# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_ci6465 _shelx_title ' CI6465 in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 244.98 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.8405 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 10.0461 _cell_length_b 21.7350 _cell_length_c 7.1893 _cell_angle_alpha 90.000 _cell_angle_beta 131.879 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 32648.15 40277.61 250.82 o 4 0 0 14452.35 15119.97 110.19 o 6 0 0 3099.34 2718.07 37.46 o 1 1 0 12679.43 13852.99 916.23 o 3 1 0 27987.99 32550.28 548.67 o 5 1 0 3529.36 3314.66 152.62 o 7 1 0 1808.61 1861.21 57.34 o 0 2 0 10041.57 7586.32 985.49 o 2 2 0 5622.46 5763.52 110.13 o 4 2 0 14287.26 16111.09 119.69 o 6 2 0 3480.47 3542.44 81.39 o 8 2 0 1272.23 1279.73 23.56 o 1 3 0 34202.51 34891.75 665.97 o 3 3 0 10584.03 11037.22 221.28 o 5 3 0 3641.88 3633.19 122.99 o 7 3 0 2185.75 2092.10 77.54 o 0 4 0 6697.25 5527.81 85.07 o 2 4 0 10400.82 10633.41 91.25 o 4 4 0 13047.63 13938.01 117.50 o 6 4 0 1380.62 1376.86 28.29 o 8 4 0 630.07 537.61 15.76 o 1 5 0 23440.91 24160.50 223.12 o 3 5 0 19315.13 20729.49 100.42 o 5 5 0 8508.60 9300.23 48.48 o 7 5 0 2984.20 2924.64 60.89 o 0 6 0 48774.63 37416.78 807.58 o 2 6 0 6986.00 6953.86 80.48 o 4 6 0 9515.48 10114.02 124.25 o 6 6 0 2981.13 3019.32 182.11 o 8 6 0 835.85 745.40 20.40 o 1 7 0 29892.88 29862.37 166.46 o 3 7 0 15676.20 16504.33 172.10 o 5 7 0 2657.37 2705.15 30.21 o 7 7 0 1034.11 1011.34 20.93 o 0 8 0 32716.22 27717.51 486.52 o 2 8 0 19124.80 20318.06 231.65 o 4 8 0 6149.05 6370.88 145.94 o 6 8 0 1984.20 1986.90 59.62 o 8 8 0 785.31 768.62 49.63 o 1 9 0 20911.30 19334.37 462.79 o 3 9 0 9327.09 9684.28 262.26 o 5 9 0 3015.88 2881.88 32.26 o 7 9 0 1476.34 1405.55 54.99 o 0 10 0 11953.36 10752.86 144.50 o 2 10 0 6334.55 6418.65 116.44 o 4 10 0 6221.95 6422.07 98.23 o 6 10 0 1455.18 1454.42 24.94 o 8 10 0 615.99 567.91 35.93 o 1 11 0 1551.58 1323.42 23.59 o 3 11 0 6075.76 6250.68 221.28 o 5 11 0 3776.87 4036.61 164.71 o 7 11 0 1078.88 1018.70 45.49 o 0 12 0 19485.53 18355.24 535.38 o 2 12 0 10097.82 10229.41 81.79 o 4 12 0 4435.38 4376.22 137.27 o 6 12 0 1916.10 1890.47 29.64 o 1 13 0 8079.05 7839.75 78.22 o 3 13 0 6328.70 6304.87 366.03 o 5 13 0 2318.90 2417.58 98.54 o 7 13 0 604.69 578.35 20.19 o 0 14 0 3353.90 3195.13 28.64 o 2 14 0 9288.48 9408.61 174.74 o 4 14 0 4105.83 4213.92 168.11 o 6 14 0 3049.83 3280.32 126.47 o 1 15 0 9958.21 9702.02 43.21 o 3 15 0 1984.02 1941.06 75.96 o 5 15 0 995.94 969.97 35.99 o 7 15 0 358.11 353.46 30.36 o 0 16 0 4021.03 3870.88 34.27 o 2 16 0 4679.30 4459.30 144.67 o 4 16 0 1048.81 1053.43 46.33 o 6 16 0 85.44 83.12 8.63 o 1 17 0 5604.65 5526.01 168.12 o 3 17 0 2521.09 2432.36 78.41 o 5 17 0 2696.96 2610.78 75.87 o 0 18 0 1114.84 1099.53 18.12 o 2 18 0 2377.47 2235.48 84.48 o 4 18 0 1445.54 1399.33 44.77 o 6 18 0 1052.04 1031.04 87.76 o 1 19 0 3294.23 3000.71 53.12 o 3 19 0 3295.57 3331.56 137.33 o 5 19 0 1153.18 1186.88 58.55 o 0 20 0 2337.79 2350.82 42.30 o 2 20 0 2287.47 2146.12 55.81 o 4 20 0 729.79 693.55 46.47 o 1 21 0 446.94 459.58 22.42 o 3 21 0 903.79 853.90 40.64 o 5 21 0 619.61 663.28 35.76 o 0 22 0 2182.35 2196.99 43.47 o 2 22 0 2338.51 2299.63 94.38 o 4 22 0 712.26 700.56 48.49 o 1 23 0 1901.88 1933.97 38.84 o 3 23 0 374.32 357.58 13.85 o 0 24 0 439.70 497.78 21.70 o 2 24 0 1411.19 1440.49 89.09 o 1 25 0 997.37 1017.78 32.31 o -9 1 1 8.20 5.01 5.29 o -7 1 1 6.70 8.94 3.07 o -5 1 1 2.24 2.38 2.10 o -3 1 1 339.93 373.61 5.24 o -1 1 1 3964.15 3827.75 41.35 o 1 1 1 51054.95 62665.69 806.50 o 3 1 1 2195.42 2426.35 17.53 o 5 1 1 0.11 -2.80 2.89 o 7 1 1 0.10 8.92 7.63 o -8 2 1 15.81 27.57 4.89 o -6 2 1 476.88 430.07 9.95 o -4 2 1 1288.33 1133.74 13.23 o -2 2 1 8752.51 7901.87 182.38 o 0 2 1 759.38 856.20 7.62 o 2 2 1 1786.29 1896.24 54.04 o 4 2 1 9.39 -2.84 2.84 o 6 2 1 0.68 0.66 3.61 o -9 3 1 0.01 -1.04 9.53 o -7 3 1 212.54 205.57 8.61 o -5 3 1 650.68 674.26 15.61 o -3 3 1 64.16 74.84 3.02 o -1 3 1 76.39 79.86 1.82 o 1 3 1 1167.26 1195.83 8.69 o 3 3 1 2.45 1.54 2.60 o 5 3 1 4.18 -1.89 2.78 o 7 3 1 46.56 39.11 6.45 o -8 4 1 153.60 145.42 9.21 o -6 4 1 423.72 413.07 36.48 o -4 4 1 132.73 140.84 7.02 o -2 4 1 6443.57 6149.65 130.88 o 0 4 1 752.31 779.97 6.23 o 2 4 1 389.89 371.03 6.77 o 4 4 1 6.79 8.70 3.07 o 6 4 1 152.62 141.49 8.27 o -9 5 1 4.65 -1.54 4.50 o -7 5 1 3.96 1.41 5.04 o -5 5 1 511.29 530.50 10.33 o -3 5 1 212.66 203.60 3.94 o -1 5 1 53.97 47.81 1.56 o 1 5 1 3728.36 3784.66 39.88 o 3 5 1 2.16 10.74 4.23 o 5 5 1 3.87 4.98 3.32 o 7 5 1 18.59 12.08 5.87 o -8 6 1 49.77 28.84 9.39 o -6 6 1 636.49 694.72 13.77 o -4 6 1 2732.97 2852.09 54.38 o -2 6 1 2562.56 2707.55 29.34 o 0 6 1 123.34 127.49 5.37 o 2 6 1 468.28 482.22 9.21 o 4 6 1 138.26 149.20 5.63 o 6 6 1 46.17 35.68 6.74 o -9 7 1 44.91 52.47 7.96 o -7 7 1 42.23 49.07 9.86 o -5 7 1 265.33 258.11 6.61 o -3 7 1 1925.10 2021.47 13.40 o -1 7 1 3635.62 3604.03 27.44 o 1 7 1 197.82 210.28 6.25 o 3 7 1 26.18 24.04 2.49 o 5 7 1 27.53 28.09 12.97 o 7 7 1 15.89 12.49 5.61 o -8 8 1 42.76 31.08 6.25 o -6 8 1 78.07 81.91 7.22 o -4 8 1 246.30 263.16 5.33 o -2 8 1 159.73 209.89 4.01 o 0 8 1 1567.43 1605.41 28.07 o 2 8 1 56.65 137.73 57.04 o 4 8 1 312.26 293.47 8.06 o 6 8 1 37.60 29.04 5.94 o -9 9 1 5.74 13.18 18.56 o -7 9 1 11.59 14.59 5.36 o -5 9 1 340.33 322.74 17.77 o -3 9 1 18.21 17.85 2.15 o -1 9 1 1577.52 1546.76 34.34 o 1 9 1 560.76 589.18 16.95 o 3 9 1 12.84 10.49 3.29 o 5 9 1 13.65 8.57 4.76 o 7 9 1 18.31 15.06 6.03 o -8 10 1 3.52 1.12 5.49 o -6 10 1 44.02 46.43 12.48 o -4 10 1 74.14 80.88 3.69 o -2 10 1 204.47 177.41 8.23 o 0 10 1 7017.92 7256.43 169.41 o 2 10 1 308.70 356.80 15.53 o 4 10 1 172.22 148.23 12.36 o 6 10 1 33.01 31.05 6.17 o -7 11 1 37.90 20.19 6.04 o -5 11 1 400.38 382.44 14.34 o -3 11 1 36.58 40.77 2.96 o -1 11 1 785.12 898.19 25.46 o 1 11 1 522.88 574.22 26.67 o 3 11 1 92.30 103.80 5.15 o 5 11 1 0.51 -1.92 4.76 o 7 11 1 0.24 0.78 5.50 o -8 12 1 1.20 -2.39 10.49 o -6 12 1 2.72 -0.65 3.51 o -4 12 1 46.53 53.25 4.14 o -2 12 1 104.77 119.94 4.00 o 0 12 1 153.20 194.70 13.17 o 2 12 1 1059.03 1079.66 17.55 o 4 12 1 6.29 9.16 4.81 o 6 12 1 0.00 -4.78 4.78 o -7 13 1 0.08 1.80 5.54 o -5 13 1 110.60 129.12 6.16 o -3 13 1 55.71 53.21 7.13 o -1 13 1 679.32 620.07 27.54 o 1 13 1 878.40 988.79 13.93 o 3 13 1 107.44 136.14 24.07 o 5 13 1 23.43 42.31 23.72 o -8 14 1 13.91 7.42 5.89 o -6 14 1 27.19 26.82 4.70 o -4 14 1 331.71 327.34 14.94 o -2 14 1 2.23 9.19 5.82 o 0 14 1 157.77 152.65 4.37 o 2 14 1 524.63 529.65 23.00 o 4 14 1 294.95 294.68 25.47 o 6 14 1 0.83 -1.14 5.44 o -7 15 1 473.44 513.89 30.48 o -5 15 1 1341.73 1401.33 65.53 o -3 15 1 425.88 422.47 16.85 o -1 15 1 171.87 190.97 14.65 o 1 15 1 48.34 43.43 3.97 o 3 15 1 15.58 14.82 5.25 o 5 15 1 85.10 94.28 10.91 o -6 16 1 280.49 305.74 10.19 o -4 16 1 191.32 181.66 9.44 o -2 16 1 710.77 688.73 23.76 o 0 16 1 218.58 202.16 8.02 o 2 16 1 55.02 57.23 4.72 o 4 16 1 2.27 1.36 5.08 o -7 17 1 58.60 48.18 7.42 o -5 17 1 1021.82 1064.43 76.06 o -3 17 1 0.91 10.67 3.97 o -1 17 1 130.58 126.43 4.78 o 1 17 1 74.93 70.34 7.78 o 3 17 1 12.92 12.50 5.60 o 5 17 1 25.84 19.98 6.27 o -6 18 1 89.57 86.90 6.80 o -4 18 1 88.57 80.18 5.84 o -2 18 1 232.00 221.72 9.36 o 0 18 1 189.11 222.76 11.94 o 2 18 1 0.07 -0.67 4.87 o 4 18 1 5.93 11.84 5.86 o -5 19 1 84.78 92.23 6.54 o -3 19 1 52.75 41.75 4.83 o -1 19 1 29.11 24.43 4.14 o 1 19 1 209.63 207.34 8.00 o 3 19 1 9.91 7.49 5.60 o 5 19 1 1.63 7.94 6.32 o -6 20 1 0.05 0.95 5.86 o -4 20 1 132.82 127.89 10.38 o -2 20 1 167.89 162.65 8.59 o 0 20 1 341.33 306.83 9.09 o 2 20 1 199.41 181.16 10.19 o 4 20 1 130.09 168.20 10.82 o -5 21 1 45.28 48.11 5.44 o -3 21 1 54.05 54.04 8.03 o -1 21 1 150.58 129.17 8.85 o 1 21 1 8.38 8.44 5.56 o 3 21 1 12.17 6.68 5.44 o -4 22 1 4.45 2.72 4.08 o -2 22 1 39.91 35.56 6.09 o 0 22 1 171.16 140.19 7.09 o 2 22 1 150.96 153.92 10.02 o -3 23 1 2.45 4.89 5.18 o -1 23 1 1.05 1.02 4.73 o 1 23 1 100.71 95.06 8.56 o 3 23 1 12.81 4.98 5.64 o -4 24 1 27.85 18.29 4.96 o -2 24 1 14.88 10.82 5.43 o 0 24 1 1.55 8.74 7.87 o 2 24 1 0.37 -4.51 5.68 o -1 25 1 62.72 56.86 6.90 o 1 25 1 1.34 6.34 6.26 o -10 0 2 79.77 75.14 11.61 o -8 0 2 2673.21 2776.32 45.60 o -6 0 2 8491.95 8816.21 79.59 o -4 0 2 7384.92 7130.58 60.08 o -2 0 2 21650.25 20731.53 83.32 o 0 0 2 592.22 526.83 25.29 o 2 0 2 101.74 91.22 7.62 o 4 0 2 138.06 149.27 7.06 o 6 0 2 646.33 618.69 23.11 o -9 1 2 2377.82 2575.77 87.35 o -7 1 2 3191.73 3229.47 29.10 o -5 1 2 29030.46 29575.42 408.44 o -3 1 2 26649.65 22732.28 484.64 o -1 1 2 13125.67 13763.02 107.58 o 1 1 2 11458.91 12582.38 57.54 o 3 1 2 6194.49 6670.44 66.25 o 5 1 2 1403.07 1459.80 31.58 o -10 2 2 1378.82 1475.57 65.19 o -8 2 2 3036.28 3265.18 42.76 o -6 2 2 6353.51 6282.35 67.84 o -4 2 2 6202.76 5559.97 81.61 o -2 2 2 33393.89 31071.33 206.37 o 0 2 2 15641.39 16390.49 187.46 o 2 2 2 18022.30 20911.13 142.77 o 4 2 2 2885.74 2823.21 52.18 o 6 2 2 752.77 662.14 22.85 o -9 3 2 1833.05 1982.53 24.06 o -7 3 2 4881.35 5135.97 65.48 o -5 3 2 18076.43 18540.26 547.41 o -3 3 2 4219.32 3877.29 84.66 o -1 3 2 60013.85 60903.45 353.21 o 1 3 2 7102.05 7710.76 81.82 o 3 3 2 3016.55 2946.46 61.94 o 5 3 2 1229.13 1222.77 20.60 o -10 4 2 848.52 894.20 22.24 o -8 4 2 2759.63 2909.58 27.49 o -6 4 2 8653.48 8986.17 257.75 o -4 4 2 29030.34 27765.24 275.32 o -2 4 2 28861.90 26837.09 226.48 o 0 4 2 11646.51 11590.42 165.03 o 2 4 2 13049.59 14245.34 130.10 o 4 4 2 1673.38 1477.06 17.32 o 6 4 2 804.02 821.58 26.94 o -9 5 2 1719.62 1837.33 23.59 o -7 5 2 1902.54 1957.07 62.61 o -5 5 2 1709.74 1389.64 16.14 o -3 5 2 2966.03 2481.08 26.14 o -1 5 2 21817.54 21902.48 195.96 o 1 5 2 8510.85 9147.30 64.62 o 3 5 2 3399.42 3405.42 75.70 o 5 5 2 769.64 722.42 15.31 o -10 6 2 497.47 513.43 22.10 o -8 6 2 3168.55 3369.58 84.57 o -6 6 2 6664.63 6625.77 64.54 o -4 6 2 15845.42 14870.38 65.69 o -2 6 2 16876.56 16105.97 69.58 o 0 6 2 9645.34 9732.15 88.62 o 2 6 2 6805.73 7401.17 212.16 o 4 6 2 1552.13 1555.10 21.00 o 6 6 2 720.45 672.22 25.84 o -9 7 2 1456.97 1527.81 22.90 o -7 7 2 2837.32 2936.43 122.01 o -5 7 2 18341.53 19387.51 659.05 o -3 7 2 14051.26 13473.57 206.05 o -1 7 2 9402.12 9313.38 81.65 o 1 7 2 5505.06 5849.17 56.86 o 3 7 2 3213.70 3392.86 143.11 o 5 7 2 903.22 857.22 66.38 o -10 8 2 616.65 616.23 16.33 o -8 8 2 1835.22 1881.55 98.11 o -6 8 2 7343.75 7444.36 185.55 o -4 8 2 9379.89 8753.70 142.94 o -2 8 2 21969.30 21037.49 109.33 o 0 8 2 3818.59 3978.52 64.21 o 2 8 2 3837.25 3937.31 122.42 o 4 8 2 1442.64 1542.17 159.11 o 6 8 2 454.83 482.88 15.86 o -9 9 2 998.72 1026.52 19.11 o -7 9 2 3624.63 3563.77 113.89 o -5 9 2 11406.08 11554.02 189.30 o -3 9 2 10651.96 10121.96 81.29 o -1 9 2 11424.38 11234.68 113.10 o 1 9 2 3682.72 3505.78 106.98 o 3 9 2 1852.99 1853.40 123.52 o 5 9 2 936.51 958.35 44.46 o -8 10 2 1800.29 1617.02 220.45 o -6 10 2 4525.45 4783.85 113.25 o -4 10 2 6350.19 6350.99 158.02 o -2 10 2 9010.33 8786.30 108.54 o 0 10 2 11652.39 11984.68 240.93 o 2 10 2 7156.20 7651.29 96.50 o 4 10 2 1435.50 1343.01 192.16 o 6 10 2 399.08 378.51 32.28 o -9 11 2 1232.75 1284.52 34.50 o -7 11 2 2758.22 2808.39 94.93 o -5 11 2 3547.48 3569.93 119.54 o -3 11 2 11990.89 11143.27 106.59 o -1 11 2 10097.32 9586.36 122.73 o 1 11 2 9657.64 9730.43 208.68 o 3 11 2 3417.41 3304.41 268.49 o 5 11 2 971.48 942.01 99.27 o -8 12 2 1477.71 1571.43 120.18 o -6 12 2 2602.37 2625.81 111.55 o -4 12 2 3923.51 3883.70 63.26 o -2 12 2 7363.93 7160.59 73.93 o 0 12 2 5922.29 5889.12 60.08 o 2 12 2 1240.66 1211.40 18.11 o 4 12 2 624.49 534.39 46.28 o -9 13 2 727.35 725.14 29.72 o -7 13 2 1571.33 1524.41 66.08 o -5 13 2 5749.91 5973.22 184.93 o -3 13 2 5362.51 5357.50 138.27 o -1 13 2 5235.21 5316.54 87.72 o 1 13 2 4489.48 4740.68 116.30 o 3 13 2 1750.16 1704.39 135.96 o 5 13 2 307.45 300.12 21.98 o -8 14 2 699.04 712.95 53.07 o -6 14 2 1051.35 1011.81 43.54 o -4 14 2 1920.08 1920.86 74.96 o -2 14 2 3490.66 3342.03 69.33 o 0 14 2 3094.50 3098.57 32.55 o 2 14 2 1887.11 2073.02 95.44 o 4 14 2 1171.82 1099.13 112.49 o -7 15 2 2636.43 2665.34 109.27 o -5 15 2 3798.59 3919.46 174.44 o -3 15 2 6783.78 6480.95 179.59 o -1 15 2 6315.57 6655.32 112.97 o 1 15 2 2190.71 2215.42 100.83 o 3 15 2 1054.85 1127.31 122.26 o 5 15 2 583.57 590.66 61.61 o -8 16 2 1093.96 1009.41 40.81 o -6 16 2 5044.72 5101.38 270.03 o -4 16 2 14557.70 14648.16 498.97 o -2 16 2 4241.47 4095.07 102.88 o 0 16 2 3015.83 3059.31 55.51 o 2 16 2 1790.18 1873.80 75.85 o 4 16 2 789.99 799.37 63.88 o -7 17 2 1271.84 1282.93 87.65 o -5 17 2 238.46 203.52 8.60 o -3 17 2 2068.16 1957.62 107.14 o -1 17 2 2159.57 2184.78 46.12 o 1 17 2 1779.93 1838.91 107.18 o 3 17 2 735.54 682.13 62.44 o -6 18 2 914.94 885.50 68.48 o -4 18 2 1389.77 1302.86 37.36 o -2 18 2 2375.26 2486.62 104.83 o 0 18 2 3827.15 3880.50 41.72 o 2 18 2 1694.60 1714.11 85.57 o 4 18 2 718.14 715.04 86.50 o -7 19 2 659.30 640.89 29.04 o -5 19 2 1730.78 1627.76 88.90 o -3 19 2 2388.57 2314.16 123.34 o -1 19 2 655.65 710.25 54.11 o 1 19 2 1095.19 1122.74 22.64 o 3 19 2 313.19 298.51 19.58 o -6 20 2 849.68 802.13 49.60 o -4 20 2 583.44 573.56 31.09 o -2 20 2 2258.70 2236.45 115.68 o 0 20 2 2607.63 2706.25 76.28 o 2 20 2 363.15 358.22 14.03 o -5 21 2 893.41 841.79 32.19 o -3 21 2 2682.41 2579.53 109.92 o -1 21 2 1455.89 1508.44 46.64 o 1 21 2 2154.93 2224.78 65.22 o -6 22 2 515.95 487.83 36.47 o -4 22 2 1519.10 1519.57 120.67 o -2 22 2 554.19 594.87 44.18 o 0 22 2 798.10 839.76 38.14 o 2 22 2 221.09 236.27 12.56 o -5 23 2 722.15 712.43 107.36 o -3 23 2 1667.24 1644.07 105.34 o -1 23 2 1038.28 1075.41 23.07 o 1 23 2 532.33 580.53 18.21 o -4 24 2 1379.01 1363.41 100.68 o -2 24 2 592.90 596.40 25.26 o 0 24 2 587.57 613.40 18.68 o -1 25 2 484.66 489.86 24.05 o -11 1 3 156.62 164.86 24.00 o -9 1 3 814.18 844.63 31.92 o -7 1 3 40.43 50.94 8.57 o -5 1 3 542.60 545.05 10.11 o -3 1 3 404.68 349.84 4.58 o -1 1 3 72.00 69.47 2.51 o 1 1 3 1305.86 1464.43 11.23 o 3 1 3 698.05 610.01 14.03 o 5 1 3 118.16 73.27 9.78 o -10 2 3 100.37 99.88 8.51 o -8 2 3 24.45 13.13 4.49 o -6 2 3 19.53 22.00 4.00 o -4 2 3 922.28 920.97 21.57 o -2 2 3 1662.64 1743.59 29.19 o 0 2 3 673.67 659.88 5.59 o 2 2 3 76.20 79.49 3.69 o 4 2 3 43.18 38.23 5.94 o -11 3 3 0.01 1.79 6.04 o -9 3 3 4.36 3.44 5.05 o -7 3 3 1.95 4.44 5.77 o -5 3 3 28.58 26.54 3.01 o -3 3 3 6445.97 6456.19 28.21 o -1 3 3 73.82 78.01 3.70 o 1 3 3 0.11 2.15 2.36 o 3 3 3 51.63 49.22 5.39 o 5 3 3 6.63 13.66 5.90 o -10 4 3 46.65 39.01 7.17 o -8 4 3 111.43 119.98 6.00 o -6 4 3 6.98 9.60 3.30 o -4 4 3 4523.11 4687.55 55.63 o -2 4 3 997.33 1130.66 15.04 o 0 4 3 254.54 229.88 4.46 o 2 4 3 0.64 6.05 3.26 o 4 4 3 24.83 23.00 4.41 o -9 5 3 173.13 177.08 7.88 o -7 5 3 235.27 238.37 7.09 o -5 5 3 33.00 50.77 12.86 o -3 5 3 138.67 115.88 3.38 o -1 5 3 227.06 232.40 6.55 o 1 5 3 2.20 6.99 3.21 o 3 5 3 49.95 41.27 4.07 o 5 5 3 0.02 2.80 8.57 o -10 6 3 2.44 3.85 4.80 o -8 6 3 0.38 -2.43 3.42 o -6 6 3 2.95 -1.68 2.54 o -4 6 3 6412.86 6827.15 30.19 o -2 6 3 655.54 760.30 10.80 o 0 6 3 49.50 54.43 4.14 o 2 6 3 42.91 32.23 3.69 o 4 6 3 10.41 16.93 4.44 o -9 7 3 19.36 20.66 4.64 o -7 7 3 86.87 97.72 4.52 o -5 7 3 26.03 29.26 2.79 o -3 7 3 83.91 89.19 2.77 o -1 7 3 329.21 341.30 7.53 o 1 7 3 3.96 6.58 3.19 o 3 7 3 19.24 15.17 4.25 o 5 7 3 0.02 0.97 5.49 o -10 8 3 0.11 -4.16 4.60 o -8 8 3 0.42 -1.75 3.56 o -6 8 3 0.03 -0.03 2.68 o -4 8 3 13.21 4.14 1.60 o -2 8 3 0.28 1.11 1.57 o 0 8 3 221.44 227.77 5.98 o 2 8 3 69.66 87.94 5.50 o 4 8 3 1.89 1.40 6.88 o -9 9 3 1.15 -2.23 3.67 o -7 9 3 25.52 15.30 3.00 o -5 9 3 785.23 811.89 18.14 o -3 9 3 34.29 43.00 2.36 o -1 9 3 375.42 412.07 7.37 o 1 9 3 150.59 151.61 9.31 o 3 9 3 20.94 20.55 4.80 o -10 10 3 102.39 111.19 7.92 o -8 10 3 0.83 0.39 3.34 o -6 10 3 15.61 14.96 2.75 o -4 10 3 632.53 625.83 13.98 o -2 10 3 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