Acta Cryst. (2004). E60, m1439-m1441  [ doi:10.1107/S1600536804022214 ]

Dichloro({N-[2-(diphenylphosphino-P)benzyl]benzylamino}diphenylphosphine-P)palladium(II) toluene solvate

M. Pretorius, D. B. G. Williams, A. Roodt and A. Muller

Online 18 September 2004

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• R factor = 0.041
• wR factor = 0.088
• Data-to-parameter ratio = 21.3

checkCIF/PLATON results

No syntax errors found






Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.00 Ratio 
PLAT230_ALERT_2_C Hirshfeld Test Diff for    C50    -   C64     ..       6.40 su    
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Pd     -   Cl2     ..       6.08 su    
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Pd     -   P2      ..       5.22 su    
PLAT244_ALERT_4_C Low  Solvent U(eq) as Compared to Neighbors  for        C02     
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist.   C02    -C03           1.37 Ang.  
PLAT720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........         21       

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   7 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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