 52.83 45.75 o -12 2 2 0.97 1.30 34.74 o -11 2 2 4.36 -10.38 31.53 o -10 2 2 1118.34 1186.68 116.56 o -9 2 2 2157.41 2340.74 190.36 o -8 2 2 65.66 71.20 33.14 o -7 2 2 474.59 494.64 44.66 o -6 2 2 369.32 408.62 30.28 o -5 2 2 250.34 275.02 34.10 o -4 2 2 673.96 552.59 47.45 o -3 2 2 4572.92 4268.80 223.86 o -2 2 2 4360.75 908.73 1563.64 o -1 2 2 1847.72 1741.19 75.48 o 0 2 2 11184.86 1222.06 5842.11 o 1 2 2 6717.57 6144.64 254.18 o 2 2 2 4.65 3.59 6.17 o 3 2 2 1487.28 1379.65 63.69 o 4 2 2 5679.79 5810.73 287.19 o 5 2 2 1033.22 1071.35 63.47 o 6 2 2 918.63 993.07 61.79 o 7 2 2 65.13 62.62 24.74 o 8 2 2 1638.61 1750.36 121.47 o 9 2 2 378.14 481.18 55.28 o 10 2 2 250.71 244.82 44.34 o 11 2 2 498.07 576.31 81.99 o 12 2 2 26.12 37.77 42.68 o -13 3 2 2.86 4.03 40.80 o -12 3 2 368.96 364.83 73.19 o -11 3 2 299.93 278.79 48.82 o -10 3 2 0.10 5.37 39.45 o -9 3 2 2.42 -15.58 33.60 o -8 3 2 3386.20 3940.86 221.05 o -7 3 2 67.68 84.87 27.06 o -6 3 2 7.86 8.49 20.59 o -5 3 2 146.08 169.18 23.55 o -4 3 2 989.94 1033.16 65.05 o -3 3 2 18.03 28.74 11.84 o -2 3 2 7190.93 1249.24 2445.28 o -1 3 2 40078.51 41872.14 2299.18 o 0 3 2 599.41 443.83 32.56 o 1 3 2 3903.61 3711.11 172.05 o 2 3 2 1212.13 1085.87 56.41 o 3 3 2 591.81 537.52 33.49 o 4 3 2 6938.26 6806.12 285.84 o 5 3 2 1334.49 1236.08 67.65 o 6 3 2 1.01 3.02 15.01 o 7 3 2 118.53 117.70 28.66 o 8 3 2 344.68 371.98 47.98 o 9 3 2 2985.81 3176.43 206.34 o 10 3 2 9.43 -1.61 25.54 o 11 3 2 13.12 43.27 35.32 o 12 3 2 104.45 88.42 51.76 o -12 4 2 1.80 5.50 36.06 o -11 4 2 265.00 215.25 55.72 o -10 4 2 68.99 60.80 39.73 o -9 4 2 693.33 744.69 65.50 o -8 4 2 66.11 73.13 27.20 o -7 4 2 233.76 280.13 36.52 o -6 4 2 380.21 527.86 47.22 o -5 4 2 5345.89 5427.59 289.32 o -4 4 2 2071.91 1970.29 149.52 o -3 4 2 163.27 185.80 23.93 o -2 4 2 596.92 405.05 182.28 o -1 4 2 728.85 886.77 59.37 o 0 4 2 223.87 290.58 33.26 o 1 4 2 2536.10 2357.84 168.61 o 2 4 2 926.27 1073.69 86.81 o 3 4 2 1313.00 1382.11 72.32 o 4 4 2 16.35 13.93 10.39 o 5 4 2 1060.60 1267.04 72.98 o 6 4 2 1045.95 1016.80 63.04 o 7 4 2 154.73 110.50 28.71 o 8 4 2 225.20 224.84 39.74 o 9 4 2 264.89 223.86 43.64 o 10 4 2 114.43 174.43 41.64 o 11 4 2 106.24 100.68 39.43 o 12 4 2 111.78 163.07 51.42 o -12 5 2 290.04 276.15 55.32 o -11 5 2 132.77 119.76 44.68 o -10 5 2 403.98 472.40 55.27 o -9 5 2 782.62 847.04 71.96 o -8 5 2 1707.38 2002.06 151.77 o -7 5 2 172.46 204.96 33.32 o -6 5 2 4.83 -18.32 17.75 o -5 5 2 18.85 20.42 15.43 o -4 5 2 822.98 779.82 55.35 o -3 5 2 51.08 32.73 12.56 o -2 5 2 908.74 485.39 201.54 o -1 5 2 240.37 282.44 59.58 o 0 5 2 5234.90 4844.81 544.09 o 1 5 2 3222.98 3379.10 237.31 o 2 5 2 5.02 3.55 12.09 o 3 5 2 1797.92 1800.25 106.18 o 4 5 2 0.02 12.40 15.19 o 5 5 2 1641.56 1653.28 102.37 o 6 5 2 40.81 61.21 21.57 o 7 5 2 81.27 94.23 23.39 o 8 5 2 119.31 95.50 33.15 o 9 5 2 26.79 20.35 28.14 o 10 5 2 80.05 92.71 39.25 o 11 5 2 141.39 207.20 51.81 o -11 6 2 28.42 18.35 31.18 o -10 6 2 13.67 17.21 27.02 o -9 6 2 689.82 721.75 66.15 o -8 6 2 641.15 688.88 62.17 o -7 6 2 65.32 88.50 27.80 o -6 6 2 408.63 460.53 46.41 o -5 6 2 194.85 225.23 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