Acta Cryst. (2004). E60, m1259-m1260  [ doi:10.1107/S1600536804019403 ]

[5-Bromo-N-(2-pyridylethylsulfanylethyl)salicylideneiminato-⁴N,N',O,S]copper(II) perchlorate

L. A. Saghatforoush, M. Hossaini Sadr, W. Lewis, J. Wikaira, W. T. Robinson and S. W. Ng

Online 13 August 2004

Key indicators

• Single-crystal X-ray study
• T = 113 K
• R factor = 0.039
• wR factor = 0.107
• Data-to-parameter ratio = 15.0

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT061_ALERT_3_B Tmax/Tmin Range Test RR' too Large .............       0.70       

Alert level C
ABSTM02_ALERT_3_C  The ratio of expected to reported Tmax/Tmin(RR') is < 0.90
            Tmin and Tmax reported:      0.145     0.576
            Tmin' and Tmax expected:      0.175     0.576
            RR' =      0.827
            Please check that your absorption correction is appropriate.
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......       0.96       
PLAT244_ALERT_4_C Low  Solvent U(eq) as Compared to Neighbors  for        Cl1     
PLAT432_ALERT_2_C Short Inter X...Y Contact  C1     ..  C13     ..       3.19 Ang.  

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion

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