# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' rmkn in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 103.61 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.7693 _cell_length_b 11.1778 _cell_length_c 12.4178 _cell_angle_alpha 71.074 _cell_angle_beta 77.684 _cell_angle_gamma 88.014 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc 1 0 0 38.5 1.81 37.22 2 0 0 1372.49 15.3 1511.3 3 0 0 794.55 22.46 830.12 4 0 0 1730.07 26.78 1388.96 5 0 0 165.48 11.56 149.34 6 0 0 221.18 10.91 199.49 7 0 0 14.91 8.33 12.21 8 0 0 2.66 9.41 0.68 9 0 0 25.31 12.7 30.67 10 0 0 23.03 14.78 24.23 -10 1 0 0.91 17.55 2.48 -9 1 0 60.22 11.95 70.11 -8 1 0 288.14 14.24 271.41 -7 1 0 86.96 9.25 99.5 -6 1 0 9.11 6.84 12.3 -5 1 0 262.56 7.7 205.1 -4 1 0 763.03 10.55 684.39 -3 1 0 902.37 9.88 863.27 -2 1 0 45.77 2.66 55.95 -1 1 0 239.93 13.02 319.38 1 1 0 20.97 2.01 26.93 2 1 0 46.99 3.06 45.04 3 1 0 840.1 44.81 888.57 4 1 0 371.69 6.83 353.32 5 1 0 309.05 17.4 277.85 6 1 0 713.94 17.51 728.55 7 1 0 77.23 9.52 76.71 8 1 0 37.52 10.83 57.78 9 1 0 33.38 13.41 29.61 10 1 0 -9.61 15.13 0.74 -11 2 0 13.44 34.63 8.27 -10 2 0 7.16 19.31 9.65 -9 2 0 6.37 13.55 0.13 -8 2 0 28.49 9.62 39.33 -7 2 0 28.14 8.47 23.64 -6 2 0 414.49 11.39 381.87 -5 2 0 833.08 16.25 879.51 -4 2 0 801.78 8.93 777.27 -3 2 0 2616.06 13.35 2749.93 -2 2 0 150.77 7.93 153 -1 2 0 718.24 24.91 832.41 0 2 0 40.21 7.44 21.75 1 2 0 5121.13 85.04 6444.99 2 2 0 780.23 28.78 932.63 3 2 0 515.73 14.72 508.77 4 2 0 355.93 14.84 381.18 5 2 0 16.71 5.54 20.14 6 2 0 432.88 13.11 409.46 7 2 0 227.28 14.34 205.47 8 2 0 5.22 11 2.07 9 2 0 -0.67 13.56 0.34 10 2 0 20.34 15.63 30.11 -10 3 0 44.84 17.41 54.64 -9 3 0 -2.11 13.8 0 -8 3 0 -0.98 12.49 2.76 -7 3 0 54.89 12.22 58.17 -6 3 0 16.02 6.29 18.04 -5 3 0 79.31 6.75 90.07 -4 3 0 1754.02 23.78 1534.34 -3 3 0 652.41 21.96 712.52 -2 3 0 3.25 3.13 0 -1 3 0 1747.74 33.02 2097.85 0 3 0 94.04 3.82 111.6 1 3 0 7855.66 41.73 8581.89 2 3 0 24.79 2.87 21.69 3 3 0 13.97 4.2 9.42 4 3 0 179.75 10.43 174.08 5 3 0 1.11 5.09 4.44 6 3 0 41.91 6.77 52.66 7 3 0 218.39 12.17 203.66 8 3 0 73.31 13.69 65.79 9 3 0 7.78 13.03 3.62 10 3 0 25.73 16.48 34.03 -10 4 0 55.58 17.9 56.87 -9 4 0 2.17 15.24 6.51 -8 4 0 73.62 13.23 107.66 -7 4 0 13.63 10.8 24.85 -6 4 0 -0.78 7.64 1.26 -5 4 0 94.68 7.04 97.13 -4 4 0 255.02 7.74 245.01 -3 4 0 -1.17 3.47 1.11 -2 4 0 1193.52 39.41 1334.02 -1 4 0 637.11 31.1 790.32 0 4 0 72.25 3.36 75.48 1 4 0 4544.66 22.2 4825.88 2 4 0 314.18 10.06 375.99 3 4 0 677.1 20.7 615.32 4 4 0 117.01 6.92 98.82 5 4 0 375.2 17.05 339.26 6 4 0 7.75 7.37 8.23 7 4 0 177.19 11.45 153.17 8 4 0 5.72 12.26 11.22 9 4 0 53.48 17.77 54.29 10 4 0 79.94 26.38 77.26 -10 5 0 17.75 24.75 6.27 -9 5 0 9.52 17.31 2.32 -8 5 0 71.89 14.5 81.34 -7 5 0 17.32 8.9 29.12 -6 5 0 6.01 7.74 8.63 -5 5 0 241.69 15.75 233.5 -4 5 0 289.94 16.39 234.35 -3 5 0 33.28 5.09 33.09 -2 5 0 35.54 6.51 35.17 -1 5 0 149.49 4.16 172.57 0 5 0 77.48 3.26 88.19 1 5 0 0.97 2.25 0 2 5 0 20.34 3.48 29.67 3 5 0 20.11 4.28 26.41 4 5 0 -1.98 6.26 1.44 5 5 0 151.87 12.78 133.06 6 5 0 1129.32 17.05 1077 7 5 0 401.02 16.35 382.28 8 5 0 7.48 12.85 0.06 9 5 0 -12.67 15.78 1.82 10 5 0 19.17 28.62 3.33 -10 6 0 -5.81 47.76 0.6 -9 6 0 24.9 18.91 21.45 -8 6 0 1.09 18.58 6.17 -7 6 0 1.11 10.22 1.43 -6 6 0 3.57 8.18 11.14 -5 6 0 101.49 9.3 91.14 -4 6 0 69.84 6.48 72.29 -3 6 0 1103.14 58.26 1099.71 -2 6 0 62.01 4.73 57.73 -1 6 0 41.08 3.49 40.87 0 6 0 48.09 4.28 49.97 1 6 0 55.22 4.51 59.22 2 6 0 4449.59 21.99 4807.17 3 6 0 319.29 28.26 320.66 4 6 0 110.71 9.34 106.01 5 6 0 106.81 8.78 94.12 6 6 0 104.82 18.78 97.47 7 6 0 113.4 10.7 88.64 8 6 0 12.94 14.23 5.57 9 6 0 -18.47 22.37 2.45 -9 7 0 3.93 21.36 3.87 -8 7 0 9.72 21.56 4.93 -7 7 0 35.93 17.88 54.66 -6 7 0 89.95 10.32 84.24 -5 7 0 60.47 17 44.97 -4 7 0 3.56 7.19 2.06 -3 7 0 1.81 5.09 1.7 -2 7 0 1.02 5.77 1.19 -1 7 0 0.75 3.36 1.09 0 7 0 180.65 17.28 208.21 1 7 0 -2.12 3.63 0 2 7 0 454.54 9.86 484.38 3 7 0 -1 7.43 2.28 4 7 0 191.06 12.25 194.61 5 7 0 142.26 32.65 143.76 6 7 0 164.42 32.42 171.76 7 7 0 37.33 12.77 40.7 8 7 0 27.17 14.63 29.63 -8 8 0 -2.22 13.85 0.16 -7 8 0 2.39 10.65 0.02 -6 8 0 45.69 10.19 48.07 -5 8 0 114.99 9.95 147.18 -4 8 0 37.66 14.96 37.03 -3 8 0 1.25 6.39 0.55 -2 8 0 20.6 6.79 18.59 -1 8 0 171.95 9.58 175.69 0 8 0 190.85 17.2 225.31 1 8 0 -3.43 4.19 0.52 2 8 0 234.3 10.06 238.56 3 8 0 361.17 20.36 333.99 4 8 0 166.23 16.08 162.67 5 8 0 2.64 10.09 6.33 6 8 0 14.73 16.03 4.12 7 8 0 17.03 13.71 9.71 8 8 0 4.69 15.78 7.98 -8 9 0 45.96 19.29 77.19 -7 9 0 123.37 35.05 109.91 -6 9 0 44.98 17.67 37.1 -5 9 0 8.07 9.42 5.1 -4 9 0 99.78 34.17 77.08 -3 9 0 5.45 7.27 4.41 -2 9 0 87.45 8.43 86.05 -1 9 0 375.47 11.99 392.58 0 9 0 68.11 5.41 64.66 1 9 0 -2.09 5.46 0.1 2 9 0 -3.49 7.06 0.03 3 9 0 606.69 20.25 632.55 4 9 0 262.91 17.15 204.87 5 9 0 3.87 10.93 0.86 6 9 0 144.66 50.9 133.47 7 9 0 7.42 14.62 0.15 -7 10 0 -2.57 14.74 1.73 -6 10 0 55.64 17.56 46.94 -5 10 0 66.65 20.61 51.67 -4 10 0 0.43 8.95 0.16 -3 10 0 4.63 8.73 1.18 -2 10 0 104.75 9.51 101.22 -1 10 0 0.88 7.59 9.6 0 10 0 167.9 10.4 126.37 1 10 0 14.72 6.94 19.41 2 10 0 -1.94 8.43 0.16 3 10 0 89.42 36.24 48.18 4 10 0 -0.07 10.81 1.81 5 10 0 134.37 52.29 115.01 6 10 0 11.68 12.04 4.41 7 10 0 11.62 19.76 16.61 -6 11 0 7.65 13.07 12.95 -5 11 0 5.55 10.52 8.54 -4 11 0 1.04 12.68 11.95 -3 11 0 19 8.68 17.37 -2 11 0 -1.57 9.01 0.54 -1 11 0 6.69 7.71 7.47 0 11 0 46.66 8.62 49.8 1 11 0 38.67 10.24 33.22 2 11 0 5.7 10.24 1.38 3 11 0 88.03 14.95 65.93 4 11 0 99.53 15.16 67.45 5 11 0 50.49 21.11 26.02 6 11 0 31.26 20.3 20.67 -4 12 0 55.6 11.36 45.36 -3 12 0 7.46 12.04 6.1 -2 12 0 9.14 9.53 1.05 -1 12 0 12.67 7.72 13.89 0 12 0 104.71 11.81 87.05 1 12 0 14.86 11.61 5.73 2 12 0 96.41 14.55 61.45 3 12 0 114.86 35.77 50.3 -2 13 0 1.62 25.72 13.27 -1 13 0 0.31 12.36 3.38 0 13 0 8.63 13.08 1.51 1 13 0 26.05 15.24 17.98 -3 -12 1 8.21 18.31 5.02 -2 -12 1 57.86 14.76 37.75 -1 -12 1 -3.64 12.03 1.98 0 -12 1 22.29 13.12 11.26 1 -12 1 84.42 11.29 63.25 2 -12 1 7.71 11.7 5.04 3 -12 1 33.1 11.77 28.17 4 -12 1 -13.37 20.72 0 -5 -11 1 29.84 21.9 52.39 -4 -11 1 234.34 20.94 161.78 -3 -11 1 21.06 12.58 18.61 -2 -11 1 36.01 11.42 37.58 -1 -11 1 -0.2 11.21 0.69 0 -11 1 0.18 10.01 1.87 1 -11 1 37.67 10.44 19.35 2 -11 1 60.62 9.04 58.05 3 -11 1 -8.02 8.02 0.09 4 -11 1 6.6 12.59 5.22 5 -11 1 24.52 14.4 23.76 6 -11 1 -2.28 21.16 5.48 -6 -10 1 23.95 13.3 20.27 -5 -10 1 21.8 13.07 13.36 -4 -10 1 64.64 14.59 66.07 -3 -10 1 78.32 12.22 64.23 -2 -10 1 3.83 8.29 0.02 -1 -10 1 2.89 7.15 3.84 0 -10 1 33.43 6.97 30.96 1 -10 1 29.23 7 30.77 2 -10 1 118.89 9 90.32 3 -10 1 11.2 9.81 11.79 4 -10 1 5.13 10.2 0.44 5 -10 1 105.05 11.48 104.65 6 -10 1 15.08 23.48 0.88 7 -10 1 -1.97 12.69 2.55 -7 -9 1 4.64 15.5 4.24 -6 -9 1 51.46 22.99 32.6 -5 -9 1 1.37 11.62 0.06 -4 -9 1 31.07 10.07 30.48 -3 -9 1 206.68 16.35 218.83 -2 -9 1 17.96 7.18 19.55 -1 -9 1 -1.15 6.25 0.51 0 -9 1 47.44 5.4 54.61 1 -9 1 0.56 4.68 1.63 2 -9 1 27.7 6.81 25.98 3 -9 1 67.19 8.81 72.91 4 -9 1 27.35 8.33 19.14 5 -9 1 5.23 7.92 5.93 6 -9 1 14.78 11.7 12.39 7 -9 1 -1.39 13.23 0.02 8 -9 1 5.3 21.05 0.23 -8 -8 1 103.4 28.55 80.55 -7 -8 1 1.02 15.13 4.54 -6 -8 1 55.67 17.81 52.83 -5 -8 1 12.2 12.85 6.87 -4 -8 1 -2.52 8.09 1.72 -3 -8 1 713.79 34.02 748.1 -2 -8 1 22.61 6.87 20.39 -1 -8 1 125.54 13.23 132.02 0 -8 1 209.41 8.16 212.42 1 -8 1 7.85 4.37 4.74 2 -8 1 84.87 20.57 99.39 3 -8 1 -0.43 6.34 0.04 4 -8 1 24.41 9.69 24.23 5 -8 1 91.98 17.21 88.02 6 -8 1 -2.57 10.67 0.24 7 -8 1 -7.25 11.73 0.75 8 -8 1 27.3 18.47 34.96 -8 -7 1 35.21 16.39 30.43 -7 -7 1 11.35 14.29 1.26 -6 -7 1 125.83 13.46 123.35 -5 -7 1 152.19 48.34 118.39 -4 -7 1 -3.95 11.27 0 -3 -7 1 405.97 29.87 444.93 -2 -7 1 23.28 8.1 21.76 -1 -7 1 121.66 7.14 131.81 0 -7 1 27.63 4.04 35.52 1 -7 1 13.42 4.07 13.5 2 -7 1 348.69 62.8 419.65 3 -7 1 99.52 15.35 90.4 4 -7 1 444.61 27.05 474.89 5 -7 1 2.69 7.57 0.33 6 -7 1 48.31 10.23 55.18 7 -7 1 30.34 18.1 25.15 8 -7 1 38.72 22.12 32.4 9 -7 1 25.52 25.19 15.2 -8 -6 1 -1.88 20.73 6.9 -7 -6 1 6.21 11.43 4.17 -6 -6 1 3.12 10.23 8.4 -5 -6 1 1010.05 36.74 1045.97 -4 -6 1 14.98 7.24 18.36 -3 -6 1 171.88 7.76 179.54 -2 -6 1 1947.98 14.92 2166.73 -1 -6 1 847.97 11.42 1040.72 0 -6 1 460.32 6.6 489.46 1 -6 1 328.35 16.71 385.98 2 -6 1 250.37 14.5 258.03 3 -6 1 529.89 24.27 539.47 4 -6 1 39.65 6.38 42.38 5 -6 1 15.51 7.11 8.68 6 -6 1 110.7 12.38 109.49 7 -6 1 30.84 10.65 39.47 8 -6 1 147.86 17.29 124.59 9 -6 1 4.47 17.78 8.09 10 -6 1 31.67 30.64 29.13 -9 -5 1 52.68 16.55 47.93 -8 -5 1 54.14 15.37 41.69 -7 -5 1 157.06 11.1 146.68 -6 -5 1 0.71 8.41 0.46 -5 -5 1 271.61 17.51 286.79 -4 -5 1 -3.54 6.33 0 -3 -5 1 45.62 4.91 57.84 -2 -5 1 1783.54 31.61 2052.98 -1 -5 1 9.11 2.95 7.71 0 -5 1 1091.2 7.57 1342.65 1 -5 1 410.9 11.5 485.04 2 -5 1 578.41 16.18 597.98 3 -5 1 70.49 20.38 70.52 4 -5 1 134.86 12.03 144.22 5 -5 1 20.67 5.86 21.75 6 -5 1 0.83 7.66 0.01 7 -5 1 2.53 7.79 1.73 8 -5 1 -5.06 13.68 0.08 9 -5 1 82.83 19.53 63.27 10 -5 1 16.72 20.21 19.8 -10 -4 1 123.28 28.43 89.88 -9 -4 1 6.03 15.37 10.21 -8 -4 1 52.05 16.57 49.67 -7 -4 1 40.72 8.82 40.11 -6 -4 1 775.84 36.28 715.03 -5 -4 1 416.5 25.15 355.53 -4 -4 1 301.35 13.39 291.47 -3 -4 1 56.92 5.03 62.04 -2 -4 1 930.21 18.59 1064.71 -1 -4 1 878.08 9.83 1168.51 0 -4 1 1.42 2.03 1.97 1 -4 1 34 4.63 47.62 2 -4 1 198.23 9.9 205.97 3 -4 1 666.72 42.14 722.55 4 -4 1 280.61 12.38 254.89 5 -4 1 -0.88 6.73 3.3 6 -4 1 78.26 10.62 80.47 7 -4 1 67.06 11.67 91.26 8 -4 1 11.07 11.8 2.65 9 -4 1 4.81 16.25 0 10 -4 1 43.5 20.4 36.7 -10 -3 1 8.73 17.46 2.32 -9 -3 1 59.86 14.95 54.99 -8 -3 1 46.3 13.65 53.63 -7 -3 1 78.62 11.92 64.37 -6 -3 1 349.32 17.16 365.79 -5 -3 1 126.88 7.44 108.49 -4 -3 1 1086.19 13.14 977.51 -3 -3 1 354.91 12.93 366.05 -2 -3 1 14.3 3.28 10.99 -1 -3 1 6975.92 25.11 7624.78 0 -3 1 242.97 4.86 318.32 1 -3 1 233.66 11.12 324.75 2 -3 1 625.1 29.45 710.97 3 -3 1 313.51 12.75 295.95 4 -3 1 300.11 13.15 290.59 5 -3 1 0.56 5.54 0.28 6 -3 1 20.3 7.55 24.37 7 -3 1 145.06 13.42 144.94 8 -3 1 4.29 11.81 4.28 9 -3 1 0.86 13.16 0.93 10 -3 1 -4.04 18.82 0.1 -10 -2 1 41.78 17.44 28.13 -9 -2 1 39.78 14.47 45.81 -8 -2 1 25.14 12.65 20.13 -7 -2 1 10.65 10.67 0.06 -6 -2 1 503.47 12.87 469.57 -5 -2 1 0.35 5.69 0.24 -4 -2 1 8.51 5.35 13.07 -3 -2 1 1132.19 24.06 914.09 -2 -2 1 12.92 3.87 3.91 -1 -2 1 9045.63 26.54 9976.6 0 -2 1 2914.66 24.77 4043.89 1 -2 1 11530.73 105.26 10734.14 2 -2 1 4629.3 75.99 5323.23 3 -2 1 19.54 3.69 19.24 4 -2 1 0.97 3.92 1.04 5 -2 1 1490.49 36.05 1455.95 6 -2 1 20.06 6.16 20.25 7 -2 1 1.46 8.8 0.13 8 -2 1 45.05 12 44.25 9 -2 1 2.86 14.16 2.55 10 -2 1 45.37 19.32 40.69 11 -2 1 1.47 30.95 4.9 -10 -1 1 60.95 17.64 67.87 -9 -1 1 69.32 16.85 54.31 -8 -1 1 8.95 11.59 2.88 -7 -1 1 181.21 11.89 160.21 -6 -1 1 210.33 10.97 205.27 -5 -1 1 61.63 5.6 78.83 -4 -1 1 1692.54 11.93 1364.24 -3 -1 1 556.03 13.91 447.3 -2 -1 1 444.03 30.83 465.32 -1 -1 1 3138.11 39.92 3450.23 0 -1 1 173.12 3.31 255.81 1 -1 1 5941.69 129.49 4652.01 2 -1 1 235.51 8.72 175.9 3 -1 1 6.9 2.9 16.1 4 -1 1 2975.55 24.19 2851.78 5 -1 1 -0.37 4.04 0.16 6 -1 1 38.14 6.84 32.13 7 -1 1 124.37 9.56 129.36 8 -1 1 -1.96 9.02 0.08 9 -1 1 -6.2 11.26 0.53 10 -1 1 -17.04 18.12 3.28 -10 0 1 30.13 14.94 7.08 -9 0 1 3.53 13.91 16.8 -8 0 1 47.2 10.96 52.44 -7 0 1 40.38 9.08 47.61 -6 0 1 133.24 11.92 128.18 -5 0 1 152.11 6.88 134.82 -4 0 1 48.88 4.25 40.77 -3 0 1 2517.23 19.61 2289.46 -2 0 1 1171.87 18.44 946.5 -1 0 1 665.68 20.1 534.57 1 0 1 6647.57 42.96 4570.59 2 0 1 5662.66 31.28 5268.56 3 0 1 5.52 2.55 4.12 4 0 1 11.34 3.56 10.79 5 0 1 57.08 4.49 68.59 6 0 1 151.06 10.56 144.05 7 0 1 -0.72 7.46 1.72 8 0 1 -3.19 9.02 4.42 9 0 1 3.34 11.12 6.85 10 0 1 2.71 15.22 5.65 -10 1 1 55.94 25.3 70.01 -9 1 1 66.68 11.75 88.46 -8 1 1 60.53 10.91 63.45 -7 1 1 94.06 9.67 98.96 -6 1 1 119.91 8.99 127.01 -5 1 1 1912.91 14.6 1703.63 -4 1 1 13.13 4.04 9.92 -3 1 1 603.48 23.57 641.12 -2 1 1 3508.62 59.94 3559.96 -1 1 1 631.17 33.86 655.63 0 1 1 19.72 1.5 23.88 1 1 1 2476.51 16.99 2493.84 2 1 1 61.44 2.94 74.01 3 1 1 102.8 4.71 83.87 4 1 1 82.47 6.24 104.52 5 1 1 268.66 9.02 239.86 6 1 1 677.88 13.7 643.06 7 1 1 198.9 10.87 173.61 8 1 1 1.81 9.87 2.54 9 1 1 43.46 12.71 52.87 10 1 1 16.57 15.64 22.97 11 1 1 -21.64 25.16 7.3 -10 2 1 17.43 17.39 28.03 -9 2 1 33.87 17.19 52.25 -8 2 1 11.4 11.91 16.44 -7 2 1 124.85 10.45 115.86 -6 2 1 155.46 8.51 136.36 -5 2 1 223.69 8.46 189.05 -4 2 1 816.84 12.25 761.11 -3 2 1 -0.92 3.49 0.01 -2 2 1 1346.39 18.06 1429.94 -1 2 1 857.18 12.32 924.98 0 2 1 3688.45 30.09 4693.27 1 2 1 1962.18 34.85 2392.82 2 2 1 923.38 13.27 961.87 3 2 1 53.76 3.73 49.06 4 2 1 72.46 4.57 88.81 5 2 1 92.9 7.17 84.43 6 2 1 79.18 7.31 49.55 7 2 1 18.67 8.63 26.83 8 2 1 22.12 10.64 15.13 9 2 1 104.09 13.35 122.35 10 2 1 10.86 14.91 5.36 -10 3 1 -18.67 18.67 1.85 -9 3 1 447.9 36.77 487.3 -8 3 1 -3.28 13.63 5.6 -7 3 1 30.09 10.36 41.42 -6 3 1 -0.55 5.58 0.87 -5 3 1 476.78 18.99 463.71 -4 3 1 105.83 9.19 87.62 -3 3 1 593.18 8.17 519.61 -2 3 1 629.06 8.09 576.46 -1 3 1 55.04 5.05 48.59 0 3 1 2342.46 25 2998.1 1 3 1 9011.21 96.54 10452.82 2 3 1 212.36 11.93 241.48 3 3 1 41.77 3.8 41.53 4 3 1 273.64 20.21 274.44 5 3 1 67.44 5.96 61.04 6 3 1 1.53 6.76 0.17 7 3 1 899.27 15.88 897.18 8 3 1 33.01 11.22 37.54 9 3 1 67.53 13.41 74.6 10 3 1 14.35 16.02 10.17 -10 4 1 18.71 18.12 24.62 -9 4 1 16.87 15.33 18.26 -8 4 1 88.07 14.42 117.45 -7 4 1 -3.52 11.38 2.4 -6 4 1 128.1 11 128.93 -5 4 1 165.38 9.1 162.35 -4 4 1 33.19 4.67 34 -3 4 1 350.8 10.43 313.86 -2 4 1 343.23 10.51 397.43 -1 4 1 169.39 5.7 196.29 0 4 1 35.72 6.33 65.46 1 4 1 859.63 32.76 1208.56 2 4 1 420.32 13.9 488.53 3 4 1 579.91 15.27 557.66 4 4 1 222.89 9.69 215.39 5 4 1 32.07 6.45 35.99 6 4 1 57.14 7.77 46.88 7 4 1 715.42 32.32 657.32 8 4 1 3.3 10.57 3.53 9 4 1 13.14 14.49 0.82 10 4 1 25.7 15.66 15.96 -10 5 1 -2 30.99 0.01 -9 5 1 25.83 17.32 31.86 -8 5 1 96.26 15.73 115.03 -7 5 1 10.18 9.66 7.59 -6 5 1 5.8 7.04 8.55 -5 5 1 32.28 6.84 35.06 -4 5 1 301.96 11.25 305.47 -3 5 1 -0.81 4.5 0.08 -2 5 1 109.22 10.46 111.97 -1 5 1 168.06 8.71 191.41 0 5 1 1434.86 15.4 1653.83 1 5 1 126.13 6.38 148.44 2 5 1 53.78 3.09 51.29 3 5 1 66.72 4.89 66.8 4 5 1 22.61 4.71 21.21 5 5 1 5.04 6.16 1.07 6 5 1 366.17 15.2 381.19 7 5 1 1.83 8.57 0.25 8 5 1 18.15 9.65 20.85 9 5 1 0.12 14.26 6.61 10 5 1 24.61 29.62 10.03 -10 6 1 39.07 42.06 8.1 -9 6 1 81.1 19.46 89.61 -8 6 1 8.68 17.19 2.53 -7 6 1 18.84 14.4 14.17 -6 6 1 5.68 7.78 4.26 -5 6 1 4.65 6.52 6.5 -4 6 1 13.76 5.53 4.77 -3 6 1 117.93 6.67 107.88 -2 6 1 129.31 7.91 133.67 -1 6 1 505.03 9.23 497.71 0 6 1 22.24 7.73 30.53 1 6 1 302.34 8.9 337.1 2 6 1 992.63 23.7 1094.42 3 6 1 757.39 30.48 724.71 4 6 1 27.89 6.23 25.38 5 6 1 17.19 6.76 23.95 6 6 1 256.38 11.96 285.5 7 6 1 118.15 9.95 130.65 8 6 1 5.27 13.93 1.52 9 6 1 -2.41 18.77 4.59 -9 7 1 13.14 28.74 14.17 -8 7 1 287.09 32.58 232.84 -7 7 1 92.52 30.71 106.53 -6 7 1 183.07 28.97 190.91 -5 7 1 142.58 18.87 138.14 -4 7 1 403.14 26.05 466.87 -3 7 1 77.76 6.51 70.94 -2 7 1 229.9 11.87 219.48 -1 7 1 579.35 10.25 598.18 0 7 1 199.49 9.1 187.81 1 7 1 30.23 3.59 26.17 2 7 1 42.91 4.85 48.59 3 7 1 92.01 10.95 88.02 4 7 1 25.13 7.78 22.86 5 7 1 204.59 43.47 200.41 6 7 1 -0.87 9.96 1.04 7 7 1 -7.94 11.73 0.92 8 7 1 17.53 13.69 18.62 9 7 1 38.41 20.98 32.28 -8 8 1 10.81 16.78 19.14 -7 8 1 14.94 12.42 8.7 -6 8 1 5.31 9.6 0.12 -5 8 1 57.49 8.76 79.57 -4 8 1 48.53 7.74 48.52 -3 8 1 677.97 63.07 728.65 -2 8 1 -0.42 5.14 0.62 -1 8 1 174.49 7.67 164.71 0 8 1 34.44 3.74 39.44 1 8 1 81.46 7.08 66.76 2 8 1 12.55 5.04 7.34 3 8 1 338.17 32.04 315.7 4 8 1 18.78 7.58 13.61 5 8 1 -6.42 7.38 0.49 6 8 1 3.93 9.43 2.55 7 8 1 71.78 12.84 73.38 8 8 1 10.88 15.61 4.72 9 8 1 14.61 25.42 16.63 -8 9 1 49.84 16.83 65.92 -7 9 1 237.93 19.37 204.95 -6 9 1 -8.06 9.57 0.45 -5 9 1 205.55 16.72 193.94 -4 9 1 10.07 7.56 6.57 -3 9 1 4.51 7.16 4.88 -2 9 1 106.19 11.5 77.68 -1 9 1 46.8 5.67 61.18 0 9 1 34.5 5.45 40.23 1 9 1 7.72 4.53 7.67 2 9 1 3.64 6.52 3.05 3 9 1 51.77 7.11 49.89 4 9 1 170.89 26.31 182.45 5 9 1 80.18 25.83 75.9 6 9 1 -1.55 10.65 2.1 7 9 1 5.37 13.54 7 8 9 1 -9.4 13.85 2.13 -7 10 1 -0.75 12.99 6.02 -6 10 1 8.61 9.76 6.3 -5 10 1 63.38 23.98 58.26 -4 10 1 0.39 8.69 0.75 -3 10 1 135.82 10.98 110.7 -2 10 1 13.33 7.38 6.43 -1 10 1 9.03 7.44 14.02 0 10 1 2.21 5.37 0.22 1 10 1 4.67 5.21 4.82 2 10 1 100.93 11.4 82.74 3 10 1 9.06 12.55 6.63 4 10 1 0.01 9.81 0.04 5 10 1 35.45 17.52 29.37 6 10 1 16.36 11.6 15.04 7 10 1 19.98 12.56 24.15 -6 11 1 13.27 12.86 21.57 -5 11 1 59.51 12.39 49.29 -4 11 1 15.68 11.92 18.33 -3 11 1 44.81 8.42 35 -2 11 1 85.66 9.15 95.83 -1 11 1 18.08 6.61 23.25 0 11 1 1.64 5.18 1.76 1 11 1 9.42 6.68 10.94 2 11 1 -3.54 9.57 5.88 3 11 1 72.69 15.62 57.91 4 11 1 72.05 14.54 49.89 5 11 1 10.53 15.2 8.49 -4 12 1 35.87 10.73 39.65 -3 12 1 7.37 9.99 4.01 -2 12 1 70.17 12.32 58.07 -1 12 1 9.6 6.64 18.02 0 12 1 78.94 20.2 76.11 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30.98 32.78 16.26 -6 -9 2 6.99 14.78 0.11 -5 -9 2 11.35 13.12 7.34 -4 -9 2 227.41 19.81 154.09 -3 -9 2 -3.83 9.69 0.06 -2 -9 2 35.96 7.76 36.95 -1 -9 2 13.15 6.99 15.75 0 -9 2 11.95 5.92 11.42 1 -9 2 92.92 7.59 100.07 2 -9 2 31.25 8.04 24.56 3 -9 2 4.41 9.04 5.09 4 -9 2 8.66 8.09 0.59 5 -9 2 49.08 10.07 41.35 6 -9 2 1.26 10.41 8.99 7 -9 2 12.6 12.83 14.07 -7 -8 2 5.9 17.41 5.71 -6 -8 2 6.16 13.21 1.1 -5 -8 2 74.52 20.8 76.12 -4 -8 2 4.48 9.89 8.87 -3 -8 2 110.07 9.22 91.63 -2 -8 2 77.26 7.24 80.97 -1 -8 2 53.36 6.77 68.39 0 -8 2 344.28 11.71 406.27 1 -8 2 7.36 5.44 9.15 2 -8 2 21.74 7.06 21.09 3 -8 2 133.84 18.02 121.49 4 -8 2 95.94 11.31 86.13 5 -8 2 198.43 14.6 224.05 6 -8 2 55.28 13.3 44.01 7 -8 2 -2.37 11.5 1.43 8 -8 2 10.58 22.27 18.64 -7 -7 2 1.85 16.04 9.7 -6 -7 2 5.49 12.83 12.31 -5 -7 2 161.68 34.1 142.18 -4 -7 2 293.53 15.59 307.5 -3 -7 2 158.43 10.5 161.98 -2 -7 2 65.31 6.5 66.04 -1 -7 2 130.98 8.63 158.12 0 -7 2 76.93 5.46 82.55 1 -7 2 204.03 11.1 250.4 2 -7 2 84.03 14.31 72.75 3 -7 2 225.61 15.14 238.12 4 -7 2 59.65 14.5 47.11 5 -7 2 14.52 7.82 12.61 6 -7 2 2.52 9.9 0.92 7 -7 2 25.56 12.39 30.27 8 -7 2 8.83 19.63 5.9 -8 -6 2 120.5 26.13 122.27 -7 -6 2 77.84 14.29 69.06 -6 -6 2 90.4 11.26 91.99 -5 -6 2 803.55 51.58 662.68 -4 -6 2 245.37 14.42 238.42 -3 -6 2 27.03 6.09 38.08 -2 -6 2 3.65 4.41 0.21 -1 -6 2 19.16 4.69 21.08 0 -6 2 46.38 4.35 46.32 1 -6 2 157.97 6.61 183.3 2 -6 2 129.67 7.06 144.91 3 -6 2 6.6 5.34 6.1 4 -6 2 102.1 10.65 98.93 5 -6 2 1.31 6.59 0.46 6 -6 2 8.8 7.63 1.76 7 -6 2 5.94 8.03 0 8 -6 2 -2.43 14.4 0.64 9 -6 2 17.2 16.66 15.12 10 -6 2 9.82 41.6 1.3 -9 -5 2 5.69 33.07 28.26 -8 -5 2 46.85 14.89 35.93 -7 -5 2 102.36 12.26 96.08 -6 -5 2 53.01 10.17 46.71 -5 -5 2 378.97 14.17 346.52 -4 -5 2 17.96 7.06 19.47 -3 -5 2 35.42 5.92 36.15 -2 -5 2 280.06 8.33 361.06 -1 -5 2 34.73 5.96 45.55 0 -5 2 323.82 9.54 407.6 1 -5 2 1043.44 72.45 1376.44 2 -5 2 72.61 5.4 77.6 3 -5 2 2.82 4.29 4.6 4 -5 2 178.65 9.07 175.35 5 -5 2 12.02 6.1 18.21 6 -5 2 104.73 9.47 102.02 7 -5 2 60.21 9.64 57.62 8 -5 2 9.32 12.56 7.43 9 -5 2 3.54 15.04 0.51 10 -5 2 46.72 25.69 12.15 -9 -4 2 26.29 17.98 17.89 -8 -4 2 0.57 14.29 0.7 -7 -4 2 11.72 12.12 11.78 -6 -4 2 2.33 8.41 7.28 -5 -4 2 182.63 13.61 161.76 -4 -4 2 79.65 7.58 70.6 -3 -4 2 90.34 7.37 79.94 -2 -4 2 67.55 4.99 74.44 -1 -4 2 147.16 7.92 142.92 0 -4 2 53.32 4.06 56.23 1 -4 2 2.1 2.96 4.66 2 -4 2 453.93 19.68 447.96 3 -4 2 -0.31 3.77 6.34 4 -4 2 226.94 8.32 226.58 5 -4 2 0.76 6.41 0 6 -4 2 -2.59 7.27 0.66 7 -4 2 156.45 13.84 161.4 8 -4 2 -5.78 11.44 2.33 9 -4 2 30.79 15.24 44.77 10 -4 2 17.95 21.51 4.3 -9 -3 2 -6.8 15.84 0.12 -8 -3 2 13.18 14.1 32.92 -7 -3 2 16.27 11.51 11.58 -6 -3 2 57.31 8.34 72.86 -5 -3 2 3.82 6.11 1.77 -4 -3 2 146.1 8.99 119.46 -3 -3 2 315.63 15.7 311.44 -2 -3 2 593.12 7.68 709.62 -1 -3 2 5.95 2.95 6.22 0 -3 2 212.59 8.67 282.63 1 -3 2 3841.18 49.97 4731.02 2 -3 2 1787.51 40.26 1903.69 3 -3 2 226.47 11.49 203.39 4 -3 2 9.99 4.69 13.51 5 -3 2 40.45 7.01 35.99 6 -3 2 554.12 30.29 478.71 7 -3 2 89.32 13.37 82.07 8 -3 2 2.81 13.03 8.89 9 -3 2 60.23 16.03 70.79 10 -3 2 -11.08 19.15 3.96 -10 -2 2 101.93 22.12 85.81 -9 -2 2 27.6 16.17 19.46 -8 -2 2 22.68 13.05 31.76 -7 -2 2 110.59 12.94 108.74 -6 -2 2 42.19 7.5 37.12 -5 -2 2 56.81 7.31 49.28 -4 -2 2 83.34 6.63 69.39 -3 -2 2 94.5 7.9 78.09 -2 -2 2 354.67 14.26 337.03 -1 -2 2 136.96 4.21 192.23 0 -2 2 255.29 4.82 314.89 1 -2 2 7.19 2.7 5.11 2 -2 2 4297.75 76.11 3938.44 3 -2 2 1.53 3.52 0.49 4 -2 2 783.62 30.88 744.8 5 -2 2 698.29 14.03 683.81 6 -2 2 43.02 6.47 40.15 7 -2 2 79.9 9.97 90.55 8 -2 2 55.77 10.94 60.43 9 -2 2 38.21 17.45 41.77 10 -2 2 22.54 17.16 20.51 11 -2 2 24.89 34.86 16.41 -10 -1 2 128.67 18.98 118.38 -9 -1 2 2.17 14.74 6.51 -8 -1 2 3.24 12.5 0.01 -7 -1 2 -4.47 9.32 0.39 -6 -1 2 13.81 8.17 9.19 -5 -1 2 509.16 21.43 397.67 -4 -1 2 754.06 18.98 619.06 -3 -1 2 30.66 4.55 21.33 -2 -1 2 793.49 30.5 699.09 -1 -1 2 154.07 4.64 216.89 0 -1 2 2332.91 24.47 2865.21 1 -1 2 5104.67 98.03 4670.14 2 -1 2 59.17 5.73 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218.62 4.6 317.16 1 1 2 2.17 2.14 0.73 2 1 2 459.42 39.21 354.92 3 1 2 1228.44 18.87 1072.74 4 1 2 66.01 5.71 71.95 5 1 2 313.11 22.12 329.88 6 1 2 2.01 5.97 0 7 1 2 74.13 7.94 108.07 8 1 2 146.9 13.1 169.33 9 1 2 41.42 12.3 49.44 10 1 2 0.3 17.13 0.4 11 1 2 6.27 30.04 26.91 -10 2 2 1.45 18.77 3.42 -9 2 2 22.12 14.3 28.69 -8 2 2 17.84 12.48 16.84 -7 2 2 45.22 9.75 41.1 -6 2 2 135.91 9.63 119.62 -5 2 2 108.54 6.79 90.61 -4 2 2 648.75 22.04 612.05 -3 2 2 189.17 6.9 162.07 -2 2 2 722.02 8.62 644.86 -1 2 2 2774.57 94.06 3301.96 0 2 2 550.24 10.92 873.55 1 2 2 449.84 25.63 551.45 2 2 2 81.74 5.34 82.48 3 2 2 46.1 3.31 46.32 4 2 2 496.92 9.23 471.4 5 2 2 25.19 4.51 30.49 6 2 2 12.8 5.23 16.96 7 2 2 322.62 12.18 338.24 8 2 2 249.7 13.9 289.99 9 2 2 1.08 12.19 3.69 10 2 2 23.99 15.04 21.42 -10 3 2 -2.01 21.42 1.31 -9 3 2 23.05 15.35 40.39 -8 3 2 18.88 13.13 8.58 -7 3 2 7.2 10.84 8.8 -6 3 2 18.48 6.75 11.9 -5 3 2 208.58 8.66 187.67 -4 3 2 38.26 4.78 32.88 -3 3 2 4.86 4.05 11.56 -2 3 2 67.41 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2 93.79 15.29 106.97 -1 5 2 2.59 1.67 1.84 0 5 2 980.09 18.66 1121.38 1 5 2 603.46 17.35 588.63 2 5 2 2.69 2.12 5.22 3 5 2 213.44 18.42 220.98 4 5 2 222.53 8.36 219.01 5 5 2 2.51 5.92 0.61 6 5 2 121.47 7.8 135.47 7 5 2 163.69 12.32 160.59 8 5 2 6.39 9.41 9.55 9 5 2 13.96 12.69 2.59 10 5 2 4.96 15.89 2.3 -9 6 2 1.96 16.49 1.48 -8 6 2 77.3 17.04 71.13 -7 6 2 3.53 8.78 0.23 -6 6 2 2.32 8.32 0.36 -5 6 2 166.44 16.41 173.74 -4 6 2 120.81 10.61 118.82 -3 6 2 172.07 10.84 180.59 -2 6 2 981.79 43.51 1148.67 -1 6 2 35.9 4.59 33.98 0 6 2 249.5 15.03 290.48 1 6 2 7.76 7.81 5.62 2 6 2 4.55 2.39 2.86 3 6 2 72.52 7.54 57.8 4 6 2 87.39 7.06 77.62 5 6 2 146.49 9.02 144.68 6 6 2 -4.97 6.37 0.83 7 6 2 11.23 10.59 14.23 8 6 2 5.89 11.94 1.1 9 6 2 11.31 15.93 17.22 -8 7 2 146.62 24.17 137.7 -7 7 2 29 10.97 34.12 -6 7 2 580.32 34.64 736.59 -5 7 2 -2.07 8.25 0.87 -4 7 2 40.13 8.13 47.33 -3 7 2 380.92 11.17 423.33 -2 7 2 35.14 6.63 29.69 -1 7 2 66.65 3.19 75.94 0 7 2 5.45 8.9 3.12 1 7 2 5.83 9.51 0.01 2 7 2 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9 -5.92 20.78 0.14 -7 5 9 -3.09 17.75 10.2 -6 5 9 53.82 17.47 49.32 -5 5 9 -2.73 15.26 5.19 -4 5 9 153.8 13.03 177.44 -3 5 9 9.62 10.18 24.92 -2 5 9 41.52 9.43 41.39 -1 5 9 0.7 7.25 6.19 0 5 9 24.62 7.49 29.7 1 5 9 250.4 10 301.33 2 5 9 56.46 7.38 57.4 3 5 9 879.8 15.29 1022.2 4 5 9 379.3 21.59 400.41 5 5 9 15.53 8.11 10.85 6 5 9 8.52 8.74 3.71 7 5 9 21.54 10.52 30.61 8 5 9 5.49 15.83 8.03 9 5 9 -0.2 18.79 2.39 10 5 9 28.06 38.18 1.23 -7 6 9 -11.34 32.77 1.01 -6 6 9 -2.39 16.91 8.25 -5 6 9 66.96 14.21 74.26 -4 6 9 104.25 12.39 94.26 -3 6 9 174.79 12.49 173.79 -2 6 9 105.07 10.59 124.49 -1 6 9 0.75 7.42 3.46 0 6 9 11.95 7.73 16.79 1 6 9 63.88 7.39 78.77 2 6 9 113.26 15.83 137.97 3 6 9 52.97 9.74 54.71 4 6 9 54.6 9.43 51.31 5 6 9 21.56 8.9 23.03 6 6 9 42.33 12.3 18 7 6 9 69.15 13.57 54.24 8 6 9 136.6 15.72 127.02 9 6 9 64.47 35.75 38.5 -6 7 9 24.58 21.31 13.71 -5 7 9 24.76 14.41 13.59 -4 7 9 5.58 13.87 1.34 -3 7 9 98.14 14.14 107.68 -2 7 9 71.23 11.41 74.49 -1 7 9 -3.92 9.46 0.24 0 7 9 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13 4.98 20.81 6.56 1 1 13 46.48 17.65 37.27 2 1 13 8.35 16.18 5.22 3 1 13 7.94 15.58 0.05 4 1 13 25.29 12.06 19.53 5 1 13 5.03 17.45 6.26 6 1 13 7.33 17.56 6.61 7 1 13 57.02 18.93 55.12 -3 2 13 1.37 23.66 0 -2 2 13 82.32 25.48 60.04 -1 2 13 8.82 20.71 5.15 0 2 13 11.27 18.6 22.86 1 2 13 12.46 15.18 14.3 2 2 13 27.14 14.49 28.33 3 2 13 27.36 15.43 23.17 4 2 13 10.03 13.19 7.27 5 2 13 12.08 17.82 6.59 6 2 13 9.9 17.27 1.41 7 2 13 17.09 18.53 10.07 -3 3 13 57.63 21.82 54.57 -2 3 13 -1.86 21.06 1.86 -1 3 13 -0.07 19.76 0.08 0 3 13 -5.51 17.38 1.68 1 3 13 291.48 20.02 266.64 2 3 13 18.21 14.16 22.78 3 3 13 2.23 13.26 8.29 4 3 13 37.57 14.35 38.92 5 3 13 14.94 19.01 21.06 6 3 13 83.39 18.22 88.94 7 3 13 41.9 18.34 38.82 8 3 13 -7.42 25.81 2.67 -4 4 13 7.75 27.86 0.74 -3 4 13 20.33 19.99 33.98 -2 4 13 -3.31 21.73 2.34 -1 4 13 -2.95 17.11 0.02 0 4 13 18.91 17.76 6.99 1 4 13 30.16 14.99 41.64 2 4 13 15.07 13.72 14.41 3 4 13 71.82 14.81 90.69 4 4 13 51.88 12.68 41.51 5 4 13 149.28 25.46 125.67 6 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8 13 5.85 12.76 17.99 3 8 13 4.64 12.45 7.34 4 8 13 0.42 13.77 9.38 5 8 13 11.04 15.02 13.54 6 8 13 11.78 16.92 11.67 7 8 13 6.88 27.37 16.41 -2 9 13 -9.19 14.77 0.02 -1 9 13 -5.64 13.85 0.11 0 9 13 6.72 11.54 1.69 1 9 13 10.74 11.94 0.81 2 9 13 1.33 12.85 6.65 3 9 13 -4.01 13.02 2.93 4 9 13 64.09 14.9 62.67 5 9 13 7.1 15.78 0.29 6 9 13 0.71 33.26 3.16 -1 10 13 40.69 14.15 30.78 0 10 13 5.07 13.48 0.11 1 10 13 -4.2 12.53 1.68 2 10 13 -6.92 15.09 3.63 3 10 13 7.09 14.72 3.3 4 10 13 -3.74 15.66 1.91 5 10 13 4.72 28.36 7.54 0 -2 14 68.04 37.69 79.47 1 -2 14 66.13 40.02 53.48 2 -2 14 66.2 39.38 43.59 3 -2 14 81.16 24.52 62.96 1 -1 14 118.52 59.86 97.96 2 -1 14 48.47 26.08 53.65 3 -1 14 -8.36 28.72 2.15 0 0 14 172.55 27.64 139.11 1 0 14 87.1 25.42 64.81 2 0 14 -3.49 18.58 1.31 3 0 14 12.83 16.81 20.85 4 0 14 -16.71 17.57 1.19 5 0 14 55.18 29.58 28.09 6 0 14 15.65 33.31 9.28 -2 1 14 61.27 49.58 30.74 -1 1 14 -0.41 26.27 4.62 0 1 14 114.38 23.51 83.34 1 1 14 19.98 18.17 22.91 2 1 14 61.89 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