Acta Cryst. (2004). E60, m1245-m1247  [ doi:10.1107/S1600536804019385 ]

A mixed-halogen tricarbonylmanganese(I) complex: fac-[MnBr_0.3Cl_0.7{Ph₂P(CH₂)₃PPh₂}(CO)₃]

M. E. Light, M. B. Hursthouse, M. A. Beckett and D. S. Brassington

Online 13 August 2004

Key indicators

• Single-crystal X-ray study
• T = 120 K
• Mean (C-C) = 0.003 Å
• R factor = 0.025
• wR factor = 0.064
• Data-to-parameter ratio = 14.2

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)...          ?
PLAT077_ALERT_4_C Unitcell contains non-integer number of atoms ..          ?
PLAT141_ALERT_4_C su on a - Axis Small or Missing (x 100000) .....         10 Ang.  
PLAT301_ALERT_3_C Main Residue  Disorder .........................       3.00 Perc. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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