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Acta Cryst. (2004). E60, m1337-m1339 [ doi:10.1107/S1600536804021002 ]
Bis(![[mu]](/logos/entities/mu_rmgif.gif)
-N-acetyl-N-phenylglycinato-![[kappa]](/logos/entities/kappa_rmgif.gif)
2O:O')bis[triaqua(1,10-phenanthroline-2N,N')lanthanum(III)] bis(N-acetyl-N-phenylglycinate) dinitrate dihydrate
Key indicators
- Single-crystal X-ray study
- T = 298 K
- Mean
![[sigma]](http://journals.iucr.org/logos/entities/sigma_rmgif.gif)
(C-C) = 0.007 Å
- R factor = 0.032
- wR factor = 0.083
- Data-to-parameter ratio = 12.7
checkCIF/PLATON results
No syntax errors found
Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ .... ?
PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.46 Ratio
PLAT222_ALERT_3_C Large Non-Solvent H Ueq(max)/Ueq(min) ... 3.07 Ratio
PLAT241_ALERT_2_C Check High U(eq) as Compared to Neighbors for C9
PLAT242_ALERT_2_C Check Low U(eq) as Compared to Neighbors for C5
PLAT244_ALERT_4_C Low Solvent U(eq) as Compared to Neighbors for N7
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C5 -C10 1.37 Ang.
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ...... C4
PLAT731_ALERT_1_C Bond Calc 0.89(3), Rep 0.893(10) ...... 3.00 su-Rat
O4 -H1 1.555 1.555
PLAT731_ALERT_1_C Bond Calc 0.90(3), Rep 0.898(10) ...... 3.00 su-Rat
O4 -H2 1.555 1.555
PLAT731_ALERT_1_C Bond Calc 0.90(3), Rep 0.896(10) ...... 3.00 su-Rat
O5 -H4 1.555 1.555
PLAT731_ALERT_1_C Bond Calc 0.90(4), Rep 0.897(10) ...... 4.00 su-Rat
O6 -H5 1.555 1.555
PLAT731_ALERT_1_C Bond Calc 0.90(3), Rep 0.902(10) ...... 3.00 su-Rat
O13 -H15 1.555 1.555
PLAT731_ALERT_1_C Bond Calc 0.91(4), Rep 0.901(10) ...... 4.00 su-Rat
O13 -H16 1.555 1.555
PLAT735_ALERT_1_C D-H Calc 0.89(3), Rep 0.893(10) ...... 3.00 su-Rat
O4 -H1 1.555 1.555
PLAT735_ALERT_1_C D-H Calc 0.90(3), Rep 0.898(10) ...... 3.00 su-Rat
O4 -H2 1.555 1.555
PLAT735_ALERT_1_C D-H Calc 0.90(3), Rep 0.896(10) ...... 3.00 su-Rat
O5 -H4 1.555 1.555
PLAT735_ALERT_1_C D-H Calc 0.90(4), Rep 0.897(10) ...... 4.00 su-Rat
O6 -H5 1.555 1.555
PLAT735_ALERT_1_C D-H Calc 0.90(3), Rep 0.902(10) ...... 3.00 su-Rat
O13 -H15 1.555 1.555
PLAT735_ALERT_1_C D-H Calc 0.91(4), Rep 0.901(10) ...... 4.00 su-Rat
O13 -H16 1.555 1.555
PLAT736_ALERT_1_C H...A Calc 1.72(3), Rep 1.720(11) ...... 2.73 su-Rat
H2 -O7 1.555 1.555
PLAT736_ALERT_1_C H...A Calc 1.88(4), Rep 1.879(17) ...... 2.35 su-Rat
H5 -O11 1.555 2.666
PLAT736_ALERT_1_C H...A Calc 2.01(3), Rep 2.015(12) ...... 2.50 su-Rat
H15 -O12 1.555 2.666
0 ALERT level A = In general: serious problem
0 ALERT level B = Potentially serious problem
23 ALERT level C = Check and explain
0 ALERT level G = General alerts; check
16 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
4 ALERT type 2 Indicator that the structure model may be wrong or deficient
1 ALERT type 3 Indicator that the structure quality may be low
2 ALERT type 4 Improvement, methodology, query or suggestion
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