# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' PK07 SOTON DATA' _shelx_refln_list_code 4 _shelx_F_calc_maximum 165.99 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.7684 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 4.3681 _cell_length_b 19.1969 _cell_length_c 15.0270 _cell_angle_alpha 90.000 _cell_angle_beta 97.570 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3850.94 3483.99 179.89 o 2 0 0 5762.98 5157.42 222.51 o 3 0 0 1570.66 1517.01 96.59 o 4 0 0 4.13 3.77 37.78 o 5 0 0 3.98 23.73 30.17 o 1 1 0 460.58 465.70 19.60 o 2 1 0 3846.11 3430.04 147.74 o 3 1 0 56.74 71.06 14.24 o 4 1 0 265.91 318.17 26.67 o 5 1 0 142.71 141.71 26.30 o 1 2 0 16832.66 15007.22 373.50 o 2 2 0 1508.03 1486.26 43.75 o 3 2 0 533.89 487.77 19.56 o 4 2 0 12.99 49.94 18.62 o 5 2 0 0.08 -1.88 22.44 o 1 3 0 11.78 26.02 3.87 o 2 3 0 142.63 154.04 9.14 o 3 3 0 354.19 318.08 14.36 o 4 3 0 3.15 11.49 12.00 o 5 3 0 18.43 13.68 23.26 o 0 4 0 475.62 499.44 19.81 o 1 4 0 6229.61 6462.03 174.00 o 2 4 0 812.94 757.09 23.25 o 3 4 0 161.29 166.34 12.98 o 4 4 0 58.78 64.33 11.58 o 5 4 0 0.09 19.14 23.48 o 1 5 0 643.49 652.04 19.31 o 2 5 0 591.29 645.11 19.91 o 3 5 0 2.06 27.08 12.18 o 4 5 0 0.46 -2.15 8.93 o 5 5 0 0.11 -25.79 25.79 o 0 6 0 38.02 209.65 27.22 o 1 6 0 1140.38 1246.46 31.78 o 2 6 0 20.67 33.95 6.82 o 3 6 0 3.51 56.46 10.72 o 4 6 0 5.04 0.18 22.48 o 5 6 0 3.89 -30.13 30.13 o 1 7 0 1834.32 1960.55 47.93 o 2 7 0 567.33 587.85 18.83 o 3 7 0 653.28 575.42 30.72 o 4 7 0 88.79 73.27 20.28 o 5 7 0 3.97 49.82 41.48 o 0 8 0 11966.75 12817.52 428.79 o 1 8 0 7729.53 7993.27 203.49 o 2 8 0 2712.06 2729.31 76.86 o 3 8 0 10.64 11.42 9.31 o 4 8 0 33.42 35.64 21.40 o 5 8 0 8.74 26.44 43.03 o 1 9 0 479.67 453.80 14.21 o 2 9 0 650.95 643.01 21.46 o 3 9 0 435.79 394.71 17.50 o 4 9 0 297.57 314.77 39.96 o 5 9 0 57.14 45.02 43.61 o 0 10 0 10228.52 10669.52 310.43 o 1 10 0 4087.30 4169.75 100.24 o 2 10 0 1313.98 1322.67 42.12 o 3 10 0 140.50 123.15 15.60 o 4 10 0 5.24 21.76 24.91 o 5 10 0 1.11 17.55 39.50 o 1 11 0 269.56 240.33 10.92 o 2 11 0 446.21 438.57 21.99 o 3 11 0 11.78 41.21 10.98 o 4 11 0 339.28 350.96 38.92 o 5 11 0 39.07 40.04 39.18 o 0 12 0 2939.87 2947.25 103.44 o 1 12 0 3225.86 3308.00 85.29 o 2 12 0 1623.39 1576.40 50.45 o 3 12 0 524.38 516.35 23.49 o 4 12 0 21.57 53.35 33.21 o 1 13 0 23.60 34.06 9.20 o 2 13 0 157.34 99.57 22.72 o 3 13 0 38.35 38.94 18.80 o 4 13 0 62.46 85.67 31.42 o 0 14 0 3.35 -0.38 16.02 o 1 14 0 906.11 865.07 26.86 o 2 14 0 657.26 650.09 42.98 o 3 14 0 1.90 20.68 25.19 o 4 14 0 30.39 21.75 29.86 o 1 15 0 50.89 23.48 12.54 o 2 15 0 1251.06 1321.68 49.50 o 3 15 0 2.64 -4.29 81.39 o 4 15 0 0.34 6.62 23.94 o 0 16 0 1194.49 1212.07 64.99 o 1 16 0 15.66 32.03 14.18 o 2 16 0 1.12 -4.96 17.32 o 3 16 0 28.92 28.31 37.83 o 4 16 0 15.28 20.16 34.94 o 1 17 0 315.02 346.26 22.93 o 2 17 0 196.63 196.47 27.42 o 3 17 0 167.32 229.77 43.13 o 4 17 0 95.38 84.88 42.59 o 0 18 0 250.26 252.98 40.89 o 1 18 0 558.68 515.30 28.75 o 2 18 0 142.98 120.01 28.23 o 3 18 0 17.13 8.37 43.83 o 1 19 0 25.12 -0.90 19.51 o 2 19 0 173.50 180.34 31.82 o 3 19 0 183.49 198.97 39.56 o 0 20 0 288.29 349.34 49.81 o 1 20 0 493.57 461.20 34.92 o 2 20 0 387.34 388.47 45.26 o 3 20 0 81.53 72.80 46.55 o 1 21 0 9.71 16.65 25.61 o 2 21 0 49.70 131.84 55.26 o 3 21 0 57.82 48.66 111.16 o 0 22 0 301.83 292.68 50.61 o 1 22 0 62.31 34.82 56.18 o 2 22 0 29.10 85.13 50.73 o 1 23 0 48.77 71.45 47.04 o 2 23 0 2.16 21.72 51.01 o 0 24 0 39.16 69.52 56.10 o 1 24 0 6.13 56.42 43.76 o -5 1 1 10.70 73.24 38.75 o -4 1 1 0.06 3.30 17.61 o -3 1 1 61.19 100.61 19.77 o -2 1 1 128.91 140.42 13.63 o -1 1 1 254.44 297.08 11.81 o 1 1 1 32.15 40.68 3.49 o 2 1 1 103.48 110.94 9.08 o 3 1 1 411.43 379.07 26.36 o 4 1 1 3.90 41.76 17.72 o 5 1 1 0.92 17.39 22.73 o -5 2 1 32.20 6.21 22.49 o -4 2 1 17.45 55.62 27.68 o -3 2 1 1356.79 1311.65 41.69 o -2 2 1 1432.14 1385.94 44.11 o -1 2 1 463.00 416.33 19.83 o 1 2 1 646.67 660.57 20.42 o 2 2 1 208.54 193.90 12.34 o 3 2 1 325.82 339.57 15.84 o 4 2 1 214.88 231.05 25.90 o 5 2 1 7.45 26.58 21.10 o -5 3 1 1.41 3.48 24.08 o -4 3 1 3.75 9.54 11.03 o -3 3 1 553.31 553.22 21.84 o -2 3 1 1000.10 955.21 25.94 o -1 3 1 26787.42 24873.60 577.29 o 0 3 1 4092.91 4193.46 103.62 o 1 3 1 2239.75 1975.85 55.85 o 2 3 1 8179.05 7819.01 279.79 o 3 3 1 606.65 598.90 28.75 o 4 3 1 51.95 60.43 25.89 o 5 3 1 7.20 86.80 50.80 o -5 4 1 59.16 35.99 43.12 o -4 4 1 506.18 622.09 23.81 o -3 4 1 1296.10 1197.79 39.14 o -2 4 1 867.10 795.91 26.03 o -1 4 1 2576.90 2708.06 70.17 o 0 4 1 294.60 340.00 9.38 o 1 4 1 1712.55 1681.87 42.07 o 2 4 1 578.08 568.62 14.99 o 3 4 1 975.08 886.04 30.36 o 4 4 1 578.33 639.63 26.23 o 5 4 1 223.81 274.08 46.62 o -5 5 1 8.76 -9.98 26.54 o -4 5 1 1.60 30.98 17.65 o -3 5 1 507.59 452.56 20.80 o -2 5 1 2806.30 2698.51 73.37 o -1 5 1 6591.48 6590.38 147.26 o 0 5 1 23153.12 23455.95 555.21 o 1 5 1 8948.52 8819.91 214.48 o 2 5 1 3741.50 3642.29 91.33 o 3 5 1 668.68 602.79 21.71 o 4 5 1 135.86 135.45 14.50 o 5 5 1 33.71 -10.81 24.13 o -5 6 1 33.58 39.86 30.87 o -4 6 1 424.20 349.88 22.07 o -3 6 1 952.56 876.55 28.55 o -2 6 1 653.03 613.76 19.39 o -1 6 1 195.04 209.55 7.55 o 0 6 1 90.30 110.82 6.91 o 1 6 1 636.24 631.16 16.05 o 2 6 1 370.25 357.26 19.90 o 3 6 1 344.25 312.84 17.17 o 4 6 1 304.05 254.01 18.95 o 5 6 1 129.40 169.97 36.38 o -5 7 1 0.05 -8.44 19.63 o -4 7 1 2.38 36.87 19.57 o -3 7 1 300.58 302.31 18.89 o -2 7 1 1739.38 1668.97 51.38 o -1 7 1 2211.11 2179.95 52.77 o 0 7 1 2952.28 2950.29 67.05 o 1 7 1 4485.07 4312.54 94.91 o 2 7 1 881.46 867.53 26.17 o 3 7 1 779.84 726.94 32.74 o 4 7 1 10.10 55.93 23.39 o 5 7 1 6.29 14.86 33.96 o -5 8 1 35.84 37.95 22.93 o -4 8 1 6.77 39.19 21.40 o -3 8 1 59.88 55.13 8.40 o -2 8 1 52.24 61.48 7.97 o -1 8 1 133.43 146.95 7.53 o 0 8 1 232.40 260.37 9.29 o 1 8 1 270.11 276.40 10.34 o 2 8 1 457.72 425.82 19.73 o 3 8 1 300.24 267.99 12.82 o 4 8 1 85.68 82.39 26.06 o 5 8 1 8.01 96.56 30.60 o -5 9 1 8.24 -20.02 30.92 o -4 9 1 35.28 36.41 21.46 o -3 9 1 115.03 91.30 10.68 o -2 9 1 32.43 38.68 7.63 o -1 9 1 1461.84 1527.13 38.49 o 0 9 1 967.54 1004.38 23.97 o 1 9 1 1138.71 1174.15 29.91 o 2 9 1 787.13 849.15 26.37 o 3 9 1 16.35 25.90 7.92 o 4 9 1 29.52 24.36 23.71 o 5 9 1 1.39 -16.56 55.92 o -5 10 1 3.93 -3.61 31.81 o -4 10 1 3.12 37.85 23.94 o -3 10 1 373.51 356.02 21.47 o -2 10 1 120.55 110.94 10.98 o -1 10 1 43.25 35.40 7.64 o 0 10 1 194.99 263.62 11.60 o 1 10 1 13.54 20.09 7.94 o 2 10 1 104.95 108.27 14.31 o 3 10 1 3.14 10.29 10.49 o 4 10 1 3.18 38.24 24.39 o 5 10 1 1.52 -31.54 31.54 o -5 11 1 4.50 -8.53 32.23 o -4 11 1 11.54 68.56 27.02 o -3 11 1 346.78 272.58 16.11 o -2 11 1 129.24 138.82 10.69 o -1 11 1 1616.75 1778.54 47.21 o 0 11 1 207.64 182.83 10.38 o 1 11 1 255.17 199.25 12.05 o 2 11 1 245.65 276.37 14.55 o 3 11 1 368.42 371.82 17.53 o 4 11 1 21.56 17.00 20.40 o 5 11 1 5.42 25.54 62.57 o -4 12 1 155.03 188.92 30.16 o -3 12 1 844.69 831.85 35.14 o -2 12 1 624.27 580.07 25.44 o -1 12 1 3.55 9.86 8.29 o 0 12 1 1.29 -8.72 8.72 o 1 12 1 242.80 201.91 11.89 o 2 12 1 176.70 155.11 12.87 o 3 12 1 269.40 215.78 15.11 o 4 12 1 148.34 156.14 30.60 o -4 13 1 0.18 5.88 36.32 o -3 13 1 26.73 -1.08 14.99 o -2 13 1 316.43 231.71 15.40 o -1 13 1 2965.25 3017.63 79.73 o 0 13 1 2346.10 2384.55 63.62 o 1 13 1 972.08 956.07 29.40 o 2 13 1 2392.69 2368.74 74.09 o 3 13 1 25.61 39.22 16.23 o 4 13 1 35.05 35.29 25.65 o -4 14 1 280.28 291.38 36.47 o -3 14 1 333.16 282.79 24.71 o -2 14 1 1548.84 1498.49 60.40 o -1 14 1 62.98 39.62 11.55 o 0 14 1 13.20 24.13 9.84 o 1 14 1 49.59 41.01 11.36 o 2 14 1 19.90 32.08 14.77 o 3 14 1 346.33 325.41 24.15 o 4 14 1 96.34 121.71 32.48 o -4 15 1 2.33 10.50 28.20 o -3 15 1 66.79 41.67 22.75 o -2 15 1 1159.87 1126.61 51.14 o -1 15 1 802.05 715.14 28.30 o 0 15 1 2452.57 2558.62 76.81 o 1 15 1 2317.06 2228.33 74.57 o 2 15 1 990.93 1014.58 53.10 o 3 15 1 293.11 299.62 34.37 o 4 15 1 51.81 0.62 40.57 o -4 16 1 84.47 93.57 33.36 o -3 16 1 121.35 154.69 35.35 o -2 16 1 100.86 95.49 17.62 o -1 16 1 604.67 576.38 28.61 o 0 16 1 15.03 35.12 19.22 o 1 16 1 273.61 216.35 28.89 o 2 16 1 266.53 177.32 25.54 o 3 16 1 141.69 80.37 31.70 o 4 16 1 45.51 37.45 35.82 o -4 17 1 14.06 53.22 40.66 o -3 17 1 275.57 290.25 47.07 o -2 17 1 224.37 194.69 23.65 o -1 17 1 496.35 541.56 27.25 o 0 17 1 822.88 790.99 48.93 o 1 17 1 2289.52 2493.58 97.78 o 2 17 1 146.28 128.83 23.36 o 3 17 1 195.14 264.54 39.82 o 4 17 1 46.54 63.01 38.15 o -3 18 1 0.59 -22.56 35.86 o -2 18 1 2.44 50.34 24.12 o -1 18 1 81.85 54.12 22.22 o 0 18 1 44.87 48.43 22.93 o 1 18 1 21.72 7.87 17.91 o 2 18 1 44.04 44.36 22.49 o 3 18 1 2.14 -30.90 30.90 o -3 19 1 8.84 34.49 43.00 o -2 19 1 9.77 14.96 28.14 o -1 19 1 6.21 41.07 20.97 o 0 19 1 214.94 208.63 29.35 o 1 19 1 80.60 42.77 21.84 o 2 19 1 38.26 40.92 27.14 o 3 19 1 5.87 -4.19 37.42 o -3 20 1 42.00 60.36 40.09 o -2 20 1 54.97 140.07 42.85 o -1 20 1 74.94 40.13 27.93 o 0 20 1 8.60 -1.27 27.93 o 1 20 1 2.37 -6.48 25.59 o 2 20 1 45.64 14.32 35.51 o 3 20 1 45.52 18.86 46.96 o -3 21 1 1.43 -29.89 59.35 o -2 21 1 9.78 32.19 32.66 o -1 21 1 22.42 26.26 25.43 o 0 21 1 67.00 76.22 33.28 o 1 21 1 92.68 129.29 31.08 o 2 21 1 2.99 64.55 78.20 o 3 21 1 0.13 47.59 81.34 o -2 22 1 100.71 47.84 51.15 o -1 22 1 52.76 55.81 41.99 o 0 22 1 27.78 85.99 33.64 o 1 22 1 47.22 77.67 65.07 o 2 22 1 14.95 3.36 43.74 o -2 23 1 61.45 67.58 51.88 o -1 23 1 116.34 153.89 44.48 o 0 23 1 335.92 304.62 39.44 o 1 23 1 246.17 288.45 46.87 o 2 23 1 160.87 118.00 63.89 o -1 24 1 36.20 49.22 41.96 o 0 24 1 1.91 54.91 34.54 o 1 24 1 54.17 77.85 43.08 o -5 0 2 8.15 11.93 39.12 o -4 0 2 157.19 160.18 30.88 o -3 0 2 731.91 581.77 74.29 o -2 0 2 2915.02 2614.02 129.47 o -1 0 2 2733.87 2662.37 107.75 o 1 0 2 27502.80 25812.01 1230.72 o 2 0 2 4101.74 3949.87 141.94 o 3 0 2 104.76 220.79 44.33 o 4 0 2 28.61 68.62 33.38 o 5 0 2 5.04 -24.15 33.23 o -5 1 2 67.37 76.17 24.12 o -4 1 2 630.91 650.23 36.92 o -3 1 2 1461.45 1454.58 67.16 o -2 1 2 1880.41 1838.86 54.04 o -1 1 2 4877.05 4885.34 147.22 o 1 1 2 955.93 925.10 26.81 o 2 1 2 1868.24 1749.45 39.69 o 3 1 2 1099.06 1154.72 51.16 o 4 1 2 390.50 452.73 36.17 o 5 1 2 97.14 68.05 31.60 o -5 2 2 0.82 87.83 35.65 o -4 2 2 113.11 88.33 22.83 o -3 2 2 459.85 482.00 22.25 o -2 2 2 1777.65 1683.63 44.88 o -1 2 2 8110.49 7429.08 258.07 o 0 2 2 694.82 767.12 20.16 o 1 2 2 3990.99 3584.89 84.38 o 2 2 2 2727.69 2421.75 56.40 o 3 2 2 260.70 293.39 14.89 o 4 2 2 75.33 127.45 21.00 o 5 2 2 6.66 29.80 21.01 o -5 3 2 52.72 29.19 33.60 o -4 3 2 132.80 145.17 12.49 o -3 3 2 705.94 690.49 32.07 o -2 3 2 645.47 644.54 29.18 o -1 3 2 27554.18 25811.36 721.58 o 0 3 2 0.38 5.12 3.65 o 1 3 2 277.98 308.57 10.34 o 2 3 2 24.76 63.30 6.90 o 3 3 2 911.48 885.98 36.25 o 4 3 2 45.65 61.09 22.19 o 5 3 2 1.60 3.14 36.62 o -5 4 2 0.26 3.50 24.91 o -4 4 2 76.53 106.31 12.23 o -3 4 2 9.87 29.12 12.64 o -2 4 2 1965.58 1918.40 57.45 o -1 4 2 257.19 234.30 12.83 o 0 4 2 24.46 29.00 3.81 o 1 4 2 1992.16 1959.93 43.81 o 2 4 2 341.68 362.28 10.35 o 3 4 2 206.96 206.98 12.16 o 4 4 2 54.60 57.58 10.74 o 5 4 2 0.08 8.65 57.46 o -5 5 2 10.85 21.13 38.74 o -4 5 2 12.09 31.39 14.75 o -3 5 2 144.75 162.30 10.87 o -2 5 2 60.66 66.50 6.72 o -1 5 2 21.30 32.53 5.44 o 0 5 2 2889.76 3047.24 69.25 o 1 5 2 21.33 26.08 4.73 o 2 5 2 445.69 453.81 14.21 o 3 5 2 0.95 19.66 8.10 o 4 5 2 6.25 6.85 18.68 o 5 5 2 0.16 -3.22 28.48 o -5 6 2 20.93 40.01 33.85 o -4 6 2 11.47 40.38 12.46 o -3 6 2 66.06 37.04 7.66 o -2 6 2 11.36 27.53 6.22 o -1 6 2 1090.59 1112.25 30.72 o 0 6 2 420.79 453.68 12.05 o 1 6 2 1521.64 1639.57 38.45 o 2 6 2 504.95 503.11 12.78 o 3 6 2 204.21 190.71 17.86 o 4 6 2 2.64 32.53 17.26 o 5 6 2 3.87 12.57 32.15 o -5 7 2 13.02 44.50 33.11 o -4 7 2 65.53 104.14 27.28 o -3 7 2 411.07 329.81 15.51 o -2 7 2 12.39 30.24 6.50 o -1 7 2 2727.65 2903.96 69.93 o 0 7 2 94.90 96.57 7.97 o 1 7 2 699.99 799.50 20.29 o 2 7 2 1847.49 1872.87 44.41 o 3 7 2 1033.18 1017.51 27.00 o 4 7 2 156.36 112.64 15.90 o 5 7 2 46.02 73.22 27.96 o -5 8 2 6.35 39.48 24.39 o -4 8 2 373.27 385.58 35.42 o -3 8 2 12.58 34.96 8.72 o -2 8 2 468.75 428.89 14.80 o -1 8 2 4348.47 4262.54 110.65 o 0 8 2 3884.28 3735.07 84.20 o 1 8 2 7563.31 7995.93 188.56 o 2 8 2 1638.78 1630.96 39.30 o 3 8 2 710.14 695.07 22.23 o 4 8 2 6.08 21.65 18.71 o 5 8 2 3.20 -25.04 41.87 o -5 9 2 76.22 112.24 25.81 o -4 9 2 370.42 375.05 35.73 o -3 9 2 838.12 837.48 36.12 o -2 9 2 1313.47 1221.01 37.08 o -1 9 2 653.66 631.19 18.57 o 0 9 2 876.19 957.47 24.92 o 1 9 2 240.90 251.45 10.08 o 2 9 2 687.60 677.54 20.79 o 3 9 2 902.41 872.98 31.63 o 4 9 2 150.24 164.56 57.18 o 5 9 2 80.99 3.42 63.27 o -5 10 2 0.26 -25.71 48.20 o -4 10 2 7.68 8.69 22.31 o -3 10 2 770.67 697.43 32.41 o -2 10 2 621.15 566.01 20.54 o -1 10 2 2594.06 2472.71 63.07 o 0 10 2 6293.77 6281.67 149.04 o 1 10 2 3018.16 2957.24 67.98 o 2 10 2 2815.88 2933.91 73.09 o 3 10 2 368.01 368.45 19.69 o 4 10 2 91.56 54.23 24.93 o 5 10 2 3.18 -14.50 43.39 o -5 11 2 48.04 70.73 36.83 o -4 11 2 37.05 70.35 28.10 o -3 11 2 1262.59 1268.29 58.96 o -2 11 2 1259.78 1248.71 45.76 o -1 11 2 466.85 457.85 15.54 o 0 11 2 1799.29 1993.01 45.81 o 1 11 2 52.87 57.45 8.33 o 2 11 2 1052.01 993.68 29.86 o 3 11 2 231.20 246.83 16.68 o 4 11 2 79.49 147.37 37.52 o -4 12 2 9.27 40.78 26.60 o -3 12 2 1007.08 1018.13 48.81 o -2 12 2 817.42 794.09 33.79 o -1 12 2 1675.86 1656.81 42.96 o 0 12 2 1896.32 1748.66 43.64 o 1 12 2 664.23 610.78 20.00 o 2 12 2 416.90 382.51 17.09 o 3 12 2 511.89 502.01 27.64 o 4 12 2 74.65 87.97 39.56 o -4 13 2 3.15 22.35 30.10 o -3 13 2 92.89 111.16 18.54 o -2 13 2 656.55 621.14 30.24 o -1 13 2 11.15 24.96 8.63 o 0 13 2 72.19 59.10 9.78 o 1 13 2 31.64 30.79 9.41 o 2 13 2 176.20 156.84 14.73 o 3 13 2 62.62 79.63 17.41 o 4 13 2 25.88 33.22 29.76 o -4 14 2 57.81 63.33 50.27 o -3 14 2 37.82 35.57 17.69 o -2 14 2 340.68 337.74 26.22 o -1 14 2 86.65 88.79 10.75 o 0 14 2 155.59 160.71 12.91 o 1 14 2 1.82 14.34 12.19 o 2 14 2 34.00 49.25 13.31 o 3 14 2 134.39 102.13 23.17 o 4 14 2 42.15 29.32 39.59 o -4 15 2 3.96 13.54 31.53 o -3 15 2 0.57 11.50 20.65 o -2 15 2 107.34 66.82 19.50 o -1 15 2 6.40 7.65 12.36 o 0 15 2 0.50 7.04 12.53 o 1 15 2 203.67 186.88 20.75 o 2 15 2 453.57 446.93 21.88 o 3 15 2 106.10 121.76 31.65 o 4 15 2 17.24 43.21 38.54 o -4 16 2 5.19 36.42 32.61 o -3 16 2 1.05 -16.57 33.09 o -2 16 2 52.38 43.16 20.38 o -1 16 2 114.86 124.23 15.44 o 0 16 2 130.35 75.39 21.33 o 1 16 2 1592.04 1477.82 63.10 o 2 16 2 39.85 61.55 10.05 o 3 16 2 12.45 59.40 39.12 o 4 16 2 2.03 4.42 38.73 o -4 17 2 86.51 47.97 34.60 o -3 17 2 130.37 168.11 37.81 o -2 17 2 86.52 154.07 24.25 o -1 17 2 80.43 60.74 15.89 o 0 17 2 1.97 16.22 23.95 o 1 17 2 131.30 118.35 21.45 o 2 17 2 69.45 73.62 23.19 o 3 17 2 225.69 136.16 33.73 o -3 18 2 0.73 70.23 39.11 o -2 18 2 148.12 152.27 28.36 o -1 18 2 381.00 348.34 24.25 o 0 18 2 989.45 989.93 54.46 o 1 18 2 1482.41 1444.50 72.95 o 2 18 2 421.27 428.47 44.29 o 3 18 2 46.71 -25.47 31.97 o -3 19 2 49.45 101.50 63.86 o -2 19 2 202.45 213.52 35.56 o -1 19 2 261.05 265.37 25.77 o 0 19 2 311.21 361.36 32.80 o 1 19 2 76.02 61.63 27.27 o 2 19 2 8.85 44.17 24.47 o 3 19 2 412.94 473.00 57.69 o -3 20 2 39.66 104.09 46.20 o -2 20 2 387.82 409.70 43.22 o -1 20 2 523.32 495.00 39.47 o 0 20 2 593.16 595.48 48.39 o 1 20 2 530.17 533.17 76.13 o 2 20 2 209.32 232.27 36.24 o 3 20 2 247.30 331.33 52.35 o -3 21 2 64.78 108.31 51.35 o -2 21 2 79.39 96.09 62.82 o -1 21 2 18.59 58.69 26.82 o 0 21 2 28.47 13.14 28.43 o 1 21 2 54.72 91.70 28.31 o 2 21 2 167.78 222.56 63.23 o -2 22 2 159.61 128.34 44.90 o -1 22 2 139.55 133.92 35.27 o 0 22 2 141.49 296.08 40.89 o 1 22 2 159.71 179.51 45.37 o 2 22 2 114.35 147.20 94.65 o -2 23 2 36.60 102.25 50.62 o -1 23 2 21.35 7.65 39.50 o 0 23 2 0.59 29.03 35.86 o 1 23 2 6.91 12.40 47.53 o 2 23 2 0.32 96.11 42.51 o -1 24 2 1.08 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