Acta Cryst. (2004). E60, m1459-m1461  [ doi:10.1107/S1600536804022779 ]

Bis(2,2'-bipyridine)-1²N:N';3²N:N'-tris(--methylacrylato-1:2²O:O')tris(--methylacrylato-2:3²O:O')(nitrato-2²O:O')dizinc(II)praseodymium(III)

Y. Zhu, W. Lu and F. Chen

Online 25 September 2004

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.007 Å
• R factor = 0.029
• wR factor = 0.090
• Data-to-parameter ratio = 14.2

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT241_ALERT_2_B Check High   U(eq) as Compared to Neighbors  for         O7     
PLAT242_ALERT_2_B Check Low    U(eq) as Compared to Neighbors  for         Pr     
PLAT413_ALERT_2_B Short Inter XH3 .. XHn     H24C   ..  H74B    ..       1.95 Ang.  

Alert level C
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.98       
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.06 Ratio 
PLAT230_ALERT_2_C Hirshfeld Test Diff for    O2     -   N3      ..       6.14 su    
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Pr     -   O2      ..       5.72 su    
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for         O3     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for         O4     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for         O5     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for         O6     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for         O9     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for        O10     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for        O11     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for        O15     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors  for        C22     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors  for        C32     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors  for        C42     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors  for        C51     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors  for        C52     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors  for        C62     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors  for        C72     
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......        C24     
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......        C34     
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......        C44     
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......        C54     
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......        C64     
PLAT380_ALERT_4_C Incorrectly Oriented X(sp2)-Methyl Moiety ......        C74     

   0 ALERT level A = In general: serious problem
   3 ALERT level B = Potentially serious problem
  25 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  21 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   7 ALERT type 4 Improvement, methodology, query or suggestion

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