# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' EuB3O6 I2/a ' _shelx_refln_list_code 4 _shelx_F_calc_maximum 246.18 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.5535 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 6.2830 _cell_length_b 8.0331 _cell_length_c 7.8406 _cell_angle_alpha 90.000 _cell_angle_beta 93.700 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 60605.30 40618.81 6933.76 o 4 0 0 14371.61 14234.34 3415.63 o 6 0 0 21953.30 25969.94 6601.25 o 8 0 0 13046.77 17691.36 4949.80 o 10 0 0 3851.98 5860.97 1326.72 o 1 1 0 29174.71 20978.80 2690.80 o 3 1 0 57812.46 48296.89 5187.75 o 5 1 0 20239.80 24383.22 3632.05 o 7 1 0 6031.88 7119.77 1165.68 o 9 1 0 6096.09 10764.05 511.65 o 11 1 0 4474.83 6846.61 1047.05 o 0 2 0 34366.93 21663.84 1415.88 o 2 2 0 23718.71 18747.28 1429.45 o 4 2 0 17448.47 17920.88 2222.76 o 6 2 0 14210.33 16553.21 2425.77 o 8 2 0 7326.45 9517.66 1521.20 o 10 2 0 3487.22 5358.95 851.23 o 1 3 0 10462.97 8844.64 1199.55 o 3 3 0 3803.78 3418.92 290.53 o 5 3 0 4848.16 5400.52 827.97 o 7 3 0 5805.59 6836.14 1050.76 o 9 3 0 3408.39 5173.68 744.48 o 11 3 0 1554.33 3111.51 840.58 o 0 4 0 138.41 252.99 90.51 o 2 4 0 3504.52 3319.18 293.50 o 4 4 0 4956.18 4995.08 848.44 o 6 4 0 1422.10 1755.24 271.98 o 8 4 0 1237.00 1945.94 303.32 o 10 4 0 1399.83 2514.82 645.01 o 1 5 0 254.26 208.01 40.66 o 3 5 0 6.65 20.54 47.12 o 5 5 0 147.10 191.17 36.92 o 7 5 0 78.74 -34.84 46.05 o 9 5 0 73.55 2.62 57.03 o 0 6 0 81.38 9.02 175.66 o 2 6 0 189.29 292.92 61.25 o 4 6 0 808.84 840.04 95.59 o 6 6 0 1112.46 1337.36 194.96 o 8 6 0 489.31 630.06 107.10 o 10 6 0 222.12 348.01 128.57 o 1 7 0 3317.53 3094.16 68.88 o 3 7 0 3954.38 3557.61 320.32 o 5 7 0 3917.21 3768.49 447.61 o 7 7 0 2671.36 3150.79 372.82 o 9 7 0 1599.25 2328.99 359.32 o 0 8 0 12587.89 10004.37 1071.16 o 2 8 0 9053.57 7559.61 736.10 o 4 8 0 5053.86 4776.53 426.45 o 6 8 0 4408.22 4232.69 625.55 o 8 8 0 4004.70 5311.99 488.65 o 1 9 0 10975.73 8302.22 645.85 o 3 9 0 13035.65 12520.09 1165.53 o 5 9 0 8241.00 8121.65 1000.72 o 7 9 0 3489.22 3808.40 448.16 o 0 10 0 15550.87 12240.60 1944.38 o 2 10 0 10858.31 9057.18 872.07 o 4 10 0 7391.33 7353.46 615.43 o 6 10 0 7224.92 7013.19 885.15 o 8 10 0 4116.61 5024.50 680.74 o 1 11 0 7557.79 5559.44 314.42 o 3 11 0 7944.91 7375.95 1008.52 o 5 11 0 4641.87 4961.49 594.23 o 7 11 0 3020.57 3213.93 494.35 o 0 12 0 4864.91 4661.89 163.58 o 2 12 0 4305.05 3944.67 354.70 o 4 12 0 4065.15 4523.81 423.38 o 6 12 0 4107.67 4340.32 565.77 o 1 13 0 1634.68 1442.91 102.58 o 3 13 0 1619.87 1590.72 145.75 o 5 13 0 2129.28 2540.04 296.82 o 0 14 0 669.04 632.25 109.03 o 2 14 0 1272.93 1162.22 155.07 o -10 1 1 692.41 1067.15 175.14 o -8 1 1 1471.80 2092.62 277.49 o -6 1 1 1564.53 1216.77 79.73 o -4 1 1 3470.70 3342.09 362.39 o -2 1 1 15688.01 15220.37 288.88 o 0 1 1 5099.09 6111.14 116.22 o 2 1 1 487.75 930.88 109.23 o 4 1 1 883.44 754.55 29.60 o 6 1 1 2516.13 3396.90 456.41 o 8 1 1 683.76 1074.16 146.77 o 10 1 1 271.57 512.34 93.31 o -11 2 1 1411.39 1973.74 352.61 o -9 2 1 1947.48 2258.29 255.13 o -7 2 1 5368.84 6322.80 895.82 o -5 2 1 13780.52 12840.99 1473.72 o -3 2 1 10377.21 8743.40 411.26 o -1 2 1 4151.36 4270.14 150.00 o 1 2 1 19648.01 20198.35 734.49 o 3 2 1 10037.27 9687.03 779.01 o 5 2 1 1472.53 1826.30 265.72 o 7 2 1 2386.87 3423.77 660.91 o 9 2 1 3396.04 5490.77 739.98 o 11 2 1 1437.62 2497.45 437.43 o -10 3 1 3897.28 5616.60 715.36 o -8 3 1 7249.85 8849.14 1331.56 o -6 3 1 8417.55 8524.29 1383.33 o -4 3 1 15400.07 12861.46 933.64 o -2 3 1 33670.20 32836.91 1872.06 o 0 3 1 22946.20 22576.33 1052.81 o 2 3 1 15874.61 13469.04 1607.38 o 4 3 1 19473.85 17624.79 1133.21 o 6 3 1 10007.26 11288.12 1492.37 o 8 3 1 4154.63 4948.75 882.19 o 10 3 1 3777.01 5706.12 875.30 o -9 4 1 4069.74 5703.64 689.26 o -7 4 1 8321.64 9524.02 1361.60 o -5 4 1 11918.75 11164.99 1306.21 o -3 4 1 13913.98 11851.51 968.99 o -1 4 1 34773.72 32649.30 717.37 o 1 4 1 40762.26 39763.69 4582.17 o 3 4 1 17329.39 16883.78 1378.49 o 5 4 1 15445.69 15893.10 2153.53 o 7 4 1 14181.40 16717.56 2061.54 o 9 4 1 5262.67 7282.69 1082.11 o -10 5 1 6397.69 9183.23 1284.91 o -8 5 1 6476.50 9345.03 872.97 o -6 5 1 8811.59 9611.90 1109.91 o -4 5 1 22071.94 19237.91 2095.27 o -2 5 1 25515.84 22567.49 1314.35 o 0 5 1 20286.96 18411.65 1922.77 o 2 5 1 39478.23 39199.12 3116.24 o 4 5 1 32357.11 34234.32 8787.73 o 6 5 1 11215.03 11552.28 1786.76 o 8 5 1 6929.62 8320.23 1079.97 o 10 5 1 6330.90 8717.01 1263.25 o -9 6 1 4431.73 6347.42 924.27 o -7 6 1 10987.30 12313.52 1512.75 o -5 6 1 10325.73 9940.91 965.44 o -3 6 1 9196.97 7675.22 769.78 o -1 6 1 23950.33 18929.94 1544.31 o 1 6 1 27069.21 25151.07 3694.35 o 3 6 1 13571.74 13897.30 1839.77 o 5 6 1 11312.48 11536.94 1335.57 o 7 6 1 8778.85 9742.81 1128.50 o 9 6 1 4114.78 5867.56 701.86 o -8 7 1 4763.79 6058.71 733.15 o -6 7 1 6993.07 7680.96 898.63 o -4 7 1 14823.28 12680.11 1773.32 o -2 7 1 18382.40 14823.58 779.63 o 0 7 1 12161.65 10294.23 1043.90 o 2 7 1 9678.90 9906.94 239.61 o 4 7 1 9552.84 9039.51 864.50 o 6 7 1 7518.17 7628.60 1108.22 o 8 7 1 4872.44 5941.87 720.25 o -9 8 1 1854.57 2699.39 309.45 o -7 8 1 2898.94 3424.65 372.61 o -5 8 1 5746.05 6457.49 739.60 o -3 8 1 6773.52 5782.88 564.04 o -1 8 1 4393.19 3439.27 219.52 o 1 8 1 4319.92 4051.56 523.31 o 3 8 1 4358.08 4297.94 339.40 o 5 8 1 2232.14 2419.05 437.64 o 7 8 1 1611.86 1710.14 304.23 o 9 8 1 1991.76 2563.67 315.56 o -8 9 1 1774.47 2439.36 238.64 o -6 9 1 2685.61 2835.10 461.57 o -4 9 1 1034.35 1164.68 236.04 o -2 9 1 1878.95 1692.19 80.33 o 0 9 1 4246.39 3935.49 248.08 o 2 9 1 1956.37 1902.98 213.07 o 4 9 1 1012.20 1159.07 158.03 o 6 9 1 1507.22 1595.82 224.52 o 8 9 1 905.89 1152.69 227.73 o -7 10 1 197.72 234.75 65.32 o -5 10 1 1.56 6.51 49.21 o -3 10 1 420.32 509.06 54.27 o -1 10 1 6.40 -57.11 57.11 o 1 10 1 17.40 -220.63 220.63 o 3 10 1 269.40 98.85 73.90 o 5 10 1 191.57 192.06 38.43 o 7 10 1 16.62 -47.00 47.00 o -6 11 1 148.20 395.37 150.31 o -4 11 1 518.37 628.25 77.87 o -2 11 1 549.27 489.07 81.83 o 0 11 1 21.33 71.97 175.96 o 2 11 1 12.97 -4.41 52.09 o 4 11 1 118.26 246.63 91.18 o 6 11 1 16.26 36.29 66.01 o -5 12 1 2245.44 2956.59 286.34 o -3 12 1 2121.81 2021.64 155.19 o -1 12 1 1709.24 1600.44 121.95 o 1 12 1 1829.85 1736.53 145.51 o 3 12 1 1067.38 1238.91 118.31 o 5 12 1 772.10 827.89 68.22 o -4 13 1 1574.36 1789.73 205.15 o -2 13 1 2944.70 2687.48 176.87 o 0 13 1 2869.46 3083.89 340.13 o 2 13 1 2350.29 2529.42 189.98 o 4 13 1 3019.81 3248.28 323.66 o -1 14 1 3351.65 3074.96 284.54 o 1 14 1 5511.55 4849.01 265.73 o -10 0 2 5202.59 7258.54 2256.00 o -8 0 2 11240.94 12168.16 3854.26 o -6 0 2 21061.90 15506.69 266.17 o -4 0 2 21753.11 19325.18 1253.56 o -2 0 2 24478.75 23764.78 326.07 o 0 0 2 39039.91 45278.23 1781.34 o 2 0 2 37662.82 41443.78 808.28 o 4 0 2 31144.10 29321.36 1925.59 o 6 0 2 21825.10 21688.61 3764.21 o 8 0 2 10618.59 13754.38 2971.01 o 10 0 2 5546.45 8363.93 1758.19 o -11 1 2 4361.80 6384.97 1068.84 o -9 1 2 7812.22 11110.66 1972.74 o -7 1 2 9165.47 8909.33 1309.71 o -5 1 2 13896.88 10967.82 908.68 o -3 1 2 27893.21 26103.42 478.96 o -1 1 2 30250.95 30887.45 1333.06 o 1 1 2 25470.55 28671.36 269.33 o 3 1 2 27720.08 28167.90 717.29 o 5 1 2 18480.14 17609.67 1514.55 o 7 1 2 10389.15 12486.07 1570.52 o 9 1 2 6570.46 8637.07 1297.76 o 11 1 2 3850.61 5789.00 801.47 o -10 2 2 3883.07 5309.97 957.91 o -8 2 2 6267.84 7668.90 1372.17 o -6 2 2 13334.49 11622.76 1255.91 o -4 2 2 20446.10 17885.15 777.38 o -2 2 2 24786.47 24850.44 522.71 o 0 2 2 49543.26 55550.08 1059.30 o 2 2 2 38988.23 42083.46 587.76 o 4 2 2 11975.70 11059.23 625.75 o 6 2 2 8270.45 7905.82 1352.55 o 8 2 2 8236.67 9792.04 1382.71 o 10 2 2 4047.48 5841.50 999.75 o -11 3 2 661.31 1249.88 396.24 o -9 3 2 2223.47 3227.48 602.68 o -7 3 2 4318.69 4331.09 649.23 o -5 3 2 5854.37 4841.23 462.20 o -3 3 2 18163.65 17900.77 531.42 o -1 3 2 29141.53 32524.80 1296.78 o 1 3 2 8323.40 8868.95 225.87 o 3 3 2 7941.04 7785.45 431.02 o 5 3 2 9171.12 8885.14 776.56 o 7 3 2 2215.02 3013.32 339.33 o 9 3 2 622.33 888.35 79.46 o -10 4 2 623.51 1201.21 486.50 o -8 4 2 542.00 798.00 158.82 o -6 4 2 2556.57 2380.34 279.57 o -4 4 2 6031.06 5445.19 106.74 o -2 4 2 3755.84 3978.06 131.54 o 0 4 2 6246.97 7038.43 152.49 o 2 4 2 9036.36 9187.65 358.42 o 4 4 2 1915.97 1996.10 434.31 o 6 4 2 658.20 755.34 166.76 o 8 4 2 1289.48 1779.31 343.34 o 10 4 2 740.70 1096.34 299.25 o -9 5 2 42.68 94.95 63.90 o -7 5 2 19.88 41.28 44.03 o -5 5 2 80.79 136.61 55.39 o -3 5 2 104.23 280.53 55.21 o -1 5 2 131.22 291.65 36.44 o 1 5 2 105.09 248.37 88.98 o 3 5 2 72.69 188.00 29.57 o 5 5 2 11.38 -48.34 48.34 o 7 5 2 96.72 97.99 52.20 o 9 5 2 80.44 85.99 85.48 o -10 6 2 130.32 22.42 140.16 o -8 6 2 132.16 -118.32 210.93 o -6 6 2 1080.76 1133.15 177.32 o -4 6 2 1671.62 1500.03 95.89 o -2 6 2 1147.68 1401.44 76.64 o 0 6 2 4121.91 4225.56 182.51 o 2 6 2 3478.33 3511.81 205.88 o 4 6 2 48.04 9.20 64.45 o 6 6 2 31.94 5.61 35.99 o 8 6 2 666.10 775.47 107.76 o 10 6 2 231.63 122.57 165.62 o -9 7 2 2433.08 3670.91 502.73 o -7 7 2 2290.43 2426.57 284.90 o -5 7 2 1386.59 1245.65 133.64 o -3 7 2 7819.33 7997.94 437.09 o -1 7 2 13080.66 12648.95 566.16 o 1 7 2 3156.04 2779.95 406.29 o 3 7 2 2836.32 2836.99 145.95 o 5 7 2 5025.21 5273.53 972.74 o 7 7 2 1522.71 1806.01 242.59 o 9 7 2 499.55 613.46 274.31 o -8 8 2 1679.37 2371.88 348.82 o -6 8 2 7245.30 6489.68 680.75 o -4 8 2 9051.00 7912.70 839.05 o -2 8 2 3470.60 3264.72 249.72 o 0 8 2 6792.07 6683.60 250.12 o 2 8 2 12537.61 11500.03 794.38 o 4 8 2 5830.25 5550.08 449.25 o 6 8 2 3378.00 3561.06 540.15 o 8 8 2 3930.13 4340.80 643.09 o -7 9 2 4736.22 4810.34 827.57 o -5 9 2 4329.88 4590.30 165.60 o -3 9 2 8067.73 7532.60 241.84 o -1 9 2 10203.75 8750.95 665.66 o 1 9 2 7128.70 6685.13 522.43 o 3 9 2 7852.91 7431.52 604.42 o 5 9 2 8690.59 8633.70 887.21 o 7 9 2 5319.09 5720.86 891.15 o -8 10 2 5161.63 6096.07 624.20 o -6 10 2 5852.80 5912.99 575.22 o -4 10 2 5946.05 5128.99 674.79 o -2 10 2 8276.19 7169.81 567.55 o 0 10 2 10497.69 9720.80 594.98 o 2 10 2 8771.14 8103.73 609.04 o 4 10 2 7214.76 7053.00 732.46 o 6 10 2 7007.28 6903.06 817.00 o -7 11 2 3864.84 4090.15 472.95 o -5 11 2 7507.39 8337.61 918.75 o -3 11 2 7213.56 6258.09 977.80 o -1 11 2 5389.13 5438.79 174.58 o 1 11 2 7388.48 6431.76 574.04 o 3 11 2 8360.21 8362.74 602.22 o 5 11 2 5461.86 5477.27 735.53 o 7 11 2 3573.56 3601.50 506.16 o -6 12 2 3487.41 4211.41 408.11 o -4 12 2 4864.53 5043.39 519.52 o -2 12 2 7512.23 6921.34 529.69 o 0 12 2 6940.64 6868.68 333.92 o 2 12 2 5006.08 5166.40 437.23 o 4 12 2 4488.69 4462.19 532.16 o 6 12 2 3131.23 3211.64 453.96 o -3 13 2 2485.15 2692.66 319.39 o -1 13 2 3817.32 3715.64 365.14 o 1 13 2 3505.80 3229.82 452.81 o 3 13 2 1583.02 1732.34 160.71 o -2 14 2 999.88 1107.29 110.13 o 0 14 2 655.07 1432.77 574.86 o 2 14 2 1127.24 1137.28 176.59 o -10 1 3 472.36 681.62 89.26 o -8 1 3 1535.65 1830.38 246.63 o -6 1 3 397.79 355.91 50.73 o -4 1 3 516.41 528.25 43.38 o -2 1 3 8855.01 9785.62 79.26 o 0 1 3 8637.70 10370.65 233.58 o 2 1 3 4368.23 5144.93 52.07 o 4 1 3 5665.46 5655.19 212.52 o 6 1 3 1591.55 1409.38 83.86 o 8 1 3 214.64 380.12 44.84 o 10 1 3 508.05 727.53 78.61 o -11 2 3 1894.43 2812.55 478.48 o -9 2 3 606.80 1107.96 370.23 o -7 2 3 1914.02 1793.89 366.43 o -5 2 3 9314.59 7960.29 291.91 o -3 2 3 6479.99 6456.33 114.03 o -1 2 3 7076.33 7773.62 59.91 o 1 2 3 31337.99 36537.76 1911.89 o 3 2 3 14338.41 15819.93 643.66 o 5 2 3 3613.77 3380.54 193.49 o 7 2 3 4507.89 4717.15 585.95 o 9 2 3 2599.23 3411.71 533.07 o -10 3 3 3761.77 4798.32 685.92 o -8 3 3 7343.16 6910.04 1255.44 o -6 3 3 6257.07 5150.28 288.37 o -4 3 3 10839.04 10257.33 292.60 o -2 3 3 34454.14 37286.82 723.15 o 0 3 3 23909.48 27056.39 507.93 o 2 3 3 9843.94 10606.31 273.70 o 4 3 3 16728.69 15375.53 1100.60 o 6 3 3 11969.30 11391.08 1191.66 o 8 3 3 3820.03 3425.81 331.02 o 10 3 3 2550.20 3471.90 415.27 o -9 4 3 5733.76 6657.33 963.60 o -7 4 3 10424.21 9392.97 1005.85 o -5 4 3 17481.65 14193.92 1034.98 o -3 4 3 16549.65 16472.86 422.34 o -1 4 3 13351.08 14897.69 337.40 o 1 4 3 22982.71 25372.23 1207.86 o 3 4 3 19520.12 19273.99 904.54 o 5 4 3 7841.00 7244.75 455.45 o 7 4 3 5991.18 5877.66 727.52 o 9 4 3 6528.96 8173.32 1134.93 o -10 5 3 4969.31 6613.14 918.12 o -8 5 3 9351.36 9862.87 1267.83 o -6 5 3 15437.74 12513.20 1136.56 o -4 5 3 18502.23 15705.70 1968.11 o -2 5 3 22738.77 24194.13 695.05 o 0 5 3 24755.28 26850.61 467.79 o 2 5 3 15040.54 15484.63 550.11 o 4 5 3 12061.84 10880.73 1042.91 o 6 5 3 13308.36 12977.23 1548.74 o 8 5 3 8613.15 9408.64 1244.14 o 10 5 3 4036.65 5394.76 712.59 o -9 6 3 5010.95 5977.21 749.22 o -7 6 3 6238.41 5654.12 586.39 o -5 6 3 11363.60 9270.80 548.37 o -3 6 3 19593.81 18742.59 919.65 o -1 6 3 16224.93 17580.38 563.67 o 1 6 3 11843.29 12320.60 707.19 o 3 6 3 14438.43 12766.79 1151.04 o 5 6 3 11614.19 11018.35 978.30 o 7 6 3 6384.05 6381.33 801.77 o 9 6 3 4457.67 5746.32 717.10 o -8 7 3 5203.87 5467.34 702.73 o -6 7 3 7344.38 6144.85 831.17 o -4 7 3 7960.61 7201.90 575.22 o -2 7 3 11829.52 12009.82 515.28 o 0 7 3 18544.91 18505.22 479.61 o 2 7 3 16722.85 15158.31 1358.62 o 4 7 3 10382.59 9729.65 898.19 o 6 7 3 6688.53 6566.32 779.53 o 8 7 3 4352.76 4668.91 720.28 o -9 8 3 993.57 1422.97 230.70 o -7 8 3 1836.75 1774.76 204.27 o -5 8 3 3270.18 2772.18 350.26 o -3 8 3 3981.69 3784.37 409.25 o -1 8 3 5902.74 5851.74 236.84 o 1 8 3 8300.90 7908.59 441.26 o 3 8 3 6178.95 6016.02 147.60 o 5 8 3 3482.89 3434.49 347.08 o 7 8 3 2464.79 2547.50 399.97 o -8 9 3 624.64 706.45 113.94 o -6 9 3 582.88 653.61 56.21 o -4 9 3 2203.25 2137.08 242.97 o -2 9 3 3696.43 3520.37 213.76 o 0 9 3 1886.49 1854.57 170.52 o 2 9 3 1637.73 1494.81 207.59 o 4 9 3 2706.81 2714.14 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