# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 2 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 228.96 _exptl_crystal_F_000 972.00 _reflns_d_resolution_high 0.7993 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.0579 _cell_length_b 12.9224 _cell_length_c 17.8260 _cell_angle_alpha 84.966 _cell_angle_beta 80.597 _cell_angle_gamma 84.398 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2051.46 1974.43 55.35 o 3 0 0 583.58 573.99 28.92 o 4 0 0 273.01 245.71 22.10 o 5 0 0 3663.80 3843.85 113.73 o 6 0 0 4731.73 4858.77 142.74 o 7 0 0 3098.54 3132.63 108.95 o 8 0 0 769.56 788.78 54.43 o 9 0 0 5.40 -5.60 34.71 o 10 0 0 289.07 287.28 45.81 o 11 0 0 788.84 726.27 68.64 o -11 1 0 138.51 193.91 55.55 o -10 1 0 430.10 401.89 52.04 o -9 1 0 1777.68 1872.58 91.09 o -8 1 0 1523.39 1422.60 72.49 o -7 1 0 938.60 971.25 56.08 o -6 1 0 1.74 -21.76 21.76 o -5 1 0 4482.22 4862.96 136.75 o -4 1 0 7807.27 8065.01 202.96 o -3 1 0 9353.21 9598.65 231.49 o -2 1 0 2429.95 2636.00 70.49 o -1 1 0 17313.49 17218.69 394.05 o 1 1 0 12086.74 12173.36 280.13 o 2 1 0 423.61 356.07 14.63 o 3 1 0 7599.73 7324.73 132.97 o 4 1 0 5577.90 5661.72 162.70 o 5 1 0 2391.49 2464.10 82.42 o 6 1 0 59.29 58.27 24.88 o 7 1 0 2290.42 2484.88 93.67 o 8 1 0 981.23 971.98 60.17 o 9 1 0 1478.94 1568.36 81.11 o 10 1 0 801.51 818.43 65.77 o 11 1 0 108.53 156.62 55.01 o -10 2 0 718.43 734.64 65.87 o -9 2 0 35.09 2.63 37.34 o -8 2 0 63.04 89.63 31.45 o -7 2 0 889.26 923.29 53.89 o -6 2 0 2669.66 2958.78 99.32 o -5 2 0 4822.09 4765.00 135.34 o -4 2 0 7032.38 7041.08 180.96 o -3 2 0 8013.64 8619.37 210.95 o -2 2 0 49407.74 47843.12 1080.11 o -1 2 0 13998.60 13186.33 304.03 o 0 2 0 15536.20 14989.64 344.83 o 1 2 0 10079.18 9889.10 229.59 o 2 2 0 17859.84 17217.46 289.93 o 3 2 0 260.42 261.53 15.46 o 4 2 0 9.77 11.97 30.50 o 5 2 0 2361.53 2479.57 82.28 o 6 2 0 2912.19 2601.19 92.16 o 7 2 0 1456.20 1547.32 49.78 o 8 2 0 466.73 379.88 41.87 o 9 2 0 103.69 55.16 40.26 o 10 2 0 812.05 861.90 66.75 o 11 2 0 509.30 432.75 65.82 o -10 3 0 175.13 181.64 44.40 o -9 3 0 818.52 960.15 67.14 o -8 3 0 964.68 968.33 59.59 o -7 3 0 871.51 838.53 51.56 o -6 3 0 225.31 235.19 29.02 o -5 3 0 122.35 90.07 21.86 o -4 3 0 1174.08 1284.68 50.83 o -3 3 0 23853.74 23580.58 545.94 o -2 3 0 1129.99 1092.03 39.09 o -1 3 0 2448.08 2414.05 66.99 o 0 3 0 92.69 111.38 11.54 o 1 3 0 14569.89 14496.17 244.69 o 2 3 0 167.44 154.57 11.92 o 3 3 0 8483.44 8347.34 154.74 o 4 3 0 12167.06 12210.97 218.02 o 5 3 0 1427.68 1369.12 44.21 o 6 3 0 2.44 -29.38 29.38 o 7 3 0 633.52 671.11 47.56 o 8 3 0 1883.11 1793.28 82.81 o 9 3 0 2056.80 1991.18 94.35 o 10 3 0 558.77 554.90 60.71 o 11 3 0 260.94 181.88 50.19 o -10 4 0 395.96 405.39 58.32 o -9 4 0 400.21 439.33 52.63 o -8 4 0 52.38 56.18 37.05 o -7 4 0 1088.86 1077.04 61.78 o -6 4 0 441.61 428.42 39.09 o -5 4 0 3330.21 3373.52 105.89 o -4 4 0 202.55 242.01 24.73 o -3 4 0 161.08 193.37 21.42 o -2 4 0 1738.03 1655.06 54.72 o -1 4 0 3766.69 3716.06 72.87 o 0 4 0 26630.50 25362.67 479.37 o 1 4 0 2380.97 2370.07 49.41 o 2 4 0 1652.77 1648.80 38.79 o 3 4 0 61.74 59.59 12.74 o 4 4 0 2679.08 2819.54 64.54 o 5 4 0 3541.32 3703.89 122.56 o 6 4 0 4399.15 4451.11 99.76 o 7 4 0 1726.52 1743.01 60.34 o 8 4 0 297.86 205.25 42.60 o 9 4 0 32.05 37.63 42.01 o 10 4 0 155.22 243.91 45.52 o 11 4 0 492.84 574.91 68.69 o -10 5 0 46.12 22.39 44.21 o -9 5 0 811.42 834.49 64.56 o -8 5 0 2333.47 2426.66 100.97 o -7 5 0 1094.73 1033.95 58.86 o -6 5 0 160.74 164.65 32.91 o -5 5 0 360.97 337.92 33.20 o -4 5 0 735.17 773.20 43.47 o -3 5 0 1120.57 1132.83 47.66 o -2 5 0 3325.65 3347.71 96.69 o -1 5 0 6615.86 6385.06 119.40 o 0 5 0 812.21 811.12 26.48 o 1 5 0 289.85 314.68 16.66 o 2 5 0 7470.93 7353.09 134.09 o 3 5 0 4414.90 4336.20 87.68 o 4 5 0 11857.55 11402.82 733.99 o 5 5 0 1434.10 1439.90 46.08 o 6 5 0 2.18 22.35 20.28 o 7 5 0 675.09 673.58 38.44 o 8 5 0 10.65 -11.05 33.91 o 9 5 0 422.36 414.93 55.26 o 10 5 0 1088.38 991.56 53.36 o -9 6 0 107.72 69.42 46.25 o -8 6 0 123.72 136.85 42.11 o -7 6 0 892.88 891.65 57.40 o -6 6 0 835.16 959.71 58.13 o -5 6 0 385.18 475.55 40.65 o -4 6 0 2645.65 2439.36 85.68 o -3 6 0 1011.09 1081.52 50.73 o -2 6 0 632.88 622.92 28.12 o -1 6 0 5825.01 6114.31 118.11 o 0 6 0 6203.53 6177.16 146.47 o 1 6 0 10359.06 10860.65 402.67 o 2 6 0 477.66 456.60 22.12 o 3 6 0 15.36 54.83 30.11 o 4 6 0 15.91 -14.48 16.41 o 5 6 0 2416.45 2545.67 65.51 o 6 6 0 1266.35 1277.07 48.61 o 7 6 0 1035.68 1047.90 46.37 o 8 6 0 457.54 447.23 111.05 o 9 6 0 43.11 43.82 45.67 o 10 6 0 173.13 295.37 58.62 o -9 7 0 477.89 367.91 58.27 o -8 7 0 961.46 953.48 65.58 o -7 7 0 388.71 334.46 45.81 o -6 7 0 1114.83 1077.48 62.36 o -5 7 0 58.14 123.90 33.98 o -4 7 0 246.15 301.31 36.66 o -3 7 0 3104.42 3139.64 152.79 o -2 7 0 1434.00 1360.75 42.69 o -1 7 0 1498.34 1505.32 44.49 o 0 7 0 563.35 565.13 38.41 o 1 7 0 4.48 63.34 44.91 o 2 7 0 4550.11 4671.25 110.10 o 3 7 0 2456.48 2439.54 75.63 o 4 7 0 2059.08 2001.42 54.70 o 5 7 0 899.19 859.69 41.38 o 6 7 0 906.64 839.16 61.03 o 7 7 0 9.58 15.84 27.90 o 8 7 0 701.74 742.55 75.22 o 9 7 0 1500.42 1591.04 64.53 o 10 7 0 738.40 817.41 77.02 o -9 8 0 82.38 9.49 44.06 o -8 8 0 0.15 -33.64 37.92 o -7 8 0 54.09 107.25 40.80 o -6 8 0 766.98 781.09 58.13 o -5 8 0 4128.56 4258.59 139.58 o -4 8 0 2071.74 2107.10 62.41 o -3 8 0 521.71 573.68 32.14 o -2 8 0 231.91 233.91 24.65 o -1 8 0 1638.24 1716.32 50.54 o 0 8 0 1549.88 1571.70 46.63 o 1 8 0 7075.36 7244.69 139.42 o 2 8 0 1771.19 1902.86 52.24 o 3 8 0 6.58 33.83 18.72 o 4 8 0 93.30 53.22 30.26 o 5 8 0 35.11 43.51 22.49 o 6 8 0 1558.10 1528.54 53.79 o 7 8 0 2131.37 2124.97 67.90 o 8 8 0 513.86 533.75 51.02 o 9 8 0 175.17 174.14 35.60 o 10 8 0 88.08 120.64 59.25 o -8 9 0 900.98 898.66 70.11 o -7 9 0 1846.84 1719.42 91.67 o -6 9 0 662.32 622.64 41.86 o -5 9 0 24.13 -27.09 27.09 o -4 9 0 2759.62 2659.35 75.98 o -3 9 0 3069.25 3029.13 79.13 o -2 9 0 2650.34 2615.39 70.22 o -1 9 0 1438.21 1415.81 47.66 o 0 9 0 742.48 764.14 34.23 o 1 9 0 547.17 517.70 60.37 o 2 9 0 2104.81 2186.28 58.65 o 3 9 0 3339.21 3378.74 80.03 o 4 9 0 5247.92 5192.06 112.56 o 5 9 0 3849.24 3729.45 90.65 o 6 9 0 564.74 558.98 47.88 o 7 9 0 197.43 207.92 76.04 o 8 9 0 325.80 314.41 39.34 o 9 9 0 919.93 928.36 76.09 o -8 10 0 4.58 -8.49 43.12 o -7 10 0 197.03 168.49 55.99 o -6 10 0 1379.63 1442.48 88.68 o -5 10 0 1215.13 1161.53 69.13 o -4 10 0 2921.67 3037.41 99.63 o -3 10 0 700.11 660.22 41.09 o -2 10 0 60.72 118.33 29.51 o -1 10 0 1559.28 1573.16 53.00 o 0 10 0 1101.58 1172.93 64.94 o 1 10 0 755.09 784.62 36.15 o 2 10 0 2033.88 2096.28 133.39 o 3 10 0 443.92 487.52 31.92 o 4 10 0 84.91 96.37 25.94 o 5 10 0 1177.95 1132.82 46.91 o 6 10 0 1218.53 1080.54 66.94 o 7 10 0 1485.88 1488.95 84.17 o 8 10 0 338.29 318.83 55.16 o 9 10 0 108.80 98.34 54.72 o -7 11 0 696.65 760.05 91.04 o -6 11 0 121.27 133.46 35.16 o -5 11 0 28.28 24.09 67.09 o -4 11 0 112.72 81.17 39.65 o -3 11 0 750.69 726.97 42.77 o -2 11 0 2990.96 2939.36 80.66 o -1 11 0 1429.27 1416.71 53.36 o 0 11 0 938.13 851.91 40.78 o 1 11 0 153.44 157.86 25.30 o 2 11 0 739.55 766.85 39.83 o 3 11 0 4536.28 4389.99 140.50 o 4 11 0 3094.45 2954.73 110.27 o 5 11 0 703.34 675.15 56.08 o 6 11 0 764.65 707.14 58.86 o 7 11 0 5.26 3.60 44.25 o 8 11 0 175.67 214.06 55.11 o -6 12 0 834.59 914.59 59.10 o -5 12 0 956.28 1037.28 58.09 o -4 12 0 717.15 668.63 47.72 o -3 12 0 873.89 859.38 50.50 o -2 12 0 326.62 362.33 36.71 o -1 12 0 241.05 268.56 33.12 o 0 12 0 1285.40 1330.00 71.03 o 1 12 0 2414.98 2585.76 99.90 o 2 12 0 859.70 955.18 58.32 o 3 12 0 32.72 20.64 30.77 o 4 12 0 1.33 -35.93 35.93 o 5 12 0 251.37 220.59 40.51 o 6 12 0 329.29 365.67 47.13 o 7 12 0 931.01 899.24 72.59 o 8 12 0 486.11 499.30 68.84 o -5 13 0 99.74 116.03 41.00 o -4 13 0 37.94 40.41 52.09 o -3 13 0 63.18 48.20 46.88 o -2 13 0 647.55 658.55 60.66 o -1 13 0 1732.42 1792.60 88.36 o 0 13 0 667.50 712.35 59.35 o 1 13 0 45.57 94.50 41.82 o 2 13 0 628.86 546.92 52.48 o 3 13 0 416.66 423.55 48.25 o 4 13 0 1122.84 1031.08 66.60 o 5 13 0 673.14 699.35 63.68 o 6 13 0 329.57 299.60 53.94 o 7 13 0 6.10 7.69 52.82 o -4 14 0 721.39 830.31 76.73 o -3 14 0 704.76 705.14 68.94 o -2 14 0 40.01 33.15 50.68 o -1 14 0 230.86 191.33 52.24 o 0 14 0 774.07 778.75 63.39 o 1 14 0 325.29 348.97 52.97 o 2 14 0 285.14 307.98 50.68 o 3 14 0 164.46 188.85 41.04 o 4 14 0 74.82 197.07 49.66 o 5 14 0 64.38 138.65 52.43 o 6 14 0 430.25 475.35 63.78 o -3 15 0 280.54 366.69 68.64 o -2 15 0 759.77 802.51 73.32 o -1 15 0 107.81 115.19 53.11 o 0 15 0 34.66 63.82 42.79 o 1 15 0 0.48 10.03 47.95 o 2 15 0 307.38 389.28 56.42 o 3 15 0 435.95 454.76 58.37 o 4 15 0 738.95 774.47 71.27 o 0 16 0 146.67 144.69 59.05 o 1 16 0 559.86 575.64 66.84 o 2 16 0 753.95 793.79 74.63 o -1 -16 1 6.81 111.73 58.52 o -4 -15 1 2.16 83.01 52.04 o -3 -15 1 265.22 320.78 61.73 o -2 -15 1 640.27 647.50 64.56 o -1 -15 1 724.30 662.40 64.75 o 0 -15 1 148.21 133.93 51.56 o 1 -15 1 50.81 127.26 54.14 o 2 -15 1 1.65 206.23 59.35 o 3 -15 1 248.44 249.17 64.70 o -6 -14 1 441.09 341.18 60.08 o -5 -14 1 421.14 446.53 59.49 o -4 -14 1 1120.00 1038.09 72.59 o -3 -14 1 1109.07 1223.67 75.61 o -2 -14 1 179.34 224.00 49.90 o -1 -14 1 104.69 124.05 44.74 o 0 -14 1 218.89 285.00 48.64 o 1 -14 1 864.90 988.73 71.03 o 2 -14 1 903.27 919.69 72.73 o 3 -14 1 351.73 393.76 60.27 o 4 -14 1 30.99 83.01 57.01 o -7 -13 1 771.60 752.46 74.92 o -6 -13 1 568.73 548.28 60.86 o -5 -13 1 235.12 281.05 52.19 o -4 -13 1 16.81 6.38 40.41 o -3 -13 1 191.76 197.12 44.35 o -2 -13 1 686.92 668.04 55.45 o -1 -13 1 560.15 561.91 53.26 o 0 -13 1 1170.71 1093.93 67.72 o 1 -13 1 202.37 275.45 47.56 o 2 -13 1 50.25 9.46 48.03 o 3 -13 1 362.81 348.20 42.67 o 4 -13 1 762.32 798.95 76.26 o 5 -13 1 636.14 673.09 54.47 o -7 -12 1 0.25 19.23 51.65 o -6 -12 1 537.50 442.20 54.57 o -5 -12 1 1083.15 1091.35 70.15 o -4 -12 1 715.03 751.59 57.20 o -3 -12 1 136.06 152.24 38.95 o -2 -12 1 734.53 748.52 54.62 o -1 -12 1 15.40 15.26 28.11 o 0 -12 1 504.37 519.96 37.99 o 1 -12 1 1866.40 1793.68 61.73 o 2 -12 1 1738.84 1719.25 62.34 o 3 -12 1 216.97 219.88 37.24 o 4 -12 1 33.32 38.89 37.32 o 5 -12 1 0.52 -34.27 89.12 o 6 -12 1 134.14 114.82 56.13 o -8 -11 1 295.62 374.09 60.08 o -7 -11 1 1118.50 1205.22 79.89 o -6 -11 1 1552.78 1515.24 81.40 o -5 -11 1 516.55 443.27 44.74 o -4 -11 1 78.82 103.68 27.45 o -3 -11 1 49.11 80.65 26.50 o -2 -11 1 2276.63 2260.46 66.03 o -1 -11 1 2638.07 2739.13 74.14 o 0 -11 1 1415.49 1430.25 51.47 o 1 -11 1 1221.02 1226.77 49.39 o 2 -11 1 96.46 102.13 42.70 o 3 -11 1 560.49 502.20 48.42 o 4 -11 1 293.29 271.99 37.20 o 5 -11 1 1788.08 1770.67 66.86 o 6 -11 1 1133.78 1081.08 100.07 o 7 -11 1 191.66 270.05 58.18 o -9 -10 1 519.99 584.31 70.74 o -8 -10 1 146.25 183.83 52.34 o -7 -10 1 2.26 33.81 30.32 o -6 -10 1 639.28 587.28 39.75 o -5 -10 1 766.20 770.84 44.86 o -4 -10 1 3608.29 3493.26 87.07 o -3 -10 1 7975.80 8016.58 179.60 o -2 -10 1 2400.36 2316.06 76.85 o -1 -10 1 11.62 29.37 23.16 o 0 -10 1 674.00 626.57 35.28 o 1 -10 1 2035.12 1967.58 78.06 o 2 -10 1 2731.86 2907.09 78.23 o 3 -10 1 1858.29 1848.94 61.99 o 4 -10 1 287.69 281.75 56.79 o 5 -10 1 51.83 127.79 57.67 o 6 -10 1 151.90 191.84 36.34 o 7 -10 1 327.72 326.41 42.62 o 8 -10 1 1161.64 1173.34 82.62 o -9 -9 1 69.89 90.11 38.62 o -8 -9 1 788.33 788.08 48.52 o -7 -9 1 1575.79 1526.63 90.16 o -6 -9 1 2747.83 2760.11 77.88 o -5 -9 1 2817.21 2800.52 75.83 o -4 -9 1 418.51 442.74 30.04 o -3 -9 1 246.21 243.89 25.36 o -2 -9 1 2092.37 2070.63 57.23 o -1 -9 1 3794.89 3744.20 85.07 o 0 -9 1 2060.50 2032.90 57.18 o 1 -9 1 867.21 859.83 37.91 o 2 -9 1 595.62 631.11 38.58 o 3 -9 1 737.93 728.60 85.66 o 4 -9 1 6074.48 5890.60 130.58 o 5 -9 1 3420.62 3387.12 159.66 o 6 -9 1 956.04 912.64 92.26 o 7 -9 1 388.03 352.08 38.15 o 8 -9 1 2.16 -18.84 49.02 o -10 -8 1 514.85 498.53 73.37 o -9 -8 1 760.39 813.48 52.57 o -8 -8 1 307.43 305.30 37.21 o -7 -8 1 426.68 385.80 55.57 o -6 -8 1 120.63 111.06 26.06 o -5 -8 1 3834.95 3687.88 88.88 o -4 -8 1 2942.44 2884.79 112.22 o -3 -8 1 2441.02 2460.77 62.78 o -2 -8 1 3202.68 3212.52 102.43 o -1 -8 1 116.81 148.54 33.86 o 0 -8 1 2529.92 2682.71 72.73 o 1 -8 1 777.59 777.13 34.44 o 2 -8 1 2542.88 2462.36 127.70 o 3 -8 1 1817.55 1765.63 69.84 o 4 -8 1 1115.50 1082.21 44.47 o 5 -8 1 21.40 94.96 30.26 o 6 -8 1 794.84 805.38 55.40 o 7 -8 1 431.71 483.34 52.63 o 8 -8 1 949.68 853.29 67.18 o 9 -8 1 558.17 691.22 67.38 o -10 -7 1 34.16 114.80 60.08 o -9 -7 1 68.30 101.67 34.65 o -8 -7 1 696.67 714.25 70.84 o -7 -7 1 2374.32 2282.98 70.34 o -6 -7 1 4321.31 4339.43 102.06 o -5 -7 1 390.45 453.65 86.58 o -4 -7 1 182.38 187.77 28.92 o -3 -7 1 200.21 182.49 19.25 o -2 -7 1 1399.01 1350.55 40.32 o -1 -7 1 5664.79 5837.99 176.24 o 0 -7 1 7896.85 7674.41 471.80 o 1 -7 1 2060.26 2048.05 53.37 o 2 -7 1 696.15 694.06 35.52 o 3 -7 1 958.98 1043.20 39.83 o 4 -7 1 2831.70 2844.85 73.27 o 5 -7 1 13149.57 12891.55 329.10 o 6 -7 1 4171.42 4415.21 141.96 o 7 -7 1 809.89 797.74 56.42 o 8 -7 1 170.58 220.00 41.97 o 9 -7 1 55.72 60.32 49.41 o -10 -6 1 567.70 597.74 69.37 o -9 -6 1 1029.55 1013.43 53.86 o -8 -6 1 677.15 723.08 59.74 o -7 -6 1 52.08 25.91 24.40 o -6 -6 1 458.27 473.24 71.18 o -5 -6 1 1125.91 1212.21 55.01 o -4 -6 1 3530.23 3529.84 79.65 o -3 -6 1 8738.52 8244.39 556.09 o -2 -6 1 2206.84 2197.98 52.28 o -1 -6 1 1480.74 1480.17 39.34 o 0 -6 1 2958.67 3113.83 127.58 o 1 -6 1 8313.85 8541.87 271.00 o 2 -6 1 2301.73 2310.15 97.98 o 3 -6 1 7897.57 8149.49 161.02 o 4 -6 1 994.34 1041.79 50.92 o 5 -6 1 1560.49 1509.94 66.99 o 6 -6 1 116.58 115.97 34.27 o 7 -6 1 551.25 615.66 48.44 o 8 -6 1 1901.12 2009.05 92.65 o 9 -6 1 1087.35 1099.63 76.19 o 10 -6 1 192.02 254.08 53.21 o -10 -5 1 177.80 208.03 48.98 o -9 -5 1 83.19 81.40 40.80 o -8 -5 1 1612.05 1600.12 63.46 o -7 -5 1 1006.68 1043.87 73.46 o -6 -5 1 3799.22 3824.56 90.94 o -5 -5 1 3602.47 3503.41 80.89 o -4 -5 1 4205.90 4456.51 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