Acta Cryst. (2004). E60, m1163-m1165  [ doi:10.1107/S1600536804017209 ]

cis-{trans-1,2-Bis[2-(diphenylphosphino)benzamido]cyclohexane-²P,P'}dichloroplatinum(II) chloroform trisolvate

S. Burger, B. Therrien and G. Süss-Fink

Online 24 July 2004

Key indicators

• Single-crystal X-ray study
• T = 153 K
• Mean (C-C) = 0.007 Å
• R factor = 0.036
• wR factor = 0.092
• Data-to-parameter ratio = 15.5

checkCIF/PLATON results

No syntax errors found



Alert level A
PLAT027_ALERT_3_A _diffrn_reflns_theta_full (too) Low ............      24.91 Deg.  

Alert level B
PLAT482_ALERT_4_B Small D-H..A Angle Rep for C1     ..  O1      ..      89.00 Deg.  

Alert level C
RINTA01_ALERT_3_C  The value of Rint is greater than 0.10
            Rint given   0.133
PLAT020_ALERT_3_C The value of Rint is greater than 0.10 .........       0.13       
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT244_ALERT_4_C Low  Solvent U(eq) as Compared to Neighbors  for        C45     
PLAT244_ALERT_4_C Low  Solvent U(eq) as Compared to Neighbors  for        C46     
PLAT244_ALERT_4_C Low  Solvent U(eq) as Compared to Neighbors  for        C47     
PLAT369_ALERT_2_C Long   C(sp2)-C(sp2) Bond  C14    -   C15    ...       1.53 Ang.  
PLAT431_ALERT_2_C Short Inter HL..A Contact  Cl6    ..  Cl9     ..       3.23 Ang.  
PLAT480_ALERT_4_C Long H...A H-Bond Reported H1     ..  O1      ..       2.66 Ang.  
PLAT480_ALERT_4_C Long H...A H-Bond Reported H1     ..  O2      ..       2.65 Ang.  
PLAT480_ALERT_4_C Long H...A H-Bond Reported H9     ..  C1X     ..       2.82 Ang.  
PLAT716_ALERT_1_C H...A   Unknown or Inconsistent Label ..........        C1X     
                    H9     C1X                                                  
PLAT717_ALERT_1_C D...A   Unknown or Inconsistent Label ..........        C1X     
                    C9     C1X                                                  
PLAT718_ALERT_1_C D-H..A  Unknown or Inconsistent Label ..........        C1X     
                    C9     H9     C1X                                           
PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd.  #          2       
              C H Cl3                                                           
PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd.  #          3       
              C H Cl3                                                           

   1 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
  16 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   4 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   9 ALERT type 4 Improvement, methodology, query or suggestion

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