# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' sa0296 in P1 [D-histidine L-tartrate]' _shelx_refln_list_code 4 _shelx_F_calc_maximum 55.48 _exptl_crystal_F_000 160.00 _reflns_d_resolution_high 0.7561 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' _cell_length_a 5.3779 _cell_length_b 7.6477 _cell_length_c 8.4860 _cell_angle_alpha 71.972 _cell_angle_beta 73.864 _cell_angle_gamma 81.002 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1532.25 1364.31 48.86 o 2 0 0 97.78 105.00 1.68 o 3 0 0 28.72 28.99 0.48 o 4 0 0 126.41 120.23 2.72 o 5 0 0 8.87 8.39 0.26 o 6 0 0 11.19 9.92 0.31 o -5 1 0 23.60 22.27 0.57 o -4 1 0 37.76 38.81 0.92 o -3 1 0 23.58 26.77 0.45 o -2 1 0 335.62 351.37 7.95 o -1 1 0 1016.18 994.76 22.50 o 0 1 0 14.98 15.14 0.45 o 1 1 0 171.76 191.99 4.28 o 2 1 0 19.09 25.19 0.59 o 3 1 0 151.83 161.13 3.61 o 4 1 0 30.61 31.08 0.75 o 5 1 0 18.94 17.51 0.46 o 6 1 0 34.13 32.63 0.81 o -5 2 0 42.27 43.46 1.04 o -4 2 0 248.02 268.40 6.00 o -3 2 0 21.92 18.45 0.46 o -2 2 0 97.75 100.65 2.30 o -1 2 0 287.23 288.21 6.53 o 0 2 0 172.72 181.50 2.89 o 1 2 0 432.81 485.48 7.70 o 2 2 0 213.87 229.87 5.13 o 3 2 0 78.95 84.02 1.91 o 4 2 0 55.88 55.59 1.29 o 5 2 0 59.04 57.39 1.35 o 6 2 0 0.66 0.72 0.10 o -5 3 0 10.84 10.51 0.31 o -4 3 0 24.26 22.21 0.39 o -3 3 0 6.62 6.17 0.19 o -2 3 0 273.38 274.00 6.22 o -1 3 0 23.30 27.89 0.67 o 0 3 0 35.70 37.31 0.61 o 1 3 0 222.62 251.80 3.22 o 2 3 0 150.07 153.11 2.44 o 3 3 0 150.93 159.26 3.58 o 4 3 0 173.76 178.11 4.02 o 5 3 0 0.98 1.23 0.11 o 6 3 0 14.00 13.48 0.40 o -3 4 0 2.25 2.31 0.11 o -2 4 0 69.94 67.08 1.57 o -1 4 0 189.16 208.44 3.33 o 0 4 0 91.27 90.82 1.47 o 1 4 0 153.40 174.28 2.23 o 2 4 0 49.95 52.86 1.23 o 3 4 0 99.06 93.37 2.14 o 4 4 0 76.07 72.04 1.68 o 5 4 0 2.90 2.86 0.22 o 6 4 0 1.11 1.11 0.12 o -4 5 0 16.10 13.70 0.39 o -3 5 0 58.98 53.75 1.29 o -2 5 0 99.73 95.91 2.23 o -1 5 0 147.98 132.17 6.18 o 0 5 0 56.36 53.41 0.93 o 1 5 0 25.09 23.39 0.41 o 2 5 0 83.39 85.11 1.38 o 3 5 0 8.35 8.06 0.26 o 4 5 0 54.95 55.79 1.33 o 5 5 0 25.68 27.69 0.73 o -4 6 0 4.18 3.59 0.17 o -2 6 0 98.34 94.77 2.22 o -1 6 0 89.65 92.64 1.52 o 0 6 0 13.03 12.24 0.24 o 2 6 0 3.65 3.08 0.15 o 3 6 0 17.98 20.04 0.54 o 4 6 0 0.63 0.50 0.09 o 5 6 0 5.32 6.45 0.26 o -4 7 0 0.37 0.38 0.10 o 0 7 0 15.64 15.19 0.42 o 1 7 0 7.23 6.08 0.22 o 2 7 0 28.04 24.85 0.65 o 3 7 0 7.99 8.90 0.30 o 4 7 0 70.13 82.97 1.96 o 0 8 0 17.12 17.79 0.50 o 1 8 0 7.54 7.65 0.35 o 2 8 0 4.01 3.71 0.18 o 3 8 0 11.82 11.16 0.37 o 0 9 0 30.56 32.19 0.60 o 1 9 0 38.80 38.37 0.97 o 0 -9 1 14.19 16.16 0.49 o -2 -8 1 3.90 4.78 0.22 o -1 -8 1 21.19 19.22 0.53 o 0 -8 1 9.34 9.10 0.39 o 1 -8 1 2.91 3.42 0.13 o 2 -8 1 5.49 6.44 0.26 o -4 -7 1 18.71 20.92 0.60 o -3 -7 1 23.72 22.26 0.60 o -2 -7 1 7.91 6.93 0.25 o -1 -7 1 10.66 11.51 0.42 o 0 -7 1 31.70 30.69 0.55 o 1 -7 1 6.48 6.84 0.35 o 2 -7 1 30.03 29.24 0.76 o 3 -7 1 0.06 0.03 0.06 o -4 -6 1 16.82 18.21 0.52 o -3 -6 1 2.81 2.66 0.14 o -2 -6 1 38.71 38.61 0.94 o -1 -6 1 47.32 44.44 0.75 o 0 -6 1 186.21 180.09 2.90 o 1 -6 1 229.77 233.75 3.87 o 2 -6 1 70.23 65.70 1.57 o 3 -6 1 7.39 6.01 0.22 o 4 -6 1 1.60 1.82 0.13 o -5 -5 1 27.45 26.96 0.72 o -4 -5 1 6.16 4.93 0.21 o -3 -5 1 8.71 8.13 0.27 o -2 -5 1 71.62 74.58 1.72 o -1 -5 1 161.38 170.50 2.74 o 0 -5 1 54.65 47.11 0.79 o 1 -5 1 181.67 163.27 5.82 o 2 -5 1 50.41 49.41 1.19 o 3 -5 1 16.60 15.43 0.43 o 4 -5 1 1.88 2.09 0.13 o -5 -4 1 4.41 4.39 0.19 o -4 -4 1 30.26 30.55 0.77 o -3 -4 1 401.04 437.23 9.75 o -2 -4 1 27.46 28.02 0.48 o -1 -4 1 92.65 105.81 1.71 o 0 -4 1 34.17 34.69 0.58 o 1 -4 1 36.56 39.35 1.02 o 2 -4 1 3.27 3.72 0.15 o 3 -4 1 12.09 11.25 0.33 o 4 -4 1 10.71 10.15 0.30 o -6 -3 1 0.94 0.75 0.11 o -5 -3 1 11.35 12.21 0.36 o -4 -3 1 118.52 114.45 2.61 o -3 -3 1 39.95 36.51 0.87 o -2 -3 1 5.94 5.97 0.12 o -1 -3 1 239.25 264.70 4.21 o 0 -3 1 477.60 531.55 8.42 o 1 -3 1 117.91 122.54 1.58 o 2 -3 1 38.66 37.23 0.61 o 3 -3 1 22.78 25.33 0.63 o 4 -3 1 121.92 122.84 2.83 o 6 -3 1 3.98 5.32 0.24 o -6 -2 1 0.30 0.10 0.08 o -5 -2 1 0.10 0.03 0.06 o -4 -2 1 27.92 26.69 0.66 o -3 -2 1 49.03 49.15 1.15 o -2 -2 1 258.25 307.17 4.88 o -1 -2 1 401.52 417.34 6.61 o 0 -2 1 536.84 563.96 8.95 o 1 -2 1 298.10 293.35 3.74 o 2 -2 1 139.75 150.51 3.43 o 3 -2 1 226.65 252.35 5.73 o 4 -2 1 110.80 115.12 1.86 o 6 -2 1 4.92 6.38 0.26 o -6 -1 1 17.70 17.41 0.48 o -5 -1 1 64.52 61.47 1.45 o -4 -1 1 63.60 57.31 1.34 o -3 -1 1 44.45 40.37 0.95 o -2 -1 1 401.69 440.51 9.80 o -1 -1 1 55.26 55.66 0.89 o 0 -1 1 1235.62 1029.56 47.52 o 1 -1 1 376.04 385.68 6.02 o 2 -1 1 98.53 98.22 2.24 o 3 -1 1 71.64 75.57 1.22 o 4 -1 1 17.59 17.82 0.44 o 6 -1 1 8.13 9.73 0.32 o -6 0 1 14.98 14.18 0.41 o -5 0 1 12.29 11.32 0.33 o -4 0 1 25.71 21.99 0.55 o -3 0 1 309.34 339.53 7.57 o -2 0 1 81.61 83.72 1.89 o -1 0 1 413.81 376.97 8.39 o 0 0 1 50.63 54.94 0.90 o 1 0 1 87.15 81.59 1.05 o 2 0 1 242.82 258.03 4.09 o 3 0 1 42.92 47.05 0.76 o 4 0 1 3.13 2.28 0.10 o 5 0 1 58.24 51.49 1.20 o 6 0 1 3.11 3.76 0.19 o -6 1 1 4.61 4.71 0.20 o -5 1 1 11.45 11.18 0.33 o -4 1 1 18.26 18.21 0.47 o -3 1 1 161.52 174.60 2.78 o -2 1 1 381.64 394.70 6.25 o -1 1 1 86.70 82.21 1.87 o 0 1 1 103.82 103.23 2.36 o 1 1 1 350.01 294.84 3.77 o 2 1 1 108.43 115.00 1.83 o 3 1 1 122.80 133.53 2.13 o 4 1 1 48.65 45.72 1.06 o 5 1 1 173.20 168.13 3.79 o 6 1 1 32.69 32.30 0.81 o -6 2 1 1.28 1.89 0.13 o -5 2 1 66.68 64.46 1.52 o -4 2 1 158.53 168.39 3.80 o -3 2 1 0.01 0.11 0.02 o -2 2 1 351.89 386.12 8.73 o -1 2 1 47.54 49.57 1.15 o 0 2 1 163.64 159.57 2.54 o 1 2 1 170.54 185.62 2.37 o 2 2 1 192.45 178.82 2.84 o 3 2 1 321.26 341.12 7.59 o 4 2 1 11.53 12.66 0.34 o 5 2 1 17.25 15.54 0.42 o 6 2 1 2.28 2.82 0.16 o -5 3 1 41.88 46.63 1.12 o -4 3 1 6.02 6.67 0.22 o -3 3 1 200.26 214.30 4.88 o -2 3 1 27.27 25.68 0.62 o 0 3 1 370.49 386.39 6.13 o 1 3 1 3073.56 2248.88 75.81 o 2 3 1 200.06 205.09 2.63 o 3 3 1 69.06 77.18 1.76 o 4 3 1 5.99 5.63 0.13 o 5 3 1 28.71 28.79 0.72 o 6 3 1 4.59 4.81 0.28 o -5 4 1 1.05 1.37 0.11 o -3 4 1 32.45 27.85 0.69 o -2 4 1 106.62 116.81 2.69 o 0 4 1 283.40 295.85 4.70 o 1 4 1 88.54 91.02 1.18 o 2 4 1 19.88 20.99 0.29 o 3 4 1 66.58 70.37 1.12 o 4 4 1 137.93 138.49 2.18 o 5 4 1 29.94 29.79 0.52 o 6 4 1 5.04 5.71 0.23 o -5 5 1 1.75 1.82 0.11 o -4 5 1 29.51 27.58 0.70 o -3 5 1 23.77 21.85 0.57 o -2 5 1 0.06 0.10 0.05 o 0 5 1 48.29 44.01 0.74 o 1 5 1 127.76 134.15 2.16 o 2 5 1 101.94 103.72 1.68 o 3 5 1 36.45 35.91 0.87 o 4 5 1 55.70 57.23 1.36 o 5 5 1 4.24 3.67 0.18 o 6 5 1 1.14 0.68 0.11 o -4 6 1 13.62 12.94 0.38 o -3 6 1 4.53 5.28 0.21 o -2 6 1 6.08 6.86 0.24 o -1 6 1 66.35 68.54 1.63 o 0 6 1 34.49 34.71 0.60 o 1 6 1 27.36 28.50 0.50 o 2 6 1 24.35 26.20 0.46 o 3 6 1 0.77 0.41 0.08 o 4 6 1 5.55 6.21 0.24 o 5 6 1 34.82 38.47 0.97 o -4 7 1 0.71 0.99 0.11 o -3 7 1 3.25 2.67 0.16 o -2 7 1 4.88 4.65 0.20 o -1 7 1 6.91 6.54 0.24 o 0 7 1 78.14 78.46 1.30 o 1 7 1 40.31 39.35 0.96 o 2 7 1 19.93 19.19 0.52 o 3 7 1 31.86 32.24 0.82 o 4 7 1 45.24 43.16 1.07 o 5 7 1 9.52 11.18 0.38 o -2 8 1 0.04 0.04 0.08 o -1 8 1 1.31 1.14 0.11 o 0 8 1 1.14 1.51 0.08 o 1 8 1 1.19 1.79 0.19 o 2 8 1 35.01 31.67 0.81 o 3 8 1 1.09 1.33 0.13 o 4 8 1 7.30 8.09 0.31 o -1 9 1 22.96 25.94 0.72 o 0 9 1 41.34 44.49 0.79 o 1 9 1 0.04 0.10 0.05 o 2 9 1 14.25 14.11 0.43 o -2 -8 2 0.80 1.08 0.13 o -1 -8 2 3.82 4.24 0.20 o 0 -8 2 7.88 7.94 0.20 o 1 -8 2 4.13 4.16 0.27 o -3 -7 2 23.45 25.18 0.68 o -2 -7 2 37.45 37.10 0.93 o -1 -7 2 23.07 21.90 0.53 o 0 -7 2 10.55 11.09 0.58 o 1 -7 2 0.68 0.86 0.07 o 2 -7 2 3.98 3.95 0.20 o 3 -7 2 6.47 6.62 0.26 o -4 -6 2 19.57 21.14 0.59 o -3 -6 2 34.49 35.49 0.89 o -2 -6 2 3.19 2.65 0.14 o -1 -6 2 2.13 1.81 0.08 o 0 -6 2 78.34 77.42 1.28 o 1 -6 2 29.92 29.94 0.53 o 2 -6 2 22.31 21.22 0.57 o 3 -6 2 7.93 7.86 0.28 o 4 -6 2 10.38 9.11 0.31 o -4 -5 2 50.94 54.37 1.32 o -3 -5 2 26.96 26.70 0.69 o -2 -5 2 67.24 64.52 1.51 o -1 -5 2 43.74 39.28 2.43 o 0 -5 2 10.20 10.63 0.22 o 1 -5 2 7.66 8.10 0.18 o 2 -5 2 48.74 47.06 1.15 o 3 -5 2 71.45 68.45 1.64 o 4 -5 2 6.14 6.14 0.24 o -5 -4 2 10.80 10.85 0.35 o -4 -4 2 29.17 26.13 0.67 o -3 -4 2 123.10 121.44 2.77 o -2 -4 2 58.73 60.87 1.42 o -1 -4 2 36.55 38.95 0.65 o 0 -4 2 152.08 164.07 2.63 o 1 -4 2 47.84 46.69 2.27 o 2 -4 2 39.75 43.34 1.05 o 3 -4 2 102.97 101.18 2.36 o 4 -4 2 23.61 22.58 0.59 o -5 -3 2 1.25 1.58 0.12 o -4 -3 2 83.86 86.16 2.00 o -3 -3 2 146.27 153.05 3.46 o -2 -3 2 117.57 131.74 2.11 o -1 -3 2 112.57 120.27 1.93 o 0 -3 2 34.86 37.51 0.62 o 1 -3 2 513.56 528.50 6.74 o 2 -3 2 220.61 240.97 3.77 o 3 -3 2 66.97 76.20 1.22 o 4 -3 2 30.41 31.60 0.58 o 5 -3 2 28.69 30.11 0.74 o -5 -2 2 25.66 25.82 0.67 o -4 -2 2 122.17 120.48 2.75 o -3 -2 2 60.53 60.45 1.40 o -2 -2 2 55.17 51.56 0.84 o -1 -2 2 782.01 816.96 15.24 o 0 -2 2 886.04 909.70 14.43 o 1 -2 2 103.64 110.93 1.43 o 2 -2 2 425.05 446.49 6.96 o 3 -2 2 3.11 4.12 0.10 o 4 -2 2 14.76 13.90 0.38 o 5 -2 2 22.25 25.53 0.65 o 6 -2 2 9.93 11.53 0.37 o -6 -1 2 8.04 7.04 0.26 o -5 -1 2 11.06 10.03 0.31 o -4 -1 2 58.95 55.62 1.31 o -3 -1 2 52.26 52.10 1.21 o -2 -1 2 365.86 409.67 6.49 o -1 -1 2 91.57 92.58 2.40 o 0 -1 2 308.83 333.52 5.28 o 1 -1 2 107.22 109.73 1.41 o 2 -1 2 104.05 109.24 1.72 o 3 -1 2 78.47 74.30 0.97 o 4 -1 2 32.06 33.11 0.45 o 5 -1 2 33.20 36.04 0.87 o 6 -1 2 8.80 10.19 0.34 o -6 0 2 1.23 1.42 0.13 o -5 0 2 26.60 23.05 0.60 o -4 0 2 47.96 44.69 1.06 o -3 0 2 173.41 149.52 3.37 o -2 0 2 73.46 81.57 1.31 o -1 0 2 431.10 423.88 6.72 o 0 0 2 1155.53 1153.91 18.30 o 1 0 2 3053.55 2537.17 57.50 o 2 0 2 234.31 240.09 3.07 o 3 0 2 110.36 117.39 1.51 o 4 0 2 5.98 6.26 0.14 o 5 0 2 37.47 38.03 0.91 o 6 0 2 0.01 0.10 0.08 o -6 1 2 7.69 8.02 0.29 o -5 1 2 7.86 7.74 0.26 o -4 1 2 80.79 79.51 1.84 o -3 1 2 32.28 28.92 0.70 o -2 1 2 79.39 91.76 1.47 o -1 1 2 362.19 405.69 9.17 o 0 1 2 878.71 847.72 19.19 o 1 1 2 895.89 851.73 13.11 o 2 1 2 106.58 111.70 1.43 o 3 1 2 9.93 11.25 0.16 o 4 1 2 94.78 94.90 1.50 o 5 1 2 17.69 14.73 0.41 o 6 1 2 17.81 17.81 0.50 o -6 2 2 1.20 1.98 0.15 o -5 2 2 57.66 63.82 1.51 o -4 2 2 40.48 44.24 1.06 o -3 2 2 64.96 75.42 1.23 o -2 2 2 76.59 80.23 1.84 o -1 2 2 59.11 58.27 1.34 o 0 2 2 404.45 425.18 9.61 o 1 2 2 593.54 604.47 7.72 o 2 2 2 209.54 226.69 2.90 o 3 2 2 257.52 261.74 3.35 o 4 2 2 6.78 6.42 0.44 o 5 2 2 23.85 22.25 0.45 o 6 2 2 7.21 6.63 0.25 o -5 3 2 6.70 7.20 0.25 o -4 3 2 20.29 21.72 0.56 o -3 3 2 18.17 18.43 0.47 o -2 3 2 0.34 0.29 0.04 o -1 3 2 0.82 1.16 0.07 o 0 3 2 388.91 408.37 9.23 o 1 3 2 292.50 307.68 3.93 o 2 3 2 7.03 6.40 0.16 o 3 3 2 127.13 130.33 1.68 o 4 3 2 55.53 58.35 0.94 o 5 3 2 11.85 11.17 0.23 o 6 3 2 8.39 7.47 0.26 o -5 4 2 1.68 2.20 0.13 o -4 4 2 16.45 13.91 0.38 o -3 4 2 23.17 22.45 0.57 o -2 4 2 99.22 98.14 2.27 o -1 4 2 147.10 138.82 3.17 o 0 4 2 25.87 25.61 0.44 o 1 4 2 26.39 23.43 0.34 o 2 4 2 5.74 6.67 0.11 o 3 4 2 27.47 26.88 0.45 o 4 4 2 17.87 17.49 0.32 o 5 4 2 0.30 0.39 0.05 o 6 4 2 10.66 9.42 0.31 o -5 5 2 0.94 1.48 0.11 o -3 5 2 78.70 71.91 1.70 o -2 5 2 8.04 7.16 0.23 o -1 5 2 62.04 61.27 1.44 o 0 5 2 32.04 31.18 0.53 o 1 5 2 46.86 47.31 0.78 o 2 5 2 86.44 81.84 2.47 o 3 5 2 79.04 71.96 1.15 o 4 5 2 234.85 235.82 3.68 o 5 5 2 48.91 48.82 0.82 o 6 5 2 0.27 0.33 0.09 o -4 6 2 8.36 8.09 0.28 o -3 6 2 10.50 11.20 0.34 o -2 6 2 58.53 55.09 1.32 o -1 6 2 8.17 6.97 0.23 o 0 6 2 127.01 115.10 1.87 o 1 6 2 7.49 8.13 0.17 o 2 6 2 115.04 120.04 1.94 o 3 6 2 15.64 12.92 0.37 o 4 6 2 34.25 32.20 0.81 o 5 6 2 8.59 9.23 0.31 o 6 6 2 8.49 9.84 0.35 o -4 7 2 1.52 1.58 0.14 o -3 7 2 10.69 10.70 0.34 o -2 7 2 20.80 19.02 0.52 o -1 7 2 174.09 162.18 3.74 o 0 7 2 186.51 183.91 2.96 o 1 7 2 53.68 52.77 0.89 o 2 7 2 19.35 16.06 0.33 o 3 7 2 37.49 36.96 0.91 o 4 7 2 14.65 15.07 0.44 o 5 7 2 15.76 15.91 0.47 o -2 8 2 4.60 4.48 0.21 o -1 8 2 6.54 6.09 0.23 o 0 8 2 33.73 34.82 0.62 o 1 8 2 0.41 0.72 0.06 o 2 8 2 17.32 15.17 0.44 o 3 8 2 4.70 4.82 0.21 o 4 8 2 1.85 1.70 0.15 o -1 9 2 0.41 0.60 0.10 o 0 9 2 16.58 16.02 0.47 o 1 9 2 3.72 4.09 0.14 o 2 9 2 18.70 17.12 0.49 o 3 9 2 4.13 5.05 0.23 o -1 -8 3 26.52 26.68 0.71 o 0 -8 3 40.23 40.49 1.03 o -2 -7 3 14.48 12.95 0.40 o -1 -7 3 8.05 7.49 0.26 o 0 -7 3 2.02 2.01 0.09 o 1 -7 3 4.62 4.61 0.20 o 2 -7 3 3.68 3.74 0.19 o -3 -6 3 9.90 9.35 0.31 o -2 -6 3 15.60 14.53 0.42 o -1 -6 3 67.07 66.70 1.11 o 0 -6 3 32.74 31.58 1.38 o 1 -6 3 19.05 17.75 0.34 o 2 -6 3 33.10 32.92 0.85 o 3 -6 3 48.27 45.54 1.15 o 4 -6 3 7.52 8.14 0.30 o -4 -5 3 5.70 5.47 0.23 o -3 -5 3 1.68 1.95 0.13 o -2 -5 3 0.98 0.76 0.09 o -1 -5 3 10.58 9.24 0.20 o 0 -5 3 10.16 9.84 0.21 o 1 -5 3 118.05 117.79 1.91 o 2 -5 3 6.31 5.98 0.22 o 3 -5 3 20.21 18.07 0.51 o 4 -5 3 6.71 6.31 0.24 o -4 -4 3 8.56 8.07 0.28 o -3 -4 3 20.40 19.80 0.52 o -2 -4 3 40.50 41.77 1.00 o -1 -4 3 45.79 45.80 0.80 o 0 -4 3 224.61 218.25 3.49 o 1 -4 3 72.16 68.51 1.12 o 2 -4 3 14.99 13.18 0.37 o 3 -4 3 11.22 9.70 0.30 o 4 -4 3 1.27 0.80 0.09 o -5 -3 3 7.64 7.52 0.27 o -4 -3 3 37.14 34.85 0.87 o -3 -3 3 153.37 159.28 3.61 o -2 -3 3 61.90 66.45 1.54 o -1 -3 3 23.22 21.30 0.37 o 0 -3 3 3.21 4.28 0.12 o 1 -3 3 68.28 70.44 1.15 o 2 -3 3 15.34 16.96 0.30 o 3 -3 3 19.67 17.65 0.32 o 4 -3 3 22.80 20.60 0.54 o -5 -2 3 1.01 0.65 0.09 o -4 -2 3 25.07 26.06 0.66 o -3 -2 3 55.62 58.02 1.36 o -2 -2 3 8.29 7.22 0.22 o -1 -2 3 203.45 215.69 3.43 o 0 -2 3 37.86 38.74 0.64 o 1 -2 3 113.49 113.24 1.46 o 2 -2 3 1.53 1.05 0.07 o 3 -2 3 36.48 38.87 0.64 o 4 -2 3 69.94 73.56 1.19 o 5 -2 3 5.05 5.22 0.22 o 6 -2 3 1.73 2.53 0.17 o -5 -1 3 8.85 8.64 0.29 o -4 -1 3 6.13 5.30 0.20 o -3 -1 3 81.35 85.52 1.96 o -2 -1 3 136.58 154.53 2.47 o -1 -1 3 160.38 185.06 2.95 o 0 -1 3 15.43 16.47 0.28 o 1 -1 3 203.54 215.46 2.76 o 2 -1 3 31.86 30.60 0.50 o 3 -1 3 0.57 0.26 0.03 o 4 -1 3 122.00 122.45 1.95 o 5 -1 3 56.70 61.14 1.41 o 6 -1 3 9.97 11.29 0.37 o -5 0 3 49.99 47.11 1.14 o -4 0 3 4.86 4.90 0.18 o -3 0 3 88.03 97.99 2.24 o -2 0 3 284.68 323.11 5.13 o -1 0 3 70.23 66.75 1.08 o 0 0 3 95.79 98.90 1.58 o 1 0 3 417.32 418.21 6.52 o 2 0 3 341.05 363.40 5.67 o 3 0 3 105.70 106.09 1.37 o 4 0 3 68.19 69.90 1.13 o 5 0 3 51.72 53.77 1.24 o 6 0 3 30.82 31.89 0.80 o -5 1 3 3.28 3.76 0.17 o -4 1 3 4.56 3.88 0.16 o -3 1 3 22.75 24.56 0.61 o -2 1 3 46.87 50.43 0.83 o -1 1 3 385.97 407.81 6.47 o 0 1 3 1217.65 1222.71 27.67 o 1 1 3 3077.85 2725.56 88.28 o 2 1 3 46.41 46.68 0.75 o 3 1 3 32.01 31.30 0.42 o 4 1 3 12.00 12.08 0.33 o 5 1 3 2.33 2.51 0.14 o 6 1 3 4.46 5.41 0.23 o -5 2 3 0.02 0.22 0.07 o -4 2 3 15.57 13.72 0.39 o -3 2 3 66.14 69.16 1.60 o -2 2 3 27.68 31.13 0.52 o -1 2 3 427.91 465.76 10.53 o 0 2 3 596.67 642.39 14.51 o 1 2 3 145.99 156.48 2.45 o 2 2 3 3.69 2.91 0.06 o 3 2 3 28.37 24.68 0.34 o 4 2 3 26.18 23.67 0.40 o 5 2 3 2.82 2.80 0.14 o 6 2 3 9.58 10.77 0.34 o -5 3 3 4.20 3.94 0.18 o -4 3 3 9.84 9.05 0.29 o -3 3 3 96.06 92.96 1.51 o -2 3 3 100.56 103.57 2.38 o -1 3 3 25.32 28.68 0.69 o 0 3 3 14.95 12.35 0.32 o 1 3 3 146.01 141.70 1.82 o 2 3 3 190.46 188.34 2.42 o 3 3 3 81.80 79.66 1.04 o 4 3 3 13.27 12.80 0.24 o 5 3 3 18.20 17.35 0.46 o 6 3 3 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