Acta Cryst. (2004). E60, m1035-m1037  [ doi:10.1107/S1600536804015508 ]

The tetrachlorodiphenylstannate(IV) salt of protonated di-2-pyridyl ketone N⁴-ethylthiosemicarbazone

R. Venkatraman, P. C. Ray and F. R. Fronczek

Online 9 July 2004

Key indicators

• Single-crystal X-ray study
• T = 102 K
• Mean (C-C) = 0.002 Å
• R factor = 0.029
• wR factor = 0.066
• Data-to-parameter ratio = 31.2

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.05 Ratio 
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.50 Ratio 
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Sn1    -   C1      ..       5.26 su    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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