data_3 # 452 at 150K _audit_creation_date 04-09-30 _audit_creation_method CRYSTALS _cell_length_a 12.5693(4) _cell_angle_alpha 90 _cell_length_b 4.85310(10) _cell_angle_beta 99.1624(15) _cell_length_c 17.2663(5) _cell_angle_gamma 90 # NOTE Fc on scale of Fo, 0.91919 # Status flags: # o - used in refinement # < - excluded by I/sigmaI cutoff # x - excluded for another reason loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 4 0 0 3430.70 3432.01 98.20 o 6 0 0 903.90 839.76 30.20 o 8 0 0 226.20 240.17 6.00 o 10 0 0 517.30 483.92 15.80 o 12 0 0 93.50 96.56 4.00 o 14 0 0 428.00 376.56 23.20 o 16 0 0 38.10 42.54 7.20 o 2 1 0 796.85 951.43 20.08 o 3 1 0 73.90 75.56 2.31 o 4 1 0 69.70 75.89 2.75 o 5 1 0 6256.05 5829.06 214.11 o 6 1 0 715.70 687.67 22.31 o 7 1 0 2.35 1.40 1.32 o 8 1 0 403.55 395.15 13.50 o 9 1 0 68.20 69.84 3.15 o 10 1 0 52.40 54.66 3.26 o 11 1 0 112.25 104.59 5.98 o 12 1 0 7.60 8.14 2.34 o 13 1 0 3.60 4.75 2.14 o 14 1 0 1.25 0.28 2.83 o 15 1 0 18.30 20.05 5.32 o 0 2 0 611.70 580.35 24.45 o 1 2 0 9.20 12.53 0.70 o 2 2 0 573.55 538.26 17.18 o 3 2 0 1995.35 2059.02 48.85 o 4 2 0 470.65 467.25 19.93 o 5 2 0 1097.55 1086.83 30.46 o 6 2 0 270.20 245.29 7.72 o 7 2 0 3.55 5.37 1.39 o 8 2 0 15.00 18.58 1.61 o 9 2 0 91.85 84.48 4.20 o 10 2 0 6.00 2.65 1.95 o 11 2 0 82.65 93.80 4.50 o 12 2 0 28.20 38.86 3.16 o 13 2 0 7.30 8.26 4.05 o 14 2 0 9.10 10.13 4.07 o 15 2 0 29.20 46.33 6.20 o 1 3 0 0.35 0.83 2.03 o 2 3 0 754.15 779.52 27.58 o 3 3 0 352.50 336.19 10.28 o 4 3 0 22.00 17.04 1.55 o 5 3 0 2.15 2.37 0.99 o 6 3 0 27.75 25.88 1.95 o 7 3 0 -0.65 0.29 2.16 o 8 3 0 73.10 70.42 3.31 o 9 3 0 3.25 9.55 1.90 o 10 3 0 3.60 1.83 1.76 o 11 3 0 33.50 41.29 3.08 o 12 3 0 68.00 70.43 4.99 o 13 3 0 34.55 38.96 4.92 o 14 3 0 6.80 7.37 3.90 o 0 4 0 55.00 53.92 4.55 o 1 4 0 44.50 36.16 3.44 o 2 4 0 15.55 14.11 2.16 o 3 4 0 367.15 390.06 15.31 o 4 4 0 40.65 41.91 2.20 o 5 4 0 9.05 4.83 1.50 o 6 4 0 195.45 197.95 7.03 o 7 4 0 46.90 60.43 3.17 o 8 4 0 387.80 404.30 14.74 o 9 4 0 11.40 15.36 2.30 o 10 4 0 0.90 0.37 3.38 o 11 4 0 27.30 23.63 3.87 o 12 4 0 13.10 15.85 3.30 o 1 5 0 27.50 29.22 2.90 o 2 5 0 77.90 78.79 5.85 o 3 5 0 483.45 455.42 20.88 o 4 5 0 4.95 6.56 2.95 o 5 5 0 47.30 51.99 5.98 o 6 5 0 -0.45 0.03 2.88 o 7 5 0 19.30 25.36 4.80 o 8 5 0 49.60 49.59 6.30 o 9 5 0 118.50 135.12 6.40 o 0 6 0 8.80 5.29 3.80 o 1 6 0 25.60 30.55 3.80 o 2 6 0 23.20 16.86 3.40 o 3 6 0 0.60 2.60 7.28 o 4 6 0 17.90 16.15 5.00 o -15 0 1 5.70 1.60 2.90 o -13 0 1 56.90 54.14 3.00 o -11 0 1 397.90 385.80 11.90 o -9 0 1 1641.50 1590.46 39.40 o -7 0 1 1835.90 1730.09 44.10 o -5 0 1 192.90 193.02 5.00 o 5 0 1 121.90 110.52 3.60 o 7 0 1 451.40 469.57 13.00 o 9 0 1 145.10 119.83 4.50 o 11 0 1 370.90 335.69 12.20 o 13 0 1 152.30 146.68 7.40 o 15 0 1 14.90 16.76 2.70 o -16 1 1 30.95 40.24 5.40 o -15 1 1 2.30 3.60 4.30 o -14 1 1 4.00 0.52 3.73 o -13 1 1 53.45 62.82 4.26 o -12 1 1 3.80 4.43 1.71 o -11 1 1 49.55 54.50 3.52 o -10 1 1 64.25 59.22 3.41 o -9 1 1 45.10 40.17 2.76 o -8 1 1 1.70 1.39 1.36 o -7 1 1 767.50 708.50 21.24 o -6 1 1 302.70 300.65 7.62 o -5 1 1 25.05 15.10 1.40 o -4 1 1 3266.95 3296.84 95.37 o -3 1 1 9709.85 9324.96 355.06 o -2 1 1 2300.20 2494.98 55.66 o 2 1 1 461.50 508.95 13.35 o 3 1 1 60.35 56.15 3.35 o 4 1 1 167.95 156.46 7.51 o 5 1 1 7.05 4.27 1.14 o 6 1 1 527.90 515.55 18.14 o 7 1 1 849.60 816.59 25.89 o 8 1 1 482.30 502.26 15.75 o 9 1 1 50.85 54.76 2.75 o 10 1 1 26.40 27.09 2.11 o 11 1 1 -0.55 2.54 2.31 o 12 1 1 340.75 344.34 16.40 o 13 1 1 -0.40 0.60 4.17 o 14 1 1 27.15 31.90 3.69 o 15 1 1 85.45 89.25 7.05 o -15 2 1 44.40 54.38 6.50 o -14 2 1 -1.05 0.06 3.91 o -13 2 1 76.20 89.97 5.59 o -12 2 1 196.00 214.52 10.15 o -11 2 1 93.45 109.72 4.80 o -10 2 1 36.50 35.12 2.83 o -9 2 1 64.85 63.59 3.35 o -8 2 1 85.25 89.15 3.96 o -7 2 1 42.30 39.44 1.97 o -6 2 1 54.15 60.02 1.96 o -5 2 1 2179.65 2117.65 49.77 o -4 2 1 30.25 25.85 1.45 o -3 2 1 1359.95 1301.62 44.77 o -2 2 1 126.60 135.24 4.46 o -1 2 1 92.25 72.62 3.72 o 0 2 1 228.45 226.12 6.27 o 1 2 1 564.75 522.93 18.18 o 2 2 1 732.05 716.89 28.39 o 3 2 1 1484.55 1401.83 44.79 o 4 2 1 180.15 165.80 6.47 o 5 2 1 3.25 1.39 1.74 o 6 2 1 50.00 51.33 2.35 o 7 2 1 10.70 6.70 1.47 o 8 2 1 456.15 426.74 14.56 o 9 2 1 -1.20 0.81 1.43 o 10 2 1 13.85 11.48 2.41 o 11 2 1 -1.45 2.79 2.55 o 12 2 1 0.85 0.11 2.42 o 13 2 1 53.00 57.77 5.08 o 14 2 1 8.95 6.06 4.10 o 15 2 1 -5.25 1.20 5.34 o -14 3 1 23.30 16.39 5.80 o -13 3 1 47.05 50.51 6.49 o -12 3 1 25.60 22.57 3.25 o -11 3 1 67.05 75.40 5.16 o -10 3 1 -1.05 0.38 2.50 o -9 3 1 8.85 16.12 2.22 o -8 3 1 158.40 137.48 5.87 o -7 3 1 255.05 243.94 8.30 o -6 3 1 73.55 80.26 3.00 o -5 3 1 278.15 279.88 7.23 o -4 3 1 94.80 87.63 3.17 o -3 3 1 3.05 0.83 0.92 o -2 3 1 20.45 21.66 1.72 o -1 3 1 122.45 107.24 5.32 o 0 3 1 6.00 3.81 1.14 o 1 3 1 136.80 123.47 4.57 o 2 3 1 1038.05 990.08 32.46 o 3 3 1 45.25 33.87 2.00 o 4 3 1 7.35 10.05 1.20 o 5 3 1 4.60 2.61 1.35 o 6 3 1 395.30 375.63 11.53 o 7 3 1 262.05 287.16 8.15 o 8 3 1 10.40 18.42 1.78 o 9 3 1 19.55 28.86 2.04 o 10 3 1 4.15 5.03 2.84 o 11 3 1 81.40 82.32 4.71 o 12 3 1 10.40 11.44 2.90 o 13 3 1 13.35 14.68 3.75 o 14 3 1 3.20 1.07 3.10 o -12 4 1 25.80 30.75 3.50 o -11 4 1 43.30 49.47 6.09 o -10 4 1 118.35 128.48 6.57 o -9 4 1 61.30 67.18 4.14 o -8 4 1 296.10 315.69 11.15 o -7 4 1 61.70 57.31 3.67 o -6 4 1 33.00 34.78 2.45 o -5 4 1 1.65 0.68 1.32 o -4 4 1 8.20 11.07 1.27 o -3 4 1 563.70 505.72 21.77 o -2 4 1 37.25 35.09 3.80 o -1 4 1 46.05 44.80 4.17 o 0 4 1 1027.85 1009.11 40.66 o 1 4 1 133.35 140.38 7.45 o 2 4 1 38.90 37.64 3.04 o 3 4 1 17.30 17.90 2.44 o 4 4 1 14.85 11.69 1.50 o 5 4 1 8.85 11.94 1.46 o 6 4 1 342.55 355.20 11.96 o 7 4 1 31.80 18.93 2.60 o 8 4 1 110.95 117.37 5.10 o 9 4 1 3.90 5.72 2.18 o 10 4 1 34.80 41.09 4.50 o 11 4 1 6.85 6.11 2.73 o 12 4 1 24.90 20.88 3.50 o -9 5 1 3.90 5.03 2.90 o -8 5 1 66.00 66.49 8.03 o -7 5 1 2.95 3.20 3.97 o -6 5 1 161.80 147.51 10.91 o -5 5 1 3.90 3.88 3.86 o -4 5 1 56.65 56.67 5.22 o -3 5 1 351.55 353.58 16.29 o -2 5 1 201.65 188.95 10.69 o -1 5 1 14.65 16.33 4.17 o 0 5 1 131.40 138.70 5.20 o 1 5 1 5.20 0.51 2.30 o 2 5 1 74.95 71.76 5.34 o 3 5 1 34.65 33.92 3.91 o 4 5 1 169.15 153.67 9.81 o 5 5 1 70.80 65.91 5.57 o 6 5 1 14.85 14.16 4.13 o 7 5 1 1.20 4.86 4.49 o 9 5 1 2.40 0.06 3.20 o -4 6 1 6.60 9.09 6.10 o -3 6 1 29.70 29.21 6.40 o -2 6 1 -1.50 1.20 3.00 o -1 6 1 15.80 26.11 4.10 o 0 6 1 6.10 5.76 3.00 o 1 6 1 -4.00 1.19 4.50 o 2 6 1 19.40 20.41 3.10 o 3 6 1 1.30 0.56 4.50 o 4 6 1 6.20 1.44 4.40 o -16 0 2 20.80 31.23 6.40 o -14 0 2 231.60 211.90 11.10 o -12 0 2 109.90 101.61 4.40 o -10 0 2 259.40 207.48 7.90 o -8 0 2 3098.80 2937.38 59.80 o -6 0 2 10.90 10.81 0.90 o 4 0 2 383.60 446.55 22.60 o 6 0 2 -0.10 0.12 0.38 o 8 0 2 6.20 5.85 1.00 o 10 0 2 98.70 98.74 3.90 o 12 0 2 2.40 3.09 1.40 o 14 0 2 109.20 104.01 6.90 o -16 1 2 27.95 36.85 5.26 o -15 1 2 7.20 4.80 5.02 o -14 1 2 20.85 22.58 4.27 o -13 1 2 4.25 5.16 2.06 o -12 1 2 477.85 466.07 20.07 o -11 1 2 24.75 26.32 2.51 o -10 1 2 1.75 2.42 2.12 o -9 1 2 186.70 167.27 6.59 o -8 1 2 71.45 79.75 3.17 o -7 1 2 192.05 172.07 6.51 o -6 1 2 839.75 794.53 19.92 o -5 1 2 64.85 66.37 2.05 o -4 1 2 1327.30 1259.56 31.93 o -3 1 2 6601.10 6416.57 149.25 o -2 1 2 2559.85 2655.92 55.77 o 1 1 2 5502.45 5611.84 229.88 o 2 1 2 2394.90 2620.93 79.90 o 3 1 2 1.80 0.55 1.00 o 4 1 2 355.35 373.31 16.99 o 5 1 2 53.95 41.22 3.14 o 6 1 2 632.75 596.38 27.48 o 7 1 2 48.10 42.38 2.25 o 8 1 2 545.00 552.81 17.62 o 9 1 2 12.05 12.57 1.75 o 10 1 2 140.20 139.77 6.45 o 11 1 2 3.95 2.53 1.71 o 12 1 2 30.95 36.55 3.24 o 13 1 2 28.90 35.02 3.41 o 14 1 2 -2.75 0.00 3.55 o 15 1 2 14.80 21.71 3.57 o -15 2 2 82.70 77.49 8.27 o -14 2 2 7.05 2.03 3.85 o -13 2 2 46.20 47.06 5.09 o -12 2 2 134.10 114.98 6.90 o -11 2 2 52.50 63.60 3.21 o -10 2 2 3.05 0.11 1.76 o -9 2 2 4.55 2.85 1.53 o -8 2 2 41.90 45.46 2.16 o -7 2 2 1509.20 1469.26 34.58 o -6 2 2 208.85 182.78 5.41 o -5 2 2 74.10 64.16 2.97 o -4 2 2 702.50 658.52 20.73 o -3 2 2 67.65 71.60 3.13 o -2 2 2 286.15 259.73 7.75 o -1 2 2 82.05 89.00 3.35 o 0 2 2 1217.60 1210.66 39.61 o 1 2 2 218.50 212.13 6.05 o 2 2 2 244.75 225.31 6.67 o 3 2 2 500.05 523.32 14.76 o 4 2 2 1315.05 1299.64 41.65 o 5 2 2 187.80 206.37 8.81 o 6 2 2 227.45 214.77 9.18 o 7 2 2 33.55 34.90 2.50 o 8 2 2 2.00 2.92 1.43 o 9 2 2 133.45 146.08 5.80 o 10 2 2 52.80 59.47 3.35 o 11 2 2 50.65 50.83 3.73 o 12 2 2 60.95 70.50 4.22 o 13 2 2 12.75 8.95 3.39 o 14 2 2 4.15 2.73 4.07 o -14 3 2 28.10 36.54 7.09 o -13 3 2 8.80 6.32 3.60 o -12 3 2 20.30 14.71 3.28 o -11 3 2 1.65 2.44 2.07 o -10 3 2 96.95 100.92 5.08 o -9 3 2 -0.80 0.22 1.64 o -8 3 2 117.65 124.27 4.70 o -7 3 2 328.20 343.70 9.55 o -6 3 2 370.30 361.98 10.01 o -5 3 2 1176.20 1127.39 29.41 o -4 3 2 372.95 350.67 9.60 o -3 3 2 3.30 5.39 1.11 o -2 3 2 532.90 516.57 16.07 o -1 3 2 73.65 60.76 3.70 o 0 3 2 4.05 8.20 1.58 o 1 3 2 1191.05 1111.39 43.60 o 2 3 2 24.95 23.85 1.51 o 3 3 2 22.30 22.94 2.03 o 4 3 2 27.90 27.94 2.20 o 5 3 2 17.85 16.34 1.66 o 6 3 2 35.65 40.65 2.20 o 7 3 2 0.05 0.05 1.15 o 8 3 2 3.95 12.00 1.61 o 9 3 2 335.25 363.50 11.81 o 10 3 2 147.50 158.98 6.82 o 11 3 2 0.20 0.47 2.68 o 12 3 2 -1.05 0.24 2.37 o 13 3 2 1.05 1.78 4.07 o -12 4 2 39.60 46.26 4.40 o -11 4 2 63.90 58.99 5.02 o -10 4 2 221.55 212.24 10.47 o -9 4 2 358.10 348.37 16.86 o -8 4 2 2.75 1.64 2.01 o -7 4 2 3.90 3.08 1.85 o -6 4 2 8.65 5.73 2.06 o -5 4 2 19.80 22.66 1.77 o -4 4 2 13.75 12.75 1.24 o -3 4 2 -0.15 2.25 1.80 o -2 4 2 126.30 125.86 5.95 o -1 4 2 33.50 28.48 3.02 o 0 4 2 1.55 0.49 3.43 o 1 4 2 28.55 23.72 2.80 o 2 4 2 27.15 20.91 2.53 o 3 4 2 225.20 216.27 10.25 o 4 4 2 335.85 346.09 11.37 o 5 4 2 880.40 866.54 35.87 o 6 4 2 42.25 40.24 2.75 o 7 4 2 4.30 4.56 1.96 o 8 4 2 42.20 42.89 3.00 o 9 4 2 -0.05 3.56 2.41 o 10 4 2 43.60 37.16 4.04 o 11 4 2 52.20 50.67 5.88 o 12 4 2 21.10 18.52 3.80 o -9 5 2 80.40 96.47 6.71 o -8 5 2 -0.15 3.06 4.86 o -7 5 2 51.30 58.99 6.50 o -6 5 2 61.90 73.68 6.21 o -5 5 2 0.85 1.18 4.03 o -4 5 2 0.20 1.62 4.73 o -3 5 2 18.80 15.94 4.12 o -2 5 2 132.00 133.17 7.97 o -1 5 2 2.20 0.94 3.02 o 0 5 2 195.85 209.22 9.90 o 1 5 2 0.00 0.02 0.01 o 2 5 2 24.20 29.24 2.30 o 3 5 2 350.30 334.91 19.82 o 4 5 2 116.80 121.92 6.62 o 5 5 2 305.40 321.84 17.61 o 6 5 2 -2.25 2.64 3.58 o 7 5 2 62.30 55.79 7.90 o 8 5 2 67.20 74.07 9.40 o 9 5 2 49.40 46.86 4.50 o -4 6 2 7.60 8.62 4.80 o -3 6 2 4.40 1.61 3.20 o -2 6 2 0.10 1.85 1.71 o -1 6 2 17.00 14.39 4.20 o 0 6 2 8.10 13.03 2.80 o 1 6 2 17.30 16.23 3.30 o 2 6 2 22.40 20.12 5.30 o 3 6 2 6.10 1.26 5.20 o 4 6 2 5.40 9.49 6.50 o -15 0 3 81.70 73.89 7.80 o -13 0 3 15.70 17.64 2.00 o -11 0 3 3.40 0.36 1.50 o -9 0 3 1196.00 1089.13 25.70 o -7 0 3 295.00 268.21 6.70 o -5 0 3 98.80 122.06 3.60 o -3 0 3 1133.10 1231.39 26.70 o 3 0 3 865.60 852.68 35.90 o 5 0 3 2729.00 2914.65 97.50 o 7 0 3 137.50 133.05 4.10 o 9 0 3 52.30 51.34 2.20 o 11 0 3 146.90 132.07 5.50 o 13 0 3 2.30 1.84 1.40 o 15 0 3 5.30 6.46 2.10 o -16 1 3 5.50 6.43 5.26 o -15 1 3 6.55 2.24 4.74 o -14 1 3 -1.35 0.01 4.12 o -13 1 3 36.35 41.52 3.32 o -12 1 3 62.40 62.39 4.14 o -11 1 3 913.80 846.11 44.70 o -10 1 3 131.30 126.97 5.45 o -9 1 3 0.55 0.18 1.43 o -8 1 3 3.75 1.67 1.10 o -7 1 3 388.35 410.83 10.71 o -6 1 3 137.85 146.97 3.86 o -5 1 3 285.80 287.77 7.22 o -4 1 3 29.00 16.46 1.30 o -3 1 3 483.75 505.33 11.09 o -2 1 3 1160.25 1229.70 30.56 o -1 1 3 938.15 1086.88 20.53 o 0 1 3 924.05 1027.85 32.72 o 1 1 3 1830.35 1900.45 86.09 o 2 1 3 580.90 574.32 25.40 o 3 1 3 78.40 68.93 2.90 o 4 1 3 961.60 1074.99 28.50 o 5 1 3 0.75 0.92 1.50 o 6 1 3 0.55 1.28 1.27 o 7 1 3 101.95 123.84 4.81 o 8 1 3 59.15 56.90 2.86 o 9 1 3 325.65 311.19 10.75 o 10 1 3 18.85 14.41 2.28 o 11 1 3 449.65 438.07 19.05 o 12 1 3 76.40 81.77 4.86 o 13 1 3 60.35 61.80 5.96 o 14 1 3 1.60 1.20 4.72 o 15 1 3 47.15 50.20 4.88 o -15 2 3 29.05 32.74 5.94 o -14 2 3 20.85 25.71 4.51 o -13 2 3 2.40 0.19 3.35 o -12 2 3 19.15 24.94 2.86 o -11 2 3 18.80 15.62 2.71 o -10 2 3 3.00 0.39 1.87 o -9 2 3 139.20 136.22 5.16 o -8 2 3 5.75 5.27 1.53 o -7 2 3 176.95 162.92 5.05 o -6 2 3 1471.60 1394.80 32.51 o -5 2 3 524.25 494.41 20.08 o -4 2 3 81.35 76.37 2.38 o -3 2 3 126.55 125.44 3.26 o -2 2 3 432.40 454.68 11.15 o -1 2 3 309.55 287.05 11.96 o 0 2 3 1044.30 1113.94 26.79 o 1 2 3 206.85 189.50 6.55 o 2 2 3 4.15 0.83 1.42 o 3 2 3 256.45 260.51 8.75 o 4 2 3 613.95 605.34 19.15 o 5 2 3 4.65 6.57 1.41 o 6 2 3 126.65 122.87 7.47 o 7 2 3 142.30 149.12 6.59 o 8 2 3 10.30 7.98 2.84 o 9 2 3 260.40 261.28 11.84 o 10 2 3 91.55 98.45 7.21 o 11 2 3 -2.95 0.61 4.36 o 12 2 3 30.40 22.23 6.33 o 13 2 3 19.00 22.09 2.40 o 14 2 3 16.20 14.75 2.50 o -14 3 3 122.65 129.81 11.11 o -13 3 3 6.60 5.65 4.63 o -12 3 3 93.75 105.42 5.90 o -11 3 3 13.05 12.73 2.46 o -10 3 3 0.50 0.01 2.56 o -9 3 3 2.35 1.99 1.50 o -8 3 3 29.60 33.43 2.06 o -7 3 3 73.90 63.79 3.45 o -6 3 3 7.35 7.64 1.81 o -5 3 3 62.25 66.85 2.43 o -4 3 3 8.05 8.14 1.18 o -3 3 3 358.95 381.33 9.45 o -2 3 3 898.60 831.69 27.52 o -1 3 3 776.25 708.73 24.89 o 0 3 3 36.05 31.72 2.72 o 1 3 3 1.40 0.74 2.60 o 2 3 3 51.75 43.32 2.51 o 3 3 3 182.30 159.45 8.51 o 4 3 3 158.50 148.01 5.51 o 5 3 3 8.35 6.94 2.60 o 6 3 3 6.10 5.88 1.66 o 7 3 3 201.10 190.52 6.42 o 8 3 3 207.45 191.87 7.23 o 9 3 3 72.70 68.92 3.47 o 10 3 3 -0.55 1.44 3.42 o 11 3 3 8.15 5.15 2.61 o 12 3 3 24.85 34.93 3.41 o 13 3 3 21.10 24.68 3.00 o -12 4 3 51.70 69.56 5.00 o -11 4 3 49.85 62.05 4.49 o -10 4 3 62.10 67.96 4.75 o -9 4 3 244.15 255.98 10.85 o -8 4 3 611.95 590.79 20.75 o -7 4 3 13.70 12.64 1.94 o -6 4 3 251.75 232.16 8.75 o -5 4 3 5.55 5.06 1.36 o -4 4 3 2.50 2.79 2.68 o -3 4 3 2.20 2.99 2.13 o -2 4 3 22.90 22.64 1.30 o -1 4 3 -0.85 1.66 1.89 o 0 4 3 58.40 56.67 3.70 o 1 4 3 16.90 12.07 3.47 o 2 4 3 472.60 471.45 11.90 o 3 4 3 73.80 68.72 5.52 o 4 4 3 0.80 3.31 1.96 o 5 4 3 26.60 27.24 2.35 o 6 4 3 82.70 92.34 4.86 o 7 4 3 4.50 4.65 2.00 o 8 4 3 138.20 135.43 6.01 o 9 4 3 76.55 68.96 4.59 o 10 4 3 23.55 30.64 4.33 o 11 4 3 -0.30 0.42 3.65 o -9 5 3 3.00 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