Acta Cryst. (2004). E60, m1106-m1107  [ doi:10.1107/S1600536804016472 ]

(Acetonitrile-N)(4'-phenyl-2,2':6',2''-terpyridine-³N)silver(I) hexafluorophosphate acetonitrile solvate

L. Hou, D. Li, Y.-G. Yin, T. Wu and S. W. Ng

Online 17 July 2004

Key indicators

• Single-crystal X-ray study
• T = 295 K
• Mean (C-C) = 0.009 Å
• R factor = 0.057
• wR factor = 0.178
• Data-to-parameter ratio = 13.0

checkCIF/PLATON results

No syntax errors found



Alert level A
ABSTM02_ALERT_3_A  The ratio of expected to reported Tmax/Tmin(RR') is < 0.50
            Tmin and Tmax reported:      0.354     0.898
            Tmin' and Tmax expected:      0.828     0.895
            RR' =      0.426
            Please check that your absorption correction is appropriate.

PLAT061_ALERT_3_A Tmax/Tmin Range Test RR' too Large .............       0.42       

Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.52       
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.51 Ratio 
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.06 Ratio 
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ag1    -   N3      ..       5.00 su    
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C23     
PLAT244_ALERT_4_C Low Solvent  U(eq) as Compared to Neighbors ....         P1     
PLAT244_ALERT_4_C Low Solvent  U(eq) as Compared to Neighbors ....        C25     
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...          9       

   2 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   4 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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