Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 60| Part 12

ISSN: 2056-9890

December 2004 issue

Highlighted illustration

Cover illustration: Isonicotinamide forms a complex with propionic acid in an unusual 1:2 stoichiometry. The crystal structure contains a variety of hydrogen bonds and other intermolecular interactions. See Oswald, Motherwell & Parsons [Acta Cryst. E60, o2380-o2383].

inorganic compounds

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Ce₂Ru₃Al₁₅, an intermetallic compound of a new structure type

A. I. Tursina, S. N. Nesterenko, E. V. Murashova, I. V. Chernyshev, H. Noël and Y. D. Seropegin

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Cs₃TaS₄

B. Deng and J. A. Ibers

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The layered gallium borophosphate Ga[B₂P₂O₇(OH)₅] refined from X-ray powder data

S.-Y. Mao, J.-X. Mi, L. G. Akselrud, Y.-X. Huang, J.-T. Zhao and R. Kniep

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metal-organic compounds

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Poly[[terachlorogold(III)potassium(I)(Au—K)]-μ-4,4′-bipyridine]

C. Song, Y.-Z. Li, Y.-Q. Chen, S.-J. Xiao and X.-Z. You

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catena-Poly[[aquanitritosilver(I)]-μ-1,4-diazabicyclo[2,2,2]octane-κ²N:N′]

Z.-L. You, H.-L. Zhu and W.-S. Liu

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Bis(μ-9-oxidofluorene-9-carboxylato-κ³O,O′:O)bis[aqua(1H-imidazole-κN³)copper(II)] methanol solvate

L.-H. Huo, S. Gao, H. Zhao and S. W. Ng

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Bis(butane-2,3-dione monooxime benzoylhydrazone-κ³O,N,N′)nickel(II) sulfate salicylhydroxamic acid

S. Gao, L.-H. Huo, H. Zhao and S. W. Ng

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μ-3,4,5,6-Tetrafluorophthalato-bis[tris(2-methyl-2-phenylpropyl)tin(IV)]

L.-J. Tian, Y.-X. Sun and S. W. Ng

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Aqua(benzene-1,3-dioxyacetato-κO)tetrakis(1H-imidazole-κN³)nickel(II) monohydrate

S. Gao, J.-W. Liu, L.-H. Huo, H. Zhao and J.-G. Zhao

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(N-Benzoyl-N-phenylhydroxaminato-κ²O,O′)(salicylaldehyde isonicotinoylhydrazonato-κ³O,N,N′)vanadium(IV) hexane hemisolvate

S. Gao, L.-H. Huo, H. Zhao and S. W. Ng

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Bis(2,2′:6′,2′′-terpyridyl-κ³N)manganese(II) dinitrate dihydrate

A. Rompel, A. D. Bond and C. J. McKenzie

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Bis(acetato-κO)[bis(2-pyridylmethyl)amine-κ³N,N′,N′′]zinc(II)–acetic acid (1/2)

R. S. Baker and R. E. Norman

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Tetra-μ-methacrylato-κ⁸O:O′-bis[(pyridine-κN)copper(II)]

B. Wu and G. Wang

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Di-μ-chloro-bis[chloro(η⁶-1,2,4-trimethylbenzene)ruthenium(II)]–dichloromethane (3/2)

B. Therrien and G. Süss-Fink

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catena-Poly[[[aqua(1,10-phenanthroline-κ²N,N′)copper(II)]-μ-benzene-1,3-dioxyacetato-κ²O:O′] dihydrate]

S. Gao, J.-W. Liu, L.-H. Huo, H. Zhao and J.-G. Zhao

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[N,N′-Bis(1-{[2-oxido-4-(2-hydroxyethoxy)phenyl]methyl}ethylidene)ethane-1,2-diamine]copper(II)

G. Usha, S. Selvanayagam, D. Velmurugan, K. Ravikumar, N. S. Kumar, A. Raghavan and A. S. Nasar

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2,2′-Bipyridyl-2-ium aqua(2,2′-bipyridyl-κ²N,N′)tetakis(nitrato-κ²O,O′)praseodymium(III) 2,2′-bipyridyl hemisolvate

I. A. Charushnikova and C. Den Auwer

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cis-Diaquamalonato(1,10-phenanthroline)manganese(II)

Q.-Z. Zhang and C.-Z. Lu

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Bis(tetraphenylarsonium) tris(2-thioxo-1,3-dithiole-4,5-dithiolato)stannate(IV) acetone solvate at 120 K

N. M. Comerlato, G. B. Ferreira, R. A. Howie and J. L. Wardell

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4,4′-Bipyridinium hexaaquacobalt(II) disulfate

X.-H. Li, Q. Miao, H.-P. Xiao and M.-L. Hu

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Rerefinement of tris(dimethylammonium) dodecamolybdophosphate in the space group R $\overline 3$ m

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catena-Poly[[[tris(pyridine-κN)cadmium(II)]-μ-{2-[3-(1-carboxylatomethyl)-4-nitrophenyl]propionato-κ²O,O′}] dihydrate]

S. Gao, L.-H. Huo, X.-F. Zhang and S. W. Ng

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Tetraaquabis(4-carboxy-1H-imidazole-5-carboxylato-κ²N,O)calcium(II) monohydrate

S. Gao, X.-F. Zhang, L.-H. Huo and H. Zhao

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Bis(9-hydroxyfluorene-9-carboxylato-κ²O,O′)tripyridinecadmium(II)

S. Gao, L.-H. Huo, Z.-Z. Lu and H. Zhao

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(η⁵-Cyclopentadienyl)(η⁶-9H-fluorene)iron(II) hexafluorophosphate

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The infinite one-dimensional polymer catena-poly[[aquabis(p-nitrobenzoato-κO)copper(II)]-μ-1,4-diazabicyclo[2.2.2]octane-κ²N:N′]

Z.-D. Lin and J.-Y. Lu

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{2-[2′-(Diethylcarbamoylmethoxy)-1,1′-binaphth-2-yloxy]-N,N-diethylacetamide-κ⁴O}(2,4,6-trinitrophenolato)manganese(II)

Y.-W. Wang, Y.-L. Guo, W.-S. Liu and K.-B. Yu

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Bis(1,10-phenanthroline)(pyridine-2,6-dicarboxylato)cadmium(II)–pyridine–2,6-dicarboxylic acid–water (1/1/4)

F. Ramezanipour, H. Aghabozorg, S. Sheshmani, A. Moghimi and H. Stoeckli-Evans

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1,1′-Dibromoferrocene

C. A. Hnetinka, A. D. Hunter, M. Zeller and M. J. G. Lesley

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trans-Bis{1-[3-(cyclohexylamino)propyliminomethyl]-2-naphtholato}copper(II) dichloride dihydrate

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Diazidobis(2,2′-bipyridine)zinc(II) monohydrate

F. Jian, C. Li, P. Sun and H. Xiao

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A cyclic dipalladium compound formed by concomitant N–C coupling and [2+3]-cycloaddition: bis{μ-1-[4-(carbodiimido)phenyl]tetrazolato-κ²N:C⁵}bis[bis(trimethylphosphine-κP)palladium(II)]

W. S. Han, H. K. Lee, Y.-J. Kim and S. W. Lee

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trans-Diaquabis[4-(4-methylphenyl)-3,5-bis(2-pyridyl)-4H-1,2,4-triazole]nickel(II) diperchlorate tetrahydrate

S.-C. Shao, Z.-D. Liu and H.-L. Zhu

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A new chalcocyanide cubane rhenium salt: tetrakis(tetraphenylphosphonium) dodecacyano-hexahedro-tetratelluriumtetrarhenate(IV) trihydrate

O. A. Efremova, Y. V. Mironov, N. V. Kuratieva and V. E. Fedorov

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Monopotassium octapyridinium tris[hexachlorobismuthate(III)]

H. Zhang and L. Fang

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Tris(1,10-phenanthroline-κ²N,N′)iron(III) trinitrate monohydrate

M. Odoko and N. Okabe

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(Oxalato-κ²O,O′)(1,10-phenanthroline-κ²N,N′)palladium(II) monohydrate

M. Odoko, Y. Wang and N. Okabe

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Pentacarbonyl(3,3′,4,4′-tetramethyl-1,1′-diphosphaferrocene-κP)tungsten(0)

L. Sieroń and A. Tosik

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catena-Poly[[[diaquabis(3-hydroxypyridine-κN)cobalt(II)]-μ-(4-carboxylatophenoxy)acetato-κ²O:O′] monohydrate]

S. Gao, C.-S. Gu, L.-H. Huo, J.-W. Liu and J.-G. Zhao

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Bis(μ-4-sulfobenzoato-κ²O:O′)bis[aqua(2,2′-bipyridine-κ²N,N′)copper(II)]

S.-R. Fan, H.-P. Xiao, L.-P. Zhang and L.-G. Zhu

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The sterically crowded four-coordinate copper(I) complex rac-bis[2,2′-bis(1-ethyl-1H-benzimidazol-2-yl)biphenyl]copper(I) trifluoromethanesulfonate toluene solvate dihydrate

R. T. Stibrany, H. J. Schugar and J. A. Potenza

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{4,4′-Di-tert-butyl-6,6′-bis(dimethoxymethyl)-2,2′-[propane-1,3-diylbis(nitrilomethylidyne)]bis(thiophenolato)-κ⁴S,N,N′,S′}nickel(II)

J. K. Bjernemose, C. J. McKenzie, P. R. Raithby and S. J. Teat

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Di-μ-chloro-bis[(N-tert-butylimido)chlorobis(pyridine-κN)titanium(IV)] perdeuterobenzene disolvate

N. Hazari, A. R. Cowley and P. Mountford

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(cis-syn-cis-Dicyclohexano-18-crown-6)potassium chlorochromate

S. A. Kotlyar, R. I. Zubatyuk, M. V. Zhigalko, O. V. Shishkin, G. N. Chuprin, A. V. Kiriyak and G. L. Kamalov

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Poly[triaqua(μ-benzene-1,3-dioxyacetato)manganese(II)]: a two-dimensional manganese(II) coordination polymer

S. Gao, J.-W. Liu, L.-H. Huo, H. Zhao and J.-G. Zhao

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catena-Poly[[(1,10-phenanthroline-κ²N,N′)copper(II)]-μ-4-carboxyimidazole-5-carboxylato(2–)-κ⁴N,O:N′,O′]

C.-S. Gu, S. Gao, L.-H. Huo, H. Zhao and J.-G. Zhao

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Chloro{2-[(5-nitrosalicylidene)aminoethyl]-1H-benzimidazole}copper(II)

X.-.H. Qiu and H.-Y. Wu

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Tetra-n-butylammonium μ-bromo-di-μ-cyclohexanethiolato-bis[tricarbonylmolybdenum(I)]

Z.-F. Zhou, Y.-Q. Wei, B.-T. Zhuang, K.-C. Wu, C.-Y. Mang, T. Hong and M.-X. Zhang

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Dichlorobis(pyridinium-2-thiolato)cadmium(II)

X.-J. Wang, Q.-L. Ni, X.-S. Bi and H.-X. Jian

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Dichlorobis(triphenylphosphine oxide-κO)nickel(II)

R. Moreno-Fuquen, O. Cifuentes, J. V. Naranjo, L. M. Serratto and A. R. Kennedy

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Bis(μ-4-chlorobenzoato-κ²O:O′)bis[(2-aminopyridine-κN)silver(I)](Ag—Ag) monohydrate

Z.-L. You, H.-L. Zhu and W.-S. Liu

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(μ-Biphenyl-4,4′-dicarboxylato)bis[(2-aminopyridine)silver(I)]

Z.-D. Liu and H.-L. Zhu

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catena-Poly[[bis(ethylenediamine-κ²N,N′)copper(II)]-μ₃-1,2-dicyanoethylenedithiolato-κ⁴N:S,S′:N′-[(1,2-dicyanoethylenedithiolato-κ²S,S′)cuprate(II)]]

A.-Y. Fu, D.-Q. Wang and D.-Z. Sun

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Tris(ethylenediamine-κ²N,N′)cadmium(II) bis(1,2-dicyanoethylenedithiolato-κ²S,S′)cuprate(II)

D.-Q. Wang, A.-Y. Fu and X.-L. Wei

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Poly[cadmium(II)-μ₄-benzene-1,3-dioxyacetato]: a two-dimensional layer cadmium(II) coordination polymer

S. Gao, J.-W. Liu, L.-H. Huo, H. Zhao and J.-G. Zhao

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Poly[[bis(1H-imidazole-κN³)cadmium(II)]-μ₃-benzene-1,3-dioxyacetato]

S. Gao, J.-W. Liu, L.-H. Huo, H. Zhao and J.-G. Zhao

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Isopropoxy[2′-(2-methoxybenzoyl)-2-oxidobenzohydrazidato]oxovanadium(V)

L.-J. Chen, M.-X. Yang and S. Lin

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catena-Poly[[μ-ethylenediamine-κ²N:N′-bis[(ethylenediamine-κ²N,N′)silver(I)] bis[silver(I)-μ-barbiturato-κ²N:N′]] dihydrate]

Z.-D. Liu and H.-L. Zhu

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Bis(tetraethylammonium) bis(2-thioxo-1,3-dithiole-4,5-dithiolato)cadmium(II)

T. B. Li, W. T. Yu, D. Xu, X. Q. Wang and G. H. Zhang

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Bis(3,5-dimethyl-1,2,4-triazolato-κN⁴)bis(pivalic acid-κO)copper(II) dihydrate

J.-H. Zhou, Y.-Z. Li, B. Huang and X.-T. Chen

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Aquapentakis(1H-imidazole-κN³)cobalt(II) dibromosuccinate

D.-X. Li, D.-J. Xu and Y.-Z. Xu

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Dichloro[(4S,4′S)-4,4′-diisopropyl-2,2′-bi-1,3-oxazoline]palladium(II)

J. Kožíšek, M. Fronc, I. Svoboda, P. Kapitán and T. Gracza

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catena-Poly[[[μ-di-4-pyridyldiazene-κ²N⁴:N^4′-bis[(triphenylphosphine-κP)copper(I)]]-μ-pyridine-2-carbaldehyde azine-κN²,N:N′,N^2′] bis(tetrafluoroborate)]

M.-M. Yu, W.-F. Fu, Z.-X. Li, Z.-F. Yao and L.-F. Jia

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A linear trinuclear Co^II–Co^II–Co^II complex with μ-acetate bridges: di-μ-acetato-bis[μ-N,N′-bis(salicylidene)-1,4-butanediaminato]tricobalt(II)

Z.-L. You, H.-L. Zhu and W.-S. Liu

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A silver(I) complex with Ag⋯Ag interactions: diamminesilver(I) p-nitrobenzoate

Z.-L. You, H.-L. Zhu and W.-S. Liu

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catena-Poly[[aqua(2,2′-bipyridine-κ²N,N′)zinc(II)]-μ-4-carboxylatophenoxyacetato-κ³O,O′:O′′]

S. Gao, C.-S. Gu, L.-H. Huo, J.-W. Liu and J.-G. Zhao

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[η⁶-2-(2-Methylbenzoyloxy)ethyl methacrylate]bis(η⁶-1,2,4,5-tetramethylbenzene)tri-μ-hydrido-μ₃-oxo-triruthenium(II)(3 Ru—Ru) tetrafluoroborate

L. Vieille-Petit, B. Therrien, A. Buryak, K. Severin and G. Süss-Fink

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catena-Poly[[bis(O,O′-diethyl dithiophosphato-κ²S,S′)cadmium(II)]-μ-4,4′-bipyridine-N:N′]

T. Li, Z.-H. Li and S.-W. Du

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Tris(ethylenediamine-κ²N,N′)zinc(II) bis(1,2-dicyanoethylenedithiolato-κ²S,S′)cuprate(II)

D.-Q. Wang, A.-Y. Fu and J.-Y. He

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Dibromobis[pyridine-2(1H)-thione-κS]cadmium(II)

X.-J. Wang, Q.-L. Ni and Z.-S. Shen

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The first adduct of bis(1,3-diphenyl-1,3-propanedionato)oxovanadium(IV)

E. Meštrović, D.-K. Bučar, I. Halasz and V. Stilinović

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Tetraethylammonium [1-methylimidazole-2(3H)-thione]copper(I)-di-μ-sulfido-dioxotungstate(VI)

A. Beheshti, N. R. Brooks, W. Clegg and R. Khorrmdin

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Chloro[2-(1-ethyl-1H-benzimidazol-2-yl)phenol-κN³][2-(1-ethyl-1H-benzimidazol-2-yl)phenolato-κ²N³,O]zinc(II)

Y.-P. Tong and B.-H. Ye

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Aqua(pyridine N-oxide-κO)[tris(2-hydroxyaminopropyl)amine-κ⁴N]nickel(II) dinitrate

S. E. Edison, J. A. Krause Bauer and M. J. Baldwin

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Bis(μ-3-carboxylatophenoxyacetato)bis[(1H-imidazole)copper(II)] dihydrate

S. Gao, C.-S. Gu, L.-H. Huo, J.-W. Liu and J.-G. Zhao

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A two-dimensional coordination polymer containing copper(II): poly[[(1H-benzimidazole-κN³)copper(II)]-μ₃-3-carboxylatophenoxyacetato-κ⁴O,O′:O′′:O′′′]

S. Gao, C.-S. Gu, L.-H. Huo, J.-W. Liu and J.-G. Zhao

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Tris(ethylenediamine-κ²N,N′)zinc(II) bis(1,2-dicyanoethylenedithiolato-κ²S,S′)nickelate(II)

A.-Y. Fu, D.-Q. Wang and T. Yu

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Bis[4-chloro-2-(2-hydroxyethyliminomethyl)phenolato-κ²N,O]copper(II)

H. Liu, H. Wang, D. Niu and Z. Lu

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Poly[sodium(I)-μ₃-bis(ethylenedioxy)borato]

G. J. Gainsford and T. Kemmitt

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Diaquabis(pyridine-2-carboxamide-κ²N¹,O²)copper(II) squarate

İ. Uçar, A. Bulut, O. Z. Yeşilel, H. I. Ölmez and O. Büyükgüngör

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A redetermination of cis-aquabis(glycinato-κ²N,O)copper(II)

B. M. Casari, A. H. Mahmoudkhani and V. Langer

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Bis(tetra-n-butylammonium) tetrakis[chloro(μ₃-sulfido)copper(I)]tungstate(VI): a second polymorph

M. Hossaini Sadr, S. M. Seyed Ahmadian, N. R. Brooks and W. Clegg

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(2,2′-Bipyridine)bromodiimidazolecopper(II) bromide

F.-Y. Xia, X.-H. Li and X.-X. Lei

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trans-Diaquabis{2-[3-(dimethylamino)prop-2-enoyl]pyridine}nickel(II) bis(tetrafluoroborate) dimethylformamide tetrasolvate

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μ-Oxo-bis(μ-2-furancarboxylato)bis{[N-methyl-N,N-bis(2-pyridylmethyl)amine]iron(III)} bis(perchlorate) methanol solvate

A. Nielsen, A. D. Bond and C. J. McKenzie

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Ferrocenylbenzoic acid

F. Jian, H. Ma, P. Sun and H. Xiao

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[2,6-Bis(2-pyridylamino)pyridine]dichlorocadmium(II)

L. Huang, S.-H. Tang, X.-N. Fang and X.-R. Zeng

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cis-Dicarbonyl(hydroxydi-2-pyridylmethanolato-κ³N,O,N′)(triphenylphosphine-κP)rhenium(I) dimethyl sulfoxide hemisolvate

M. Bakir and I. Hassan

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Poly[[aqua(1,10-phenanthroline-κ²N,N′)copper(II)]-μ-4-sulfonatobenzoato-κ²O⁴:O¹]

S.-R. Fan, H.-P. Xiao, L.-P. Zhang, G.-Q. Cai and L.-G. Zhu

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Bis[2-(benzylamino)pyridine-κN]silver(I) perchlorate

C.-Q. Wan, Q.-S. Li, H.-B. Song, F.-B. Xu and Z.-Z. Zhang

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μ-4,4′-Bipyridine-bis[aqua(N-salicylideneaspartato)copper(II)]

B.-Y. Lou, D.-Q. Yuan, B.-L. Wu and M.-C. Hong

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A dimeric tellurastannoxane carbonate cluster, tetra-tert-butyl-di-μ₃-carbonato-tetrakis[4-(N,N-dimethylamino)phenyl]di-μ-oxo-ditelluriumditin chloroform tetrasolvate

J. Beckmann, D. Dakternieks, A. Duthie and C. Mitchell

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Bis[4-amino-3-methyl-1H-1,2,4-triazole-5(4H)-thione]dichlorocopper(II) dihydrate

X.-Q. Cai, L.-X. Zhang, G.- Xiang, A.-J. Zhang and M.-L. Hu

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catena-Poly[[[diaquacobalt(II)]-μ-tartrato-κ⁴O,O′:O′′,O′′′] monohydrate]

D.-X. Li, D.-J. Xu and Y.-Z. Xu

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A novel coordination mode for a phospholyl ligand: μ-phosphindolyl-κ²P:P-μ-1-phenyl-phosphindolyl-κ²C²:P-bis[tetracarbonylmanganese(I)]

A. Decken, B. E. Wilkins and F. Bottomley

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Hexaaquamagnesium(II) bis[(4-oxo-4H-pyridin-1-yl)acetate] dihydrate

J.-G. Zhao, Z.-Y. Zhang, L.-H. Huo and S. Gao

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organic compounds

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Hyperolactone C

S. L. Crockett, W. Schühly, F. Belaj and I. A. Khan

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1-(Diphenylphosphinoyl)-3,3-dimethylbut-1-yne

J.-M. Gu, M.-S. Xu and X.-R. Hu

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1-Ethoxy-4-nitrobenzene

B. McBurney, P. C. D. Foss, E. M. Reed, T. D. Shine, N. M. Glagovich, B. L. Westcott, G. Crundwell, M. Zeller and A. D. Hunter

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4-Fluorobenzaldehyde picoloylhydrazone

S.-C. Shao, Z.-L. You, S.-H. Fan, L.-L. Tang, Y.-S. Lin and H.-L. Zhu

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2-Nitrobenzaldehyde picoloylhydrazone

S.-C. Shao, Z.-L. You, S.-H. Fan, L.-L. Tang, Z.-D. Xiong and H.-L. Zhu

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Pyridine-2-carboxaldehyde picoloylhydrazone

S.-C. Shao, Z.-L. You, L.-L. Tang, Y.-S. Lin and H.-L. Zhu

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2-Nitrobenzaldehyde salicylhydrazone

S.-C. Shao, Z.-L. You, Z.-D. Xiong, B. Chen and H.-L. Zhu

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2,6-Difluorobenzonitrile

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4-[(Z)-(4-Methoxyanilino)phenylmethylene]-5-methyl-2-phenyl-2H-pyrazol-3(4H)-one

F. Bao, X.-Q. Lü, Y.-Q. Qiao, Q. Wu and S. W. Ng

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A monoclinic modification of N-(3,4-dibenzoyl-2,5-dimethylpyrrol-1-yl)-4-methoxybenzamide

S. Gao, L.-H. Huo and S. W. Ng

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Rerefinement of the co-crystal of 4-hydroxypyridine with 4-hydroxypyridinium nitrate

S. Gao, Z.-Z. Lu, L.-H. Huo, S. M. Zain and S. W. Ng

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Ethylenediammonium bis(3-carboxy-4-hydroxybenzenesulfonate) tetrahydrate

S. Gao, L.-H. Huo and S. W. Ng

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1,5-Dimethyl-4-[(4-nitrobenzylidene)amino]-2-phenyl-2,3-dihydro-1H-pyrazol-3-one

Z.-X. Li and X.-L. Zhang

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p-Tolyl 2,3-anhydro-5,6-O-isopropylidene-1-thio-β-D-gulofuranoside

Y. Bai, T. L. Lowary and M. J. Ferguson

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Pentafluorophenylboronic acid

P. N. Horton, M. B. Hursthouse, M. A. Beckett and M. P. Rugen-Hankey

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2-(2-Fluoro-5-methylbenzoyl)-N-phenyl-2-(1H-1,2,4-triazol-1-yl)ethanethioamide

L.-Z. Xu, Y.-Q. Qin, C.-Y. Zhu, S.-H. Yang and K. Li

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1,1-Diphenyl-2,2-bis(trimethylsilylethynyl)ethene

H. Berger, P. Bubenitschek, H. Hopf and P. G. Jones

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(3aS,8aS,9R,9aS)-9-Hydroxy-2,3,3a,7,8,8a,9,9a-octahydrofuro[3,2-f]indolizin-6(4H)-one

V. Vrábel, J. Kožíšek, V. Langer, Š. Marchalín and F. Szemes

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[1-(Diphenylphosphinoyl)propa-1,2-dienyl]benzene

W.-M. Xu, X.-R. Hu and J.-M. Gu

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1′-Methyl-2′′-phenylcyclohexane-1-spiro-4′-[acenaphthene-1-spiro-2′-pyrrolidine-3′-spiro-4′′(5′′H)-[1,3]oxazole]-2,5′′-dione

S. Selvanayagam, D. Velmurugan, K. Ravikumar, J. Jayashankaran, R. R. Durga and R. Raghunathan

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Pyridazine-3,6-dicarboxylic acid monohydrate

W. Starosta and J. Leciejewicz

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2-Hydroxy-2-phenyl-4,7-dihydroisophosphindolinium chloride

A. Decken, E. D. Gill and F. Bottomley

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Mycophenolate mofetil

H. S. Yathirajan, B. Nagaraj, S. L. Gaonkar, R. S. Narasegowda, P. Nagaraja and M. Bolte

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1-(4-Fluorophenyl)-1,3-dihydroisobenzofuran-5-carbonitrile

H. S. Yathirajan, B. Nagaraj, S. L. Gaonkar, R. S. Narasegowda, P. Nagaraja and M. Bolte

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A monoclinic polymorph of isoxsuprine hydrochloride

H. S. Yathirajan, B. Nagaraj, R. S. Narasegowda, P. Nagaraja and M. Bolte

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Diphenyl 2-(α,α,4-trichlorobenzyl)phenyl phosphate

A. G. Pinkus, K. K. Klausmeyer, R. P. Feazell, L. Y. C. Meng and T. C. Chang

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Bis[3-(trimethylsilyl)propyl] methylenebisphosphonate

C. C. McLauchlan, D. C. Stepinski and A. W. Herlinger

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A low-temperature redetermination of the monoclinic β-form of cyclooctaselenium

T. Maaninen, J. Konu and R. S. Laitinen

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2,6-Dimethyl-4H-1-benzopyran-4-one

B. Arslan, C. Kazak and H. Göker

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A new amine phosphate templated by tris(2-aminoethyl)amine

A. Dakhlaoui, L. S. Smiri and A. Driss

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4-(4-Methylphenyl)-3-(4-pyridyl)-4H-1,2,4-triazole

L. Mazur, A. E. Koziol and B. Modzelewska-Banachiewicz

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(Z)-3,6-Diethynyl-3,6-dihydroxycyclohexa-1,4-diene

A. Bandyopadhyay, B. Varghese and S. Sankararaman

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6-(2,4-Difluorophenyl)-3-(3-methylphenyl)-7H-1,2,4-triazolo[3,4-b][1,3,4]thiadiazine

G.-Q. Xiang, L.-X. Zhang, A.-J. Zhang, X.-Q. Cai and M.-L. Hu

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4-(Dimethylamino)pyridinium 2-butoxy-3-dicyanomethylene-4-oxocyclobut-1-en-1-olate

R. I. Zubatyuk, V. N. Baumer, A. L. Tatarets, L. D. Patsenker and O. V. Shishkin

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Ethyl 5-(5-oxo-2,3-dihydro-5H-oxazolo[2,3-a]isoindol-9b-ylmethyl)-4-(2,5,5-trimethyl-1,3-dioxan-2-yl)isoxazole-3-carboxylate: the product of a novel synthetic method

J. Nelson, B. Twamley and N. R. Natale

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2,2′:6′,2′′-Terpyridine N,N′,N′′-trioxide

S. E. McKay, K. A. Wheeler and S. C. Blackstock

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A synthetic fragment of a cyclic depsipeptide, aureobasidine A: tert-butoxycarbonyl-L-allo-isoleucyl-N-methyl-L-valine (Boc-L-allo-Ile-L-MeVal-OH)

H. Oku, R. Naito, K. Yamada and R. Katakai

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7b-tert-Butyl-1a,2,5,6-tetrahydro-2-hydroxy-2-methyl-4H-oxireno[2,3-h]chromen-3(7bH)-one

C.-H. Mao, H.-B. Song, Q.-M. Wang, R.-Q. Huang, L. Chen and J. Shang

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Methyl 4-[(2-butyl-4-chloro-5-formyl-1H-imidazol-1-yl)methyl]benzoate

F. Yang, H. Xiao and F. Jian

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6-Chloro-2,3,4,5-tetrahydro-7,8-dimethoxy-1-(4-methoxyphenyl)-1H-3-benzazepine

J. Yan and D. Cheng

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[2-(Dimethylamino)benzyl][(N–B)-2-(dimethylammonio)benzyl]phenylborate

H.-B. Tong, X.-H. Wei, D.-S. Liu and S.-P. Huang

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Prop-2-ynyl 1,2,3,4-tetra-O-acetyl-β-D-glucopyranuronate

D. P. Temelkoff, P. Norris and M. Zeller

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1,1′,8,8′-Tetramethoxy-10,10′-bianthrone

Z.-W. Shi, Y.-Z. Li, Y. Li, G.-Y. Lu and S.-H. Liu

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7-Methoxy-2,3-dihydro-1H-cyclopenta[b]chromen-1-one

F. Huo, C. Yin and P. Yang

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3-Benzyl-4-(4-methylphenyl)-1H-1,2,4-triazole-5(4H)-thione

S. Ö. Yıldırım, M. Akkurt, M. Koparır, A. Cansız, M. Şekerci and F. W. Heinemann

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4,5-Bis(benzoylsulfanyl)-1,3-dithiol-2-one

N. M. Comerlato, G. B. Ferreira, J. M. S. Skakle and J. L. Wardell

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C—H⋯N contacts in 4-phenyl-3-(4-pyridyl)-4H-1,2,4-triazole

L. Mazur, A. E. Koziol and B. Modzelewska-Banachiewicz

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N-[(1S,2S,3R)-2-Bromo-3-(tert-butyldiphenylsilyloxy)-1-phenyl-4-(phenylsulfonyl)butyl]-4-methylbenzenesulfonamide

K. Ravikumar, G. Y. S. K. Swamy, S. Raghavan and C. Naveenkumar

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4-(1,3-Dioxoisoindolin-2-yl)benzaldehyde

X.-G. Liu, Y.-Q. Feng, P. Wu, X. Chen and F. Li

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2-Acetamido-4,5-dinitrotoluene: a test molecule for the CCDC `Blind Structure Prediction Test, 2004'

D. J. Watkin, W. D. S. Motherwell, R. I. Copper and S. Pantos

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1-(2-Pyridyl)pyrrolidine-2-thione

M. S. Datt, C. B. Koning, M. A. Fernandes and J. P. Michael

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N,N,N-Tris(3-methylphenyl)amine

T. Manifar, S. Rohani and M. Jennings

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2-(4-tert-Butylbenzyl)-3-phenylinden-1-one

J. W. Karban, J. L. Morgan, J. M. Dees and K. K. Klausmeyer

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N-Cyclohexyl-2-oxo-2H-1-benzopyran-3-carboxamide

N. E. Magaña-Vergara, F. J. Martínez-Martínez, I. I. Padilla-Martínez, H. Höpfl and E. V. García-Báez

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1,3-Bis(3,4-dicyanophenoxy)benzene

Ö. Deveci, Ş. Işık, M. Yavuz, N. Akdemir, E. Ağar and C. Kantar

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1,4-Bis(2-pyridylsulfanyl)butane

Y.-B. Xie and J.-R. Li

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2-(4-Chlorophenyl)-5-methyl-7,8-dihydro-6H-cyclopenta[e][1,3]oxazolo[3,2-a]pyridin-9-ium perchlorate

D. V. Albov, V. B. Rybakov, E. V. Babaev and L. A. Aslanov

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(1R,5S,8R)-1,8-Dihydroxy-6-oxa-3-azabicyclo[3.2.1]octan-2-one

F. Punzo, D. J. Watkin, M. I. Simone and G. W. J. Fleet

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4,4′-Dithiodiphenol: a chain of rings generated by two pairs of O—H⋯O hydrogen bonds

Q.- Ni, X.-J. Wang, J.-Q. Zeng and H.-X. Jian

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5-(2-Chlorobenzoyl)-1,3-benzoxazol-2(3H)-one

Ş. Işık, Y. Köysal, M. Yavuz, M. Köksal and H. Erdoğan

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6-Benzylamino-2-(2-hydroxyethylamino)-9-methylpurine-1,7-diium bis(perchlorate) monohydrate

Z. Trávníček and V. Kryštof

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10-Cyclopropyl-9-(4-hydroxy-3-methoxyphenyl)-3,3,6,6-tetramethyl-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione

S. Tu, X. Zhang and J. Xu

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1,8-Anthraquinono-18-crown-5 monohydrate

E. Weber, D. Kunze and W. Seichter

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3-Azido-3-deoxy-2,2′:5,6-di-O-isopropylidene-2-C-hydroxmethyl-D-gulono-1,4-lactone

C. C. Harding, H. Shallard-Brown, D. J. Watkin, R. Soengas and G. W. J. Fleet

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16α,17-Epoxy-4-pregnene-3,20-dione

S. Wang, Y. Wang, Q. Nie, L. Zhou and J. Wu

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2-Amino-4-(3,4-dichlorophenyl)-4H-pyrano[3,2-c]coumarin-3-carbonitrile N,N-dimethylformamide solvate

D. Shi, N. Wu, Q. Zhuang and Y. Zhang

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3-[(4-Bromo-2-thienyl)methylenehydrazinocarbonyl]-1H-1,2,4-triazole

J.-G. Yang and F.-Y. Pan

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1-[(2,4-Dichlorobenzoyl)methyl]-4-(N,N-dimethylamino)pyridinium bromide

T. V. Sundar, V. Parthasarathi, K. Sarkunam, M. Nallu, B. Walfort and H. Lang

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3,5,7-Triaza-1-azoniatricyclo[3.3.1.1^3,7]decane perchlorate

R. Kruszynski and A. Trzesowska

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Trimethoprim–hydrogen malonate (1/1)

M. Hemamalini, P. T. Muthiah and R. J. Butcher

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2,4-Bis(pyridine-2-carbonyl)-1-(2-pyridyl)-3,5-di-p-tolylcyclohex-1-ol

K. R. Krishnapriya, N. Sampath, S. Aravindhan, M. N. Ponnuswamy and M. Kandaswamy

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1-Ethyl-4-hydroxyquinolin-2(1H)-one

V. N. Baumer, O. V. Shishkin, I. V. Ukrainets, L. V. Sidorenko and S. A. E. Kayal

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2-Amino-4-(4-methoxyphenyl)-5-oxo-4H,5H-pyrano[3,2-c]chromene-3-carbonitrile N,N-dimethylformamide solvate

D.-Q. Shi, N. Wu, Q. Zhuang and Y. Zhang

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Ethyl 2-amino-4-(4-methoxyphenyl)-7-methyl-5-oxopyrano[3,2-c]pyran-3-carboxylate

D.-Q. Shi, L.-H. Niu, X.-S. Wang, Q.-Y. Zhuang and Y. Zhang

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9-[Ethoxy(8-quinolylamino)methyl]anthracene

B. Huang, Y.-Z. Li, J.-H. Zhou, X.-T. Chen and S.-H. Liu

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3-(2-Furyl)-4-(4-methoxyphenyl)-1H-1,2,4-triazole-5(4H)-thione

S. Ö. Yıldırım, M. Akkurt, M. Koparır, A. Cansız, M. Şekerci and F. W. Heinemann

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2-Amino-7-methyl-4-(3,4-methylenedioxyphenyl)-5-oxopyrano[3,2-c]pyran-3-carbonitrile N,N-dimethylformamide solvate

D.-Q. Shi, L.-H. Niu, X.-S. Wang, Q.-Y. Zhuang and Y. Zhang

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(E)-N¹-[(6-Chloropyridin-3-yl)methyl]-N²-cyano-N¹-methylacetamidine

D. Chopra, T. P. Mohan, K. S. Rao and T. N. Guru Row

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N-(3-Fluorophenyl)-9H-xanthen-9-ylideneamine

D. Chopra, K. Nagarajan and T. N. Guru Row

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1,2,4,5-Tetrakis(2-tert-butyl-4-methylphenoxymethyl)benzene

B. Arslan, C. Kazak, N. Akdemir, C. Kantar and E. Ağar

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A 1:2 co-crystal of isonicotinamide and propionic acid

I. D. H. Oswald, W. D. S. Motherwell and S. Parsons

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tert-Butyl diphenylphosphinate

I. D. Grice, I. D. Jenkins, W. K. Busfield, K. A. Byriel and C. H. L. Kennard

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trans-2-(Dimethoxyphosphinoyl)-1-phenyl-1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-isoindol-2-yloxy)ethene

I. D. Grice, I. D. Jenkins, W. K. Busfield, K. A. Byriel and C. H. L. Kennard

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1,4-Bis[2-(6-bromohexyl)-2H-tetrazol-5-yl]benzene

A. F. M. Fleming, F. Kelleher, M. F. Mahon, J. McGinley, K. C. Molloy and V. Prajapati

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3′-Isopropyl-8′,8′-dimethyl-2-benzofuran-1-spiro-7′-bicyclo[4.2.0]octa-1′(6′),2′,4′-trien-3-one

P. N. D. Singh, J. Pika, J. A. Krause Bauer and A. D. Gudmundsdóttir

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Pentyltriphenylphosphonium bromide

E. W. Czerwinski

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N-{3-Cyano-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazol-5-yl}benzamide

P. Zhong, Z. Yang, S. Li and R. Tang

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(R,R)-N,N′-Bis(5-chlorosalicylidene)-1,2-cyclohexanediamine

M.-H. Yang, Y.-Z. Li, C.-J. Zhu, Y. Pan and S.-H. Liu

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(4R,9S)-4-Hydroxymethyl-3,8-dioxa-1,6-diazaspiro[4.4]nonane-2,7-dithione monohydrate

G. Cioci, N. Leconte, A. Tatibouët, P. Rollin, S. Pérez and A. Imberty

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1,3,5-Trichloro-1λ⁶,2,4,6-thiatriazin-1-one

T. J. Clark, A. J. Lough, T. Chivers and I. Manners

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1-(4-Chlorophenyl)-3-(1H-1,2,4-triazol-1-yl)propan-1-one

L.-Z. Xu, H.-B. Song, J.-H. Liu, K. Li and G.-D. Shi

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2-(1,1,2,2-Tetrachloroethylsulfanyl)-3a,4,7,7a-tetrahydro-1H-isoindole-1,3(2H)-dione

D. Chopra, T. P. Mohan, K. S. Rao and T. N. Guru Row

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N-[(9E)-2-Chloro-9-thia-9H-xanthen-9-ylidene]-N-(4-fluorophenyl)amine

D. Chopra, K. Nagarajan and T. N. Guru Row

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2-(2,4-Dichlorophenyl)-1-(1H-1,2,4-triazol-1-yl)hexan-2-ol (hexaconazole)

D. Chopra, T. P. Mohan, K. S. Rao and T. N. Guru Row

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(4E)-3-[(2-Chloro-4,5-dihydro-1,3-thiazol-5-yl)methyl]-5-methyl-N-nitro-1,3,5-oxadiazinan-4-imine (thiamethaxam)

D. Chopra, T. P. Mohan, K. S. Rao and T. N. Guru Row

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(2E)-1-[(6-Chloropyridin-3-yl)methyl]-N-nitroimidazolidin-2-imine (imidachloprid)

D. Chopra, T. P. Mohan, K. S. Rao and T. N. Guru Row

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Ethyl 5-[(4,6-dimethoxypyrimidin-2-yl)ureidosulfonyl]-1-methyl-1H-pyrazole-4-carboxylate

D. Chopra, T. P. Mohan, K. S. Rao and T. N. Guru Row

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Methyl 2(E)-methoxyimino-2-[2-(2-methylphenoxymethyl)phenyl]acetate

D. Chopra, T. P. Mohan, K. S. Rao and T. N. Guru Row

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Pyridinium nitrate at 290 K

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Pyridinium nitrate at 120 K

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6-Isopropoxy-5-isopropylpyrimidine-2,4(1H,3H)-dione

W. Lewis, R. H. McKeown and W. T. Robinson

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1-Hydroxymethyl-2,2-diphenylethyl 2,4,6-trimethylphenyl ketone

A. G. Pinkus, K. K. Klausmeyer, R. P. Feazell, S. Logaraj and P. W. Hurd

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Conformational chirality of chemically symmetric molecules and a superlattice through enantioselective self-assembly: 1,1,1-tris[(4-cyanophenoxy)methyl]ethane

W. Xu, Z.-G. Zou, P. Guo and Y.-X. Lu

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Bis(2-pyrimidinyl) disulfide dihydrate: a redetermination

G. B. Jensen, G. Smith, D. S. Sagatys, P. C. Healy and J. M. White

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6-Methoxycarbonyl-2-methyl-1H-benzimidazol-3-ium nitrate hemihydrate

C.-F. Ding, S.-S. Zhang, X.-M. Li, H. Xu and P.-K. Ouyang

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5-(2-Furyl)-3-hydroxy-1-phenylpenta-2,4-dien-1-one

A. F. Arrieta and A. Mostad

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9-Chloro-10-(dimethoxymethyl)anthracene

W.-B. Yuan, L. Yan and R.-D. Yang

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Turn-over of an oxazoline ring induced by chiral change of a folded ascidiacyclamide analogue: cyclo(Ile-D–aThr–D-Val–Thz–Ile–D-Oxz–D-Val–Thz) N,N-dimethylformamide disolvate

A. Asano and M. Doi

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A sterically constrained bis(2,2′:6′,2′′-terpyridine) ligand

A. C. Benniston, W. Clegg, R. W. Harrington and P. Li

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2,2′-Dinitrodibenzyl

H. S. Yathirajan, B. Nagaraj, P. Nagaraja and D. E. Lynch

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4-(1H-Indol-3-yl)-2,6-bis(4-methoxyphenyl)pyridine

S. Tu, T. Li and F. Fang

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Ethyl 2-amino-4-(4-chlorophenyl)-6-(4-methoxyphenyl)pyridine-3-carboxylate

Y. Zhu, S. Tu, F. Fang and J. Xu

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A synthetic intermediate of enantiopure N-protected β-hydroxyvaline, (2R)-2-[N-(tert-butoxycarbonyl)amino]-3-methylbutane-1,3-diol

H. Oku, R. Naito, K. Yamada and R. Katakai

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6-Chloro-3-(4-chlorophenyl)-3,4-dihydroquinazolin-2(1H)-one acetone hemisolvate

D.-Q. Shi, Z.-Y. Li, C.-L. Shi, X.-S. Wang and Y. Zhang

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1-(4-Chlorophenyl)-3-(4-trifluoromethylbenzoylhydrazino)-2-propenone

L.-R. Wen, W.-S. Guo, M. Li, X.-M. Li, S.-S. Zhang, P.-K. Ouyang and Z.-Q. Ke

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3-Anilino-1-(2-fluoro-5-methylphenyl)-3-(methylsulfanyl)-2-(1H-1,2,4-triazol-1-yl)prop-2-en-1-one

L. Xu, C. Zhu, G. Si, Y. Qin and K. Li

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Benzylideneacetone 2,4-dinitrophenylhydrazone

S. Shan, Z. Fan, W.-X. Hu and D.-J. Xu

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1-Amino-5-benzoyl-4-phenylpyrimidin-2(1H)-one

N. Dege, M. Şekerci, A. Çetin, M. Dinçer, M. Gülcan, A. Cansız and O. Büyükgüngör

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The polyfunctionalized enaminone ethyl [(Z)-2-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidenemethyl)-1-methyl-3-oxo-but-1-enylamino]acetate

I. Vencato, S. Cunha, J. Ferrari, H. B. Napolitano and C. Lariucci

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(1,5-Dimethyl-6-oxo-1,2,4,5-tetrazinan-3-yl)imidazolium chloride

A. M. Mills, J.-Z. Wu, E. Bouwman, J. Reedijk and A. L. Spek

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1,5-Dimethyl-1,2,4,5-tetrazinane-3,6-dione

A. M. Mills, J.-Z. Wu, E. Bouwman, J. Reedijk and A. L. Spek

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N-(p-Nitrophenylsulfonyl)-1H-pyrrole

Z. Gültekin, W. Frey and T. Hökelek

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Bis(dimethylammonium) terephthalate

E. V. Karpova, M. A. Zakharov, S. I. Gutnikov and R. S. Alekseyev

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Ethyl 4H-thieno[3,2-b]pyrrole-5-carboxylate

J. T. Chantson and D. C. Liles

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7-Chloro-2,2-dimethyl-3-(4-methylphenyl)-1,2-dihydroquinazolin-4(3H)-one

D. Shi, C. Shi, Q. Zhuang and Y. Zhang

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1-(4-Methoxyphenyl)-2-(2-nitrophenoxy)propan-1-one

I. Vencato, P. H. Ferri, S. C. Santos, L. S. Santos, C. Lariucci and H. B. Napolitano

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N-tert-Butyl-4-chloro-5-methyl-2-nitroaniline

Y. Zhang, T.-Y. Feng and S.-Y. Li

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{3-[2-Methoxy-5-(1-methyl-1-phenylethyl)phenyl]-2,5-diphenyl-1,2,3,4-tetrahydro-4-isoxazol-4-yl}(2-thienyl)methanone

V. Sridharan, S. Pon Saravanakumar, S. Muthusubramanian, K. Anitha and B. Sridhar

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Bis(3-methylpyrazolium) chloranilate

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1-(2,6-Dihydroxyphenyl)ethanone

H.-R. Huang, X.-K. Xia, Z.-G. She, Y.-C. Lin, L. L. P. Vrijmoed and E. B. G. Jones

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Dibromodiphenyltellurium(IV)

J. Beckmann, D. Dakternieks, A. Duthie and C. Mitchell

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1-(2-Morpholinoethyl)-3-(3-phenylacryloyl)thiourea

B. M. Yamin and I. N. Hassan

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(1S,2R,4S,5R)-tert-Butyl 7-oxo-3-oxa-6-azatricyclo[3.2.1.0^2,4]octane-6-carboxylate

M. Meltzer, M. Marsch, T. Carell and K. Harms

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2-Amino-4-(2,5-dichlorophenyl)-5-(1H-1,2,4-triazol-1-yl)-1,3-thiazole

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2-Butyl-4-chloro-1-(4-nitrobenzyl)-1H-imidazole-5-carboxaldehyde

S. L. Gaonkar, H. S. Yathirajan, B. Nagaraj, R. S. Narasegowda and D. E. Lynch

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N′-tert-Butyl-N'-(3,5-dimethylbenzoyl)-N-(4-carboxyphenoxy)oxalyl-N-(4-ethylbenzoyl)hydrazine

C.-H. Mao, H.-B. Song, Q.-M. Wang, R.-Q. Huang, L. Chen and J. Shang

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