# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' sad in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 314.72 _exptl_crystal_F_000 1128.00 _reflns_d_resolution_high 0.8389 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' _cell_length_a 21.7307 _cell_length_b 8.1038 _cell_length_c 15.1428 _cell_angle_alpha 90.000 _cell_angle_beta 121.595 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11365.44 10964.54 282.90 o 4 0 0 32304.27 31597.26 807.97 o 6 0 0 2708.73 2438.19 89.59 o 8 0 0 30.97 180.22 38.77 o 10 0 0 21158.60 20922.43 572.35 o 12 0 0 68.64 184.93 61.56 o 14 0 0 752.10 834.17 95.48 o 16 0 0 2153.64 2375.46 146.69 o 18 0 0 1759.46 2200.74 146.43 o 20 0 0 9.57 70.59 82.77 o 22 0 0 45.84 460.50 121.67 o 1 1 0 15958.97 16082.02 238.84 o 3 1 0 8013.61 8538.46 131.49 o 5 1 0 11618.13 11523.53 271.64 o 7 1 0 1623.74 1486.08 48.70 o 9 1 0 3649.40 3753.64 96.50 o 11 1 0 1048.29 1188.70 123.31 o 13 1 0 1519.13 1811.15 121.74 o 15 1 0 571.54 621.33 123.11 o 17 1 0 188.35 182.95 82.77 o 19 1 0 346.62 264.51 64.45 o 21 1 0 93.93 76.75 91.94 o 0 2 0 5519.18 5948.40 165.94 o 2 2 0 20814.46 21722.10 327.24 o 4 2 0 42755.70 43288.64 552.18 o 6 2 0 2550.83 2819.09 144.56 o 8 2 0 492.55 461.57 33.00 o 10 2 0 1243.41 1194.61 55.33 o 12 2 0 149.83 -33.29 183.56 o 14 2 0 195.82 220.45 140.21 o 16 2 0 556.19 511.97 93.51 o 18 2 0 89.55 -74.26 74.26 o 20 2 0 65.16 -76.23 76.23 o 1 3 0 2419.98 1978.02 47.75 o 3 3 0 196.43 251.89 22.83 o 5 3 0 9907.25 9970.41 301.04 o 7 3 0 221.09 144.69 19.68 o 9 3 0 1740.87 1836.00 107.27 o 11 3 0 3301.57 3603.05 101.68 o 13 3 0 1001.61 1097.03 113.42 o 15 3 0 691.70 746.02 97.31 o 17 3 0 19.26 101.64 80.81 o 19 3 0 255.04 138.05 94.56 o 0 4 0 1762.03 1312.68 132.68 o 2 4 0 3239.64 3019.15 54.83 o 4 4 0 12344.86 12789.16 212.25 o 6 4 0 25292.49 25128.08 829.12 o 8 4 0 243.17 223.13 33.77 o 10 4 0 1226.41 1138.16 98.30 o 12 4 0 525.29 565.97 69.87 o 14 4 0 162.12 -22.00 72.69 o 16 4 0 420.93 362.80 94.17 o 18 4 0 3.73 51.73 88.80 o 20 4 0 414.44 655.00 140.27 o 1 5 0 3018.18 2781.66 98.47 o 3 5 0 3817.74 3885.77 213.43 o 5 5 0 1666.33 1528.16 55.77 o 7 5 0 2582.74 2524.94 75.61 o 9 5 0 4544.52 4297.42 232.96 o 11 5 0 165.53 561.98 199.47 o 13 5 0 470.54 318.66 84.08 o 15 5 0 483.21 340.79 91.16 o 17 5 0 126.36 275.44 113.95 o 0 6 0 6535.86 7292.58 263.91 o 2 6 0 3307.69 3135.24 85.73 o 4 6 0 341.77 359.18 77.81 o 6 6 0 575.39 590.83 48.92 o 8 6 0 44.55 34.97 92.24 o 10 6 0 1721.04 1546.49 214.23 o 12 6 0 2.27 466.13 108.18 o 14 6 0 60.56 32.22 83.69 o 16 6 0 90.40 352.84 110.54 o 1 7 0 285.13 153.31 53.11 o 3 7 0 872.50 779.41 72.50 o 5 7 0 26.93 52.00 52.13 o 7 7 0 467.00 451.56 58.09 o 9 7 0 117.55 261.31 84.93 o 11 7 0 956.16 773.66 119.05 o 13 7 0 3.09 343.54 116.44 o 15 7 0 77.44 -90.11 90.11 o 0 8 0 1399.27 1162.12 114.60 o 2 8 0 2061.71 2074.50 116.30 o 4 8 0 965.71 1088.12 84.66 o 6 8 0 398.28 400.72 110.08 o 8 8 0 951.43 1230.23 103.44 o 10 8 0 253.33 223.83 97.97 o 12 8 0 1076.05 1046.47 160.31 o 1 9 0 400.68 482.45 79.35 o 3 9 0 1525.98 2013.44 117.98 o 5 9 0 458.94 430.66 116.70 o 7 9 0 843.34 1020.95 106.92 o -21 1 1 3.38 126.52 103.99 o -19 1 1 642.10 747.41 80.78 o -17 1 1 2948.56 3431.56 197.77 o -15 1 1 1459.90 1647.93 79.52 o -13 1 1 14.45 -41.93 53.83 o -11 1 1 800.73 763.03 48.16 o -9 1 1 8548.91 7784.34 165.88 o -7 1 1 2912.50 2565.82 54.85 o -5 1 1 7902.32 6663.15 164.18 o -3 1 1 1374.73 1184.67 29.71 o -1 1 1 4284.59 4750.39 85.79 o 1 1 1 8888.96 9188.26 244.51 o 3 1 1 50883.34 50530.82 864.50 o 5 1 1 13646.35 14101.74 268.25 o 7 1 1 1085.63 1054.11 44.79 o 9 1 1 9026.86 9250.53 381.59 o 11 1 1 8868.55 9460.39 259.85 o 13 1 1 223.47 435.12 85.98 o 15 1 1 238.61 107.64 68.50 o 17 1 1 143.78 334.56 58.71 o 19 1 1 290.27 333.33 100.85 o 21 1 1 5.79 -91.16 91.16 o -22 2 1 287.87 405.49 123.38 o -20 2 1 495.77 455.13 114.73 o -18 2 1 652.31 1293.23 144.07 o -16 2 1 1035.53 1584.45 98.10 o -14 2 1 5373.58 5662.85 567.44 o -12 2 1 421.28 337.61 41.41 o -10 2 1 5661.68 5867.85 137.71 o -8 2 1 5767.68 5985.80 256.90 o -6 2 1 448.70 293.17 24.83 o -4 2 1 65022.96 63200.82 801.35 o -2 2 1 4674.87 3898.48 129.74 o 0 2 1 9764.37 9048.68 177.04 o 2 2 1 32533.50 33055.18 835.31 o 4 2 1 223.92 214.51 25.49 o 6 2 1 22174.49 22101.41 290.62 o 8 2 1 151.96 184.27 25.88 o 10 2 1 3288.94 4127.39 179.76 o 12 2 1 3851.55 4412.23 221.87 o 14 2 1 811.41 1019.24 396.26 o 16 2 1 261.77 251.47 74.00 o 18 2 1 414.64 511.71 105.04 o 20 2 1 552.51 712.10 119.45 o -21 3 1 404.53 792.39 127.17 o -19 3 1 168.24 17.55 83.95 o -17 3 1 390.43 1009.28 140.67 o -15 3 1 240.12 261.03 96.40 o -13 3 1 6209.20 5621.50 221.34 o -11 3 1 7749.12 7923.38 398.75 o -9 3 1 5824.76 6655.71 192.47 o -7 3 1 11175.69 11907.92 275.11 o -5 3 1 14438.82 14297.95 268.20 o -3 3 1 5364.07 5200.62 127.45 o -1 3 1 769.82 883.30 35.60 o 1 3 1 1322.21 1437.48 83.58 o 3 3 1 1140.70 1044.18 73.21 o 5 3 1 22309.22 22544.21 323.93 o 7 3 1 1830.47 1650.78 36.89 o 9 3 1 186.41 256.35 55.31 o 11 3 1 900.03 1045.03 98.88 o 13 3 1 1959.98 1998.78 130.32 o 15 3 1 3573.95 3489.12 183.36 o 17 3 1 705.54 797.76 116.83 o 19 3 1 303.09 384.93 118.53 o -20 4 1 27.64 407.33 131.76 o -18 4 1 254.09 63.91 87.88 o -16 4 1 26.25 246.23 103.73 o -14 4 1 310.59 370.92 102.81 o -12 4 1 876.92 1080.61 83.82 o -10 4 1 557.65 411.55 44.92 o -8 4 1 8947.48 9077.39 245.37 o -6 4 1 3423.41 3256.42 84.36 o -4 4 1 885.89 657.43 43.23 o -2 4 1 1856.42 1587.21 42.08 o 0 4 1 297.23 226.20 44.22 o 2 4 1 1753.93 1443.60 133.88 o 4 4 1 4592.58 5050.79 101.60 o 6 4 1 1670.08 1393.94 71.65 o 8 4 1 218.47 197.58 30.18 o 10 4 1 185.64 469.02 134.64 o 12 4 1 50.79 145.77 67.45 o 14 4 1 150.95 174.59 75.31 o 16 4 1 940.80 864.42 118.92 o 18 4 1 86.63 340.92 117.09 o -19 5 1 35.72 111.20 99.80 o -17 5 1 4.69 213.36 105.30 o -15 5 1 218.32 300.19 95.74 o -13 5 1 9.42 107.22 209.56 o -11 5 1 1249.64 1296.30 76.81 o -9 5 1 1199.92 1416.83 141.89 o -7 5 1 416.71 467.38 73.18 o -5 5 1 6592.67 7094.64 326.48 o -3 5 1 825.36 1422.08 315.28 o -1 5 1 14.29 12.71 37.55 o 1 5 1 602.67 505.53 84.12 o 3 5 1 1703.34 1593.98 55.75 o 5 5 1 6011.11 6338.01 163.85 o 7 5 1 3575.40 3381.78 101.06 o 9 5 1 64.74 -18.58 44.36 o 11 5 1 125.90 70.73 71.77 o 13 5 1 358.63 278.71 81.20 o 15 5 1 337.64 172.23 89.19 o 17 5 1 126.22 -28.42 101.77 o -18 6 1 231.75 368.17 111.46 o -16 6 1 396.67 674.51 132.54 o -14 6 1 489.86 870.32 118.53 o -12 6 1 242.65 508.24 237.52 o -10 6 1 3628.33 3643.71 240.14 o -8 6 1 460.93 479.64 76.34 o -6 6 1 501.74 469.11 58.82 o -4 6 1 1464.01 1403.89 73.01 o -2 6 1 5295.06 5611.76 156.05 o 0 6 1 10576.22 11612.77 260.89 o 2 6 1 5409.33 5552.86 120.49 o 4 6 1 4335.81 4341.15 113.62 o 6 6 1 2590.69 2622.95 128.31 o 8 6 1 4564.98 4471.07 226.89 o 10 6 1 128.13 83.52 53.11 o 12 6 1 276.23 360.83 105.43 o 14 6 1 169.91 540.26 120.50 o 16 6 1 402.43 513.02 136.34 o -15 7 1 401.55 865.99 143.94 o -13 7 1 1678.78 1769.32 157.95 o -11 7 1 838.98 1036.60 370.00 o -9 7 1 376.04 326.06 107.45 o -7 7 1 1531.71 1666.13 85.58 o -5 7 1 163.80 243.61 64.64 o -3 7 1 1213.86 1230.22 156.64 o -1 7 1 2040.97 2354.78 108.49 o 1 7 1 819.54 983.22 186.90 o 3 7 1 735.61 704.64 66.21 o 5 7 1 12.86 70.54 38.96 o 7 7 1 61.03 115.88 141.47 o 9 7 1 518.90 664.09 84.29 o 11 7 1 1485.32 1406.13 154.02 o 13 7 1 103.59 142.76 111.33 o -12 8 1 1.54 372.36 129.14 o -10 8 1 58.23 -97.97 97.97 o -8 8 1 714.12 889.02 102.58 o -6 8 1 84.43 107.04 70.30 o -4 8 1 1156.26 1297.26 100.01 o -2 8 1 16.62 -50.42 50.42 o 0 8 1 270.85 209.79 60.75 o 2 8 1 15.07 131.34 59.07 o 4 8 1 4.94 -23.06 237.45 o 6 8 1 4.36 -59.78 59.78 o 8 8 1 69.58 156.95 248.91 o 10 8 1 6.64 -65.72 84.28 o -7 9 1 52.55 55.49 73.75 o -5 9 1 112.27 205.04 136.74 o -3 9 1 16.96 47.97 150.68 o -1 9 1 50.03 378.96 197.44 o 1 9 1 77.41 10.83 67.09 o 3 9 1 50.31 -48.42 101.31 o 5 9 1 60.15 67.55 73.79 o 7 9 1 4.10 197.62 79.68 o -22 0 2 7.48 32.22 112.64 o -20 0 2 4.92 19.78 94.56 o -18 0 2 1762.57 1771.28 134.12 o -16 0 2 362.10 313.94 79.89 o -14 0 2 2886.42 2720.31 133.46 o -12 0 2 1508.69 1568.84 136.87 o -10 0 2 5241.45 4411.17 152.58 o -8 0 2 2736.27 2468.97 98.36 o -6 0 2 293.49 201.31 28.95 o -4 0 2 201.70 362.40 25.54 o -2 0 2 57718.42 64374.85 1623.67 o 0 0 2 10200.18 10271.70 270.46 o 2 0 2 99047.47 93023.57 1652.65 o 4 0 2 45295.61 44228.04 1133.57 o 6 0 2 34357.00 32700.97 852.63 o 8 0 2 36842.98 36183.02 947.46 o 10 0 2 7417.40 7430.50 238.24 o 12 0 2 3362.35 3588.66 153.76 o 14 0 2 207.53 187.82 74.39 o 16 0 2 136.29 284.34 86.31 o 18 0 2 3.31 -84.08 84.08 o 20 0 2 590.05 775.36 128.22 o -23 1 2 6.54 200.52 114.34 o -21 1 2 928.19 1195.80 108.83 o -19 1 2 37.70 -140.27 140.27 o -17 1 2 909.02 947.71 74.34 o -15 1 2 1542.00 1574.98 79.92 o -13 1 2 1341.30 1303.82 113.55 o -11 1 2 1855.90 1879.60 58.72 o -9 1 2 3725.85 3197.54 248.19 o -7 1 2 1194.69 946.24 37.68 o -5 1 2 11971.93 10526.50 1018.91 o -3 1 2 9201.64 9721.50 336.60 o -1 1 2 18.43 7.75 25.87 o 1 1 2 24488.61 23417.53 299.99 o 3 1 2 7320.87 6789.77 128.36 o 5 1 2 7170.88 6632.51 209.97 o 7 1 2 9318.12 9865.65 204.29 o 9 1 2 100.06 109.48 30.43 o 11 1 2 4269.53 4481.27 124.42 o 13 1 2 162.58 145.60 54.16 o 15 1 2 1019.85 1240.29 215.52 o 17 1 2 3.22 23.74 145.38 o 19 1 2 507.78 1108.16 158.35 o -22 2 2 228.26 455.00 126.91 o -20 2 2 30.78 165.81 119.84 o -18 2 2 45.63 221.08 84.08 o -16 2 2 54.91 34.06 42.86 o -14 2 2 110.86 -19.75 39.96 o -12 2 2 273.88 232.66 69.35 o -10 2 2 355.68 259.81 38.35 o -8 2 2 296.17 334.93 85.00 o -6 2 2 2400.88 2481.53 61.62 o -4 2 2 16490.41 17463.69 631.81 o -2 2 2 5163.42 5306.71 128.96 o 0 2 2 8134.96 9211.31 126.04 o 2 2 2 3370.62 3423.50 53.47 o 4 2 2 4964.98 5197.76 78.03 o 6 2 2 56.20 92.01 41.16 o 8 2 2 389.15 486.13 61.32 o 10 2 2 1924.12 1949.22 73.96 o 12 2 2 71.32 60.59 47.94 o 14 2 2 40.75 58.81 65.36 o 16 2 2 142.38 10.61 84.22 o 18 2 2 15.28 -60.64 86.18 o -21 3 2 128.70 110.28 130.32 o -19 3 2 47.75 93.12 101.90 o -17 3 2 89.29 215.84 82.91 o -15 3 2 2497.56 2796.01 162.14 o -13 3 2 399.75 355.21 108.97 o -11 3 2 595.08 650.29 54.09 o -9 3 2 3914.95 3733.93 96.51 o -7 3 2 1151.68 1281.27 38.11 o -5 3 2 24164.46 22947.48 348.84 o -3 3 2 3126.96 2998.64 176.38 o -1 3 2 776.60 795.04 94.11 o 1 3 2 4813.64 4183.58 68.96 o 3 3 2 1041.37 854.10 22.58 o 5 3 2 3417.37 3311.84 73.86 o 7 3 2 44.88 128.53 72.51 o 9 3 2 292.68 360.01 149.93 o 11 3 2 299.19 343.54 68.11 o 13 3 2 1821.84 1538.67 118.14 o 15 3 2 93.25 67.98 78.19 o 17 3 2 224.22 18.34 92.86 o 19 3 2 122.59 -105.30 105.30 o -20 4 2 139.15 367.12 129.01 o -18 4 2 176.21 403.27 115.65 o -16 4 2 729.32 1011.77 124.69 o -14 4 2 671.49 984.66 111.33 o -12 4 2 3462.02 4059.25 183.89 o -10 4 2 131.90 85.92 67.32 o -8 4 2 7598.87 7560.75 174.43 o -6 4 2 20.73 50.75 26.28 o -4 4 2 4286.75 3831.13 201.27 o -2 4 2 1331.90 1171.57 36.09 o 0 4 2 1986.24 1714.86 38.92 o 2 4 2 12439.40 13001.17 181.01 o 4 4 2 11186.25 10413.99 179.82 o 6 4 2 9342.59 9347.28 166.83 o 8 4 2 1657.63 1340.77 67.08 o 10 4 2 715.76 665.34 85.53 o 12 4 2 54.47 142.63 71.90 o 14 4 2 1154.51 1587.66 139.88 o 16 4 2 230.60 17.29 82.25 o 18 4 2 30.09 415.58 135.82 o -19 5 2 563.26 185.98 104.65 o -17 5 2 1122.74 1749.41 170.53 o -15 5 2 437.22 527.56 114.99 o -13 5 2 15.61 -124.23 124.23 o -11 5 2 3095.22 3477.93 114.73 o -9 5 2 1830.87 1747.30 79.86 o -7 5 2 1816.47 1743.58 61.56 o -5 5 2 553.20 418.65 55.83 o -3 5 2 4518.94 4519.53 82.98 o -1 5 2 9731.79 9849.79 147.30 o 1 5 2 4647.15 4920.90 180.13 o 3 5 2 483.08 395.23 38.38 o 5 5 2 540.45 471.14 39.76 o 7 5 2 3010.76 2832.25 79.86 o 9 5 2 1815.17 2032.21 91.58 o 11 5 2 525.99 707.25 104.39 o 13 5 2 629.17 692.98 118.14 o 15 5 2 66.48 147.61 106.87 o 17 5 2 598.74 957.28 158.87 o -18 6 2 347.01 330.97 113.29 o -16 6 2 84.23 -90.37 90.37 o -14 6 2 201.35 5.50 88.80 o -12 6 2 2271.35 2571.96 113.92 o -10 6 2 3070.07 3536.39 229.60 o -8 6 2 2110.43 2076.10 79.06 o -6 6 2 111.38 113.12 40.82 o -4 6 2 72.34 194.34 56.61 o -2 6 2 7372.09 7026.21 179.25 o 0 6 2 385.49 356.88 38.16 o 2 6 2 2550.23 2619.34 98.14 o 4 6 2 567.66 513.23 64.69 o 6 6 2 126.28 53.16 51.86 o 8 6 2 1549.69 1759.71 141.03 o 10 6 2 1954.27 1507.28 94.82 o 12 6 2 498.89 539.09 119.45 o 14 6 2 14.47 -91.42 95.35 o -15 7 2 26.57 735.02 134.25 o -13 7 2 4.56 251.75 164.50 o -11 7 2 88.05 249.53 228.55 o -9 7 2 1565.76 1548.20 162.60 o -7 7 2 56.75 342.57 204.65 o -5 7 2 268.77 186.88 129.40 o -3 7 2 484.85 386.76 94.82 o -1 7 2 522.19 540.39 60.83 o 1 7 2 8.98 41.05 128.88 o 3 7 2 1226.51 1318.51 79.94 o 5 7 2 1336.98 1499.56 106.37 o 7 7 2 94.75 6.22 41.27 o 9 7 2 2.83 184.95 59.36 o 11 7 2 0.65 131.27 148.39 o 13 7 2 13.56 -42.17 95.48 o -12 8 2 10.71 133.33 146.82 o -10 8 2 728.23 973.26 149.18 o -8 8 2 61.02 59.91 243.35 o -6 8 2 1871.13 2056.29 222.98 o -4 8 2 1034.11 986.16 90.85 o -2 8 2 1446.00 1436.75 97.95 o 0 8 2 2199.30 2019.84 183.49 o 2 8 2 572.02 554.41 75.06 o 4 8 2 960.59 842.34 82.61 o 6 8 2 108.16 -58.99 58.99 o 8 8 2 818.12 620.29 118.53 o 10 8 2 1279.03 856.97 158.28 o -9 9 2 477.50 206.41 144.07 o -7 9 2 1138.85 1441.31 213.88 o -5 9 2 1334.84 1485.68 133.00 o -3 9 2 811.82 891.11 132.94 o -1 9 2 619.01 589.35 160.11 o 1 9 2 455.01 395.72 214.93 o 3 9 2 1025.06 1035.65 266.14 o 5 9 2 774.52 873.51 182.64 o -23 1 3 146.56 78.58 112.51 o -21 1 3 710.65 680.36 351.73 o -19 1 3 5336.36 5858.15 171.42 o -17 1 3 1199.37 1618.80 90.71 o -15 1 3 1586.56 1567.32 61.38 o -13 1 3 893.52 738.21 55.98 o -11 1 3 2069.06 2240.62 135.30 o -9 1 3 10626.64 10494.87 214.57 o -7 1 3 1164.75 886.34 78.13 o -5 1 3 4615.57 4692.94 244.13 o -3 1 3 56028.05 61237.49 1097.67 o -1 1 3 16329.41 15563.90 289.74 o 1 1 3 970.20 985.58 39.24 o 3 1 3 6123.37 5956.71 100.93 o 5 1 3 1172.80 1311.72 43.30 o 7 1 3 249.90 425.12 70.01 o 9 1 3 12.60 -40.73 40.73 o 11 1 3 17.02 -30.47 30.47 o 13 1 3 3.93 14.60 58.48 o 15 1 3 716.22 865.47 125.67 o 17 1 3 8.05 161.36 87.36 o 19 1 3 26.73 -93.91 93.91 o -22 2 3 756.50 1150.47 156.91 o -20 2 3 944.59 996.57 135.16 o -18 2 3 38.88 -42.76 171.44 o -16 2 3 4222.65 3972.39 154.48 o -14 2 3 3415.42 3219.39 178.84 o -12 2 3 4683.38 4196.46 211.46 o -10 2 3 7831.22 7411.50 586.24 o -8 2 3 2002.34 1702.36 105.11 o -6 2 3 12584.57 9641.47 1757.00 o -4 2 3 9049.73 8753.80 172.18 o -2 2 3 2924.06 2791.25 95.87 o 0 2 3 10410.27 11123.88 151.95 o 2 2 3 4077.10 3394.42 72.96 o 4 2 3 6519.81 6546.87 95.95 o 6 2 3 4007.06 3772.22 62.42 o 8 2 3 1267.11 1340.08 54.50 o 10 2 3 2210.87 2113.29 212.11 o 12 2 3 735.11 610.07 54.04 o 14 2 3 547.41 781.12 112.77 o 16 2 3 696.80 673.73 117.74 o 18 2 3 64.46 57.63 86.05 o -21 3 3 315.20 653.29 135.03 o -19 3 3 74.10 -59.59 84.22 o -17 3 3 10.77 9.17 75.96 o -15 3 3 5000.76 4488.71 199.86 o -13 3 3 3060.98 2943.64 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