Acta Cryst. (2004). E60, o1431-o1432  [ doi:10.1107/S1600536804016575 ]

2-Amino-N-(2-chlorophenyl)-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide

Vasu, K. A. Nirmala, D. Chopra, S. Mohan and J. Saravanan

Online 31 July 2004

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• R factor = 0.052
• wR factor = 0.143
• Data-to-parameter ratio = 10.2

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.97 Ratio 
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C14     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C11     
PLAT340_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...          5       
PLAT352_ALERT_3_C Short   N-H Bond (0.87A)   N2     -   H3N    ...       0.76 Ang.  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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