# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # #data_u4 data_I _shelx_title ' U4' _shelx_refln_list_code 4 _shelx_F_calc_maximum 86.24 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.7299 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.0522 _cell_length_b 9.9537 _cell_length_c 9.9895 _cell_angle_alpha 83.607 _cell_angle_beta 80.386 _cell_angle_gamma 89.477 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 135.82 166.09 2.45 o 3 0 0 335.77 316.77 1.95 o 4 0 0 713.45 816.57 4.30 o 5 0 0 97.37 92.84 1.47 o 6 0 0 28.42 26.24 1.12 o 7 0 0 10.54 9.39 1.09 o 8 0 0 64.24 68.60 2.41 o 9 0 0 10.68 13.14 1.30 o -9 1 0 123.17 122.31 2.07 o -8 1 0 44.26 41.30 1.46 o -7 1 0 111.21 106.49 1.52 o -6 1 0 63.17 67.90 1.06 o -5 1 0 17.16 17.03 0.92 o -4 1 0 1480.13 1551.99 14.17 o -3 1 0 91.95 93.49 1.16 o -2 1 0 2798.08 2958.64 20.88 o -1 1 0 0.99 5.97 1.85 o 1 1 0 0.55 7.39 1.73 o 2 1 0 784.00 776.00 4.19 o 3 1 0 128.91 134.87 1.35 o 4 1 0 295.09 291.31 2.25 o 5 1 0 5.78 4.63 0.93 o 6 1 0 175.61 175.65 2.64 o 7 1 0 279.95 270.29 2.89 o 8 1 0 15.20 17.64 1.07 o 9 1 0 305.40 307.57 2.65 o -9 2 0 135.81 131.50 7.29 o -8 2 0 152.44 146.68 3.31 o -7 2 0 54.97 55.63 1.80 o -6 2 0 470.39 468.02 4.49 o -5 2 0 5.34 5.48 0.95 o -4 2 0 127.18 120.41 1.65 o -3 2 0 33.58 27.06 1.08 o -2 2 0 47.68 44.63 1.25 o -1 2 0 27.71 16.42 1.60 o 0 2 0 0.19 0.22 1.81 o 1 2 0 232.09 244.89 4.72 o 2 2 0 14.86 15.11 1.41 o 3 2 0 91.03 93.19 1.52 o 4 2 0 67.51 60.61 1.35 o 5 2 0 43.89 36.14 1.09 o 6 2 0 0.88 0.55 0.85 o 7 2 0 107.09 101.77 2.48 o 8 2 0 100.91 104.77 1.68 o 9 2 0 22.56 20.81 1.88 o -9 3 0 2.87 1.50 3.85 o -8 3 0 11.94 14.61 1.59 o -7 3 0 206.72 201.58 4.76 o -6 3 0 8.99 13.81 0.98 o -5 3 0 464.11 449.59 4.64 o -4 3 0 11.68 12.31 0.96 o -3 3 0 369.20 353.46 3.76 o -2 3 0 83.62 74.92 1.53 o -1 3 0 410.76 461.69 8.43 o 0 3 0 1690.87 1583.32 44.48 o 1 3 0 3382.84 3333.18 80.15 o 2 3 0 322.95 299.05 4.10 o 3 3 0 1751.19 1694.93 18.89 o 4 3 0 215.36 213.38 3.65 o 5 3 0 156.94 158.68 1.43 o 6 3 0 280.12 281.12 3.31 o 7 3 0 1.12 -0.20 0.93 o 8 3 0 17.82 17.00 1.08 o 9 3 0 19.23 17.31 1.34 o -9 4 0 388.32 369.92 7.57 o -8 4 0 2.19 3.99 1.33 o -7 4 0 520.70 513.99 9.79 o -6 4 0 15.44 19.13 1.06 o -5 4 0 234.98 238.74 3.50 o -4 4 0 402.17 438.66 5.27 o -3 4 0 37.49 30.68 1.12 o -2 4 0 1321.85 1377.16 24.71 o -1 4 0 830.93 798.46 19.35 o 0 4 0 92.77 99.01 1.54 o 1 4 0 122.40 112.86 2.56 o 2 4 0 813.66 771.89 14.70 o 3 4 0 89.13 91.74 1.79 o 4 4 0 214.67 199.16 2.72 o 5 4 0 343.56 335.31 6.58 o 6 4 0 88.25 85.27 1.47 o 7 4 0 524.66 513.41 9.91 o 8 4 0 343.47 321.47 4.11 o 9 4 0 357.27 342.80 18.87 o -8 5 0 87.41 86.63 2.61 o -7 5 0 227.66 230.35 3.91 o -6 5 0 287.86 293.56 3.64 o -5 5 0 926.50 921.57 9.70 o -4 5 0 90.43 96.75 1.59 o -3 5 0 947.15 930.14 12.88 o -2 5 0 183.37 168.92 1.75 o -1 5 0 253.37 289.84 4.20 o 0 5 0 760.06 754.27 15.64 o 1 5 0 226.58 273.37 2.41 o 2 5 0 206.51 199.46 4.65 o 3 5 0 133.92 154.64 1.59 o 4 5 0 6.14 6.05 1.41 o 5 5 0 18.19 15.32 1.05 o 6 5 0 9.47 10.04 1.16 o 7 5 0 54.08 53.58 1.37 o 8 5 0 37.70 36.07 1.29 o -8 6 0 107.27 107.69 4.67 o -7 6 0 166.11 165.19 2.25 o -6 6 0 11.90 12.90 0.89 o -5 6 0 135.74 127.76 1.59 o -4 6 0 42.93 39.01 2.31 o -3 6 0 16.97 17.21 1.04 o -2 6 0 0.17 2.59 1.40 o -1 6 0 0.10 1.97 1.11 o 0 6 0 40.62 48.95 1.51 o 1 6 0 22.95 12.46 1.23 o 2 6 0 17.74 23.65 1.13 o 3 6 0 147.12 136.34 3.04 o 4 6 0 27.78 30.01 1.40 o 5 6 0 3.36 1.72 1.02 o 6 6 0 46.74 45.88 1.05 o 7 6 0 72.77 75.63 1.25 o 8 6 0 21.46 20.97 1.23 o -8 7 0 11.98 9.58 1.39 o -7 7 0 88.90 90.09 2.07 o -6 7 0 24.23 23.13 1.13 o -5 7 0 54.30 55.82 1.12 o -4 7 0 59.91 59.79 1.18 o -3 7 0 12.76 14.49 1.03 o -2 7 0 74.08 72.55 1.34 o -1 7 0 290.86 286.25 5.98 o 0 7 0 42.06 42.96 2.24 o 1 7 0 29.20 30.97 1.11 o 2 7 0 645.49 617.63 11.44 o 3 7 0 280.36 271.85 2.00 o 4 7 0 483.24 463.92 7.77 o 5 7 0 389.01 376.89 2.45 o 6 7 0 14.23 13.23 1.69 o 7 7 0 77.21 77.55 1.38 o 8 7 0 41.18 40.12 1.32 o -7 8 0 310.23 305.43 3.46 o -6 8 0 34.84 33.56 1.17 o -5 8 0 469.43 469.54 7.74 o -4 8 0 25.01 24.96 1.15 o -3 8 0 137.15 133.52 3.40 o -2 8 0 142.34 140.49 3.39 o -1 8 0 274.81 261.89 6.07 o 0 8 0 435.31 437.62 10.37 o 1 8 0 1390.33 1326.48 22.57 o 2 8 0 106.78 107.38 1.53 o 3 8 0 807.27 801.76 4.90 o 4 8 0 50.58 47.30 1.60 o 5 8 0 220.57 227.06 2.40 o 6 8 0 243.85 242.45 4.37 o 7 8 0 29.60 27.80 1.36 o -7 9 0 328.41 331.54 4.54 o -6 9 0 19.40 22.00 1.48 o -5 9 0 63.88 61.88 1.11 o -4 9 0 17.80 19.42 1.09 o -3 9 0 50.71 48.52 1.21 o -2 9 0 235.46 223.45 5.14 o -1 9 0 12.01 11.14 1.75 o 0 9 0 786.89 742.62 7.90 o 1 9 0 68.72 68.64 2.07 o 2 9 0 1056.27 1009.23 13.50 o 3 9 0 22.50 22.32 1.11 o 4 9 0 792.73 760.77 7.88 o 5 9 0 0.19 1.31 1.07 o 6 9 0 276.69 275.03 1.65 o 7 9 0 27.48 26.24 1.72 o -6 10 0 55.87 54.11 1.81 o -5 10 0 58.55 59.22 1.25 o -4 10 0 83.33 78.93 1.37 o -3 10 0 106.60 102.71 1.55 o -2 10 0 0.88 0.77 1.01 o -1 10 0 106.20 98.15 1.88 o 0 10 0 104.71 100.49 1.42 o 1 10 0 64.45 57.86 1.27 o 2 10 0 252.65 242.60 4.09 o 3 10 0 0.02 1.15 1.05 o 4 10 0 90.19 94.39 1.36 o 5 10 0 28.87 32.55 2.04 o 6 10 0 1.07 2.54 1.24 o -5 11 0 7.75 9.45 1.19 o -4 11 0 106.10 111.02 1.72 o -3 11 0 53.03 53.94 1.34 o -2 11 0 308.20 315.72 3.89 o -1 11 0 5.80 4.06 0.90 o 0 11 0 429.08 428.90 6.98 o 1 11 0 74.31 79.56 1.87 o 2 11 0 97.06 95.52 2.07 o 3 11 0 67.03 69.08 1.17 o 4 11 0 22.35 26.37 1.62 o 5 11 0 7.25 6.71 1.34 o -4 12 0 73.48 73.59 1.41 o -3 12 0 23.82 26.13 1.47 o -2 12 0 23.68 26.24 1.05 o -1 12 0 0.05 0.91 1.09 o 0 12 0 1.74 1.08 1.23 o 1 12 0 163.10 167.20 1.78 o 2 12 0 63.49 67.24 3.22 o 3 12 0 261.98 272.45 2.45 o 4 12 0 137.76 142.47 1.88 o -2 13 0 217.04 223.53 7.64 o -1 13 0 1.58 3.96 1.21 o 0 13 0 429.71 443.72 5.40 o 1 13 0 10.59 11.85 1.40 o 2 13 0 405.14 413.43 4.65 o -2 -13 1 25.08 26.59 1.64 o -1 -13 1 24.30 28.05 1.39 o 0 -13 1 14.20 14.08 1.25 o 1 -13 1 0.16 1.24 1.07 o 2 -13 1 6.99 9.54 1.05 o -4 -12 1 255.58 236.38 2.93 o -3 -12 1 8.27 6.03 1.22 o -2 -12 1 98.50 100.50 1.63 o -1 -12 1 4.18 7.16 1.12 o 0 -12 1 1.17 1.36 1.28 o 1 -12 1 9.15 12.70 1.16 o 2 -12 1 27.05 25.88 1.40 o 3 -12 1 1.50 2.13 1.17 o 4 -12 1 1.85 3.17 1.23 o -5 -11 1 0.65 1.33 1.12 o -4 -11 1 11.74 12.73 1.32 o -3 -11 1 17.71 15.81 1.70 o -2 -11 1 9.67 12.27 1.60 o -1 -11 1 124.32 124.26 2.80 o 0 -11 1 104.10 99.14 1.39 o 1 -11 1 33.92 34.00 1.87 o 2 -11 1 48.58 47.58 1.07 o 3 -11 1 67.84 70.05 1.89 o 4 -11 1 20.50 21.00 1.18 o 5 -11 1 114.93 119.21 1.55 o -6 -10 1 15.28 15.20 1.03 o -5 -10 1 40.31 44.46 1.35 o -4 -10 1 14.75 17.32 1.26 o -3 -10 1 21.50 22.92 1.99 o -2 -10 1 172.03 176.42 2.57 o -1 -10 1 16.13 15.54 1.01 o 0 -10 1 215.77 209.85 5.07 o 1 -10 1 80.08 84.73 1.53 o 2 -10 1 22.32 19.22 1.18 o 3 -10 1 36.43 38.17 1.24 o 4 -10 1 55.96 58.13 2.34 o 5 -10 1 3.14 4.28 1.23 o 6 -10 1 164.77 166.32 2.47 o -6 -9 1 2.30 4.72 1.32 o -5 -9 1 58.28 57.20 1.60 o -4 -9 1 4.44 5.45 1.20 o -3 -9 1 235.18 236.33 2.24 o -2 -9 1 49.89 51.58 1.34 o -1 -9 1 9.03 9.39 1.35 o 0 -9 1 271.87 257.69 2.69 o 1 -9 1 107.01 100.10 1.46 o 2 -9 1 288.01 290.02 3.33 o 3 -9 1 25.01 24.51 1.26 o 4 -9 1 118.29 120.82 2.50 o 5 -9 1 0.38 0.14 1.27 o 6 -9 1 2.81 4.22 1.26 o 7 -9 1 27.55 27.37 1.41 o -7 -8 1 55.42 52.46 1.37 o -6 -8 1 45.46 45.62 1.13 o -5 -8 1 266.85 259.15 4.41 o -4 -8 1 0.18 0.91 1.12 o -3 -8 1 839.45 799.01 8.92 o -2 -8 1 209.48 204.36 2.61 o -1 -8 1 785.56 738.07 10.11 o 0 -8 1 684.82 652.36 12.25 o 1 -8 1 146.71 139.83 2.08 o 2 -8 1 289.40 277.80 4.63 o 3 -8 1 17.05 17.54 1.15 o 4 -8 1 2.39 2.59 1.16 o 5 -8 1 0.75 0.90 1.03 o 6 -8 1 36.10 33.06 1.14 o 7 -8 1 69.41 71.10 1.66 o -7 -7 1 0.08 0.46 1.12 o -6 -7 1 13.11 13.04 1.20 o -5 -7 1 6.29 7.90 1.04 o -4 -7 1 66.64 63.16 1.59 o -3 -7 1 16.45 16.70 1.24 o -2 -7 1 432.76 409.93 5.30 o -1 -7 1 8.19 6.55 0.96 o 0 -7 1 309.21 297.29 5.69 o 1 -7 1 124.75 125.27 1.51 o 2 -7 1 2.16 4.03 1.17 o 3 -7 1 119.03 123.00 1.75 o 4 -7 1 81.40 81.30 1.12 o 5 -7 1 70.91 70.64 1.54 o 6 -7 1 4.19 3.38 0.89 o 7 -7 1 342.30 346.76 4.69 o 8 -7 1 18.09 16.84 1.22 o -8 -6 1 58.66 59.39 1.31 o -7 -6 1 26.80 28.19 1.33 o -6 -6 1 156.06 151.48 2.58 o -5 -6 1 9.79 11.06 1.17 o -4 -6 1 23.80 23.39 1.26 o -3 -6 1 274.68 273.71 4.98 o -2 -6 1 251.93 251.88 2.94 o -1 -6 1 418.23 427.29 7.69 o 0 -6 1 955.77 929.90 22.31 o 1 -6 1 5.44 7.74 1.49 o 2 -6 1 360.81 351.56 5.75 o 3 -6 1 136.24 138.00 1.29 o 4 -6 1 107.09 102.10 2.18 o 5 -6 1 209.49 204.99 1.88 o 6 -6 1 9.89 9.21 1.01 o 7 -6 1 255.85 253.36 4.18 o 8 -6 1 25.61 27.54 1.28 o -8 -5 1 3.79 2.73 1.05 o -7 -5 1 329.10 323.36 5.07 o -6 -5 1 14.81 13.91 1.17 o -5 -5 1 1087.81 1073.61 7.60 o -4 -5 1 174.05 172.83 2.03 o -3 -5 1 551.72 561.07 5.08 o -2 -5 1 277.48 278.17 3.78 o -1 -5 1 0.10 1.27 1.08 o 0 -5 1 177.93 191.83 3.78 o 1 -5 1 10.44 4.63 1.12 o 2 -5 1 110.59 126.37 2.02 o 3 -5 1 0.08 0.25 1.10 o 4 -5 1 43.82 51.19 1.02 o 5 -5 1 43.90 39.60 1.11 o 6 -5 1 2.99 4.04 1.06 o 7 -5 1 90.35 87.39 1.92 o 8 -5 1 3.07 4.46 1.00 o -8 -4 1 12.55 12.07 1.23 o -7 -4 1 272.03 272.38 1.83 o -6 -4 1 1.59 0.64 1.20 o -5 -4 1 40.42 38.75 1.35 o -4 -4 1 5.66 7.48 1.21 o -3 -4 1 5.01 5.96 1.12 o -2 -4 1 228.33 222.04 2.35 o -1 -4 1 41.66 49.67 1.44 o 0 -4 1 567.94 573.89 12.03 o 1 -4 1 872.92 925.40 16.93 o 2 -4 1 0.21 2.76 1.03 o 3 -4 1 793.65 830.16 3.63 o 4 -4 1 32.97 29.12 1.00 o 5 -4 1 58.33 64.43 1.07 o 6 -4 1 160.06 160.25 1.32 o 7 -4 1 51.12 50.21 1.50 o 8 -4 1 409.21 408.21 3.70 o 9 -4 1 102.06 92.61 6.01 o -9 -3 1 33.43 32.02 3.32 o -8 -3 1 30.80 28.34 1.06 o -7 -3 1 26.50 25.86 1.09 o -6 -3 1 5.43 5.26 0.87 o -5 -3 1 22.07 22.11 1.22 o -4 -3 1 17.18 18.41 1.58 o -3 -3 1 9.40 7.28 1.25 o -2 -3 1 75.09 76.06 1.42 o -1 -3 1 371.34 344.74 5.40 o 0 -3 1 1563.80 1579.59 33.68 o 1 -3 1 288.46 276.64 5.31 o 2 -3 1 889.19 882.97 14.22 o 3 -3 1 165.25 153.52 1.33 o 4 -3 1 4.41 4.38 1.00 o 5 -3 1 372.15 348.58 3.59 o 6 -3 1 106.36 104.64 1.34 o 7 -3 1 228.14 222.93 3.21 o 8 -3 1 53.64 57.49 1.47 o 9 -3 1 14.63 12.43 1.49 o -9 -2 1 40.48 43.91 2.01 o -8 -2 1 49.53 49.35 1.53 o -7 -2 1 340.77 338.76 4.64 o -6 -2 1 9.84 10.66 1.07 o -5 -2 1 519.53 503.32 5.30 o -4 -2 1 1035.16 1009.40 7.48 o -3 -2 1 55.78 52.96 1.38 o -2 -2 1 2049.43 2003.47 15.34 o -1 -2 1 2157.06 2054.09 31.10 o 0 -2 1 100.67 111.61 2.05 o 1 -2 1 2725.33 2631.58 40.07 o 2 -2 1 13.08 11.56 1.48 o 3 -2 1 678.03 638.74 3.52 o 4 -2 1 15.94 19.86 1.05 o 5 -2 1 56.08 52.01 1.10 o 6 -2 1 5.13 6.53 0.84 o 7 -2 1 12.27 14.81 1.28 o 8 -2 1 21.36 23.17 1.37 o 9 -2 1 138.69 134.92 11.26 o -9 -1 1 83.12 89.69 1.81 o -8 -1 1 68.55 67.71 1.35 o -7 -1 1 256.10 263.90 3.33 o -6 -1 1 418.08 424.91 8.41 o -5 -1 1 107.48 112.94 1.25 o -4 -1 1 563.27 587.37 7.39 o -3 -1 1 0.17 5.12 1.16 o -2 -1 1 728.82 760.47 8.16 o -1 -1 1 279.48 267.57 2.92 o 0 -1 1 517.74 517.85 5.92 o 1 -1 1 1797.33 1761.31 28.64 o 2 -1 1 44.78 44.27 1.43 o 3 -1 1 729.80 805.09 6.78 o 4 -1 1 459.18 475.22 3.82 o 5 -1 1 216.02 229.99 1.62 o 6 -1 1 107.70 118.10 1.57 o 7 -1 1 31.59 32.93 1.30 o 8 -1 1 16.61 15.25 1.04 o 9 -1 1 0.08 -0.78 1.58 o -9 0 1 42.16 46.33 1.59 o -8 0 1 81.24 77.26 1.74 o -7 0 1 4.85 6.35 1.15 o -6 0 1 352.55 371.58 4.11 o -5 0 1 50.67 47.13 1.15 o -4 0 1 2546.21 2757.22 48.72 o -3 0 1 16.12 15.43 1.22 o -1 0 1 118.25 132.71 2.28 o 1 0 1 504.93 492.11 4.60 o 2 0 1 1577.22 1564.70 13.58 o 3 0 1 8.67 15.59 1.16 o 4 0 1 62.10 75.53 1.28 o 5 0 1 0.06 1.75 0.91 o 6 0 1 143.54 131.87 1.41 o 7 0 1 0.60 2.90 0.94 o 8 0 1 21.29 21.68 1.04 o 9 0 1 7.11 7.80 1.46 o -9 1 1 128.20 137.40 2.48 o -8 1 1 41.29 37.83 1.77 o -7 1 1 502.40 521.94 5.86 o -6 1 1 13.54 15.04 1.12 o -5 1 1 582.48 603.43 10.61 o -4 1 1 147.71 139.63 2.88 o -3 1 1 596.48 663.54 8.00 o -2 1 1 1462.51 1502.94 14.95 o -1 1 1 1877.09 1814.37 33.85 o 0 1 1 105.66 113.99 2.42 o 1 1 1 2280.51 2153.92 20.10 o 2 1 1 2429.20 2556.35 23.60 o 3 1 1 46.61 68.76 1.31 o 4 1 1 1910.11 1990.49 12.67 o 5 1 1 8.92 8.44 1.02 o 6 1 1 455.92 480.35 3.92 o 7 1 1 0.77 1.39 0.98 o 8 1 1 24.39 28.10 1.16 o 9 1 1 23.50 22.97 1.21 o -9 2 1 31.18 32.76 3.68 o -8 2 1 9.32 11.09 1.39 o -7 2 1 0.41 2.41 3.75 o -6 2 1 249.95 245.64 3.62 o -5 2 1 214.32 213.78 1.60 o -4 2 1 191.96 179.37 2.40 o -3 2 1 867.16 836.79 9.08 o -2 2 1 1102.56 1114.16 13.33 o -1 2 1 146.51 145.63 2.96 o 0 2 1 7438.08 6968.38 552.42 o 1 2 1 599.18 554.78 7.35 o 2 2 1 2021.90 1978.58 17.44 o 3 2 1 255.09 254.20 4.16 o 4 2 1 79.55 88.42 1.27 o 5 2 1 55.27 50.86 1.07 o 6 2 1 0.01 -0.26 1.06 o 7 2 1 11.06 11.33 1.06 o 8 2 1 37.92 44.34 1.16 o 9 2 1 1.47 1.97 1.25 o -9 3 1 3.80 4.95 1.89 o -8 3 1 37.54 43.11 3.10 o -7 3 1 19.70 18.72 1.28 o -6 3 1 7.40 8.06 1.22 o -5 3 1 146.34 142.02 3.26 o -4 3 1 284.80 280.32 3.26 o -3 3 1 278.44 289.88 3.53 o -2 3 1 431.52 455.55 6.06 o -1 3 1 154.36 170.19 5.20 o 0 3 1 1690.74 1696.05 43.29 o 1 3 1 18.08 20.50 1.40 o 2 3 1 1485.52 1507.55 25.72 o 3 3 1 261.22 250.21 2.73 o 4 3 1 87.00 106.66 8.99 o 5 3 1 48.45 49.44 1.52 o 6 3 1 172.73 170.41 3.51 o 7 3 1 31.14 28.24 1.00 o 8 3 1 95.72 98.42 2.43 o 9 3 1 51.17 52.35 1.91 o -8 4 1 16.98 19.32 1.77 o -7 4 1 79.22 79.20 1.44 o -6 4 1 2.20 2.59 1.15 o -5 4 1 20.36 18.57 1.02 o -4 4 1 3.81 4.62 0.95 o -3 4 1 3.51 1.80 0.87 o -2 4 1 232.34 240.56 5.99 o -1 4 1 40.81 38.04 1.69 o 0 4 1 1076.78 1089.16 28.78 o 1 4 1 21.33 11.10 1.18 o 2 4 1 348.45 353.09 5.03 o 3 4 1 2.42 5.05 1.21 o 4 4 1 1838.82 1814.79 15.94 o 5 4 1 102.30 101.33 1.94 o 6 4 1 826.54 805.87 12.52 o 7 4 1 142.04 143.34 2.41 o 8 4 1 40.39 40.77 1.53 o 9 4 1 112.84 115.63 1.26 o -8 5 1 0.05 -0.38 1.21 o -7 5 1 6.79 6.77 1.30 o -6 5 1 26.74 30.52 0.96 o -5 5 1 119.65 116.59 1.80 o -4 5 1 95.34 91.23 1.22 o -3 5 1 267.11 226.80 4.58 o -2 5 1 47.22 50.61 2.63 o -1 5 1 185.54 259.88 5.83 o 0 5 1 1921.29 1960.43 57.76 o 1 5 1 1616.20 1720.54 33.48 o 2 5 1 1451.54 1499.88 28.82 o 3 5 1 765.62 767.60 6.47 o 4 5 1 82.32 89.34 1.78 o 5 5 1 178.60 178.79 2.72 o 6 5 1 2.77 3.81 1.04 o 7 5 1 100.02 102.11 2.71 o 8 5 1 0.26 0.98 1.05 o -8 6 1 18.34 19.25 1.38 o -7 6 1 133.96 136.09 1.44 o -6 6 1 0.04 1.62 0.95 o -5 6 1 146.64 147.47 2.62 o -4 6 1 293.56 310.86 4.14 o -3 6 1 9.82 13.02 1.17 o -2 6 1 759.18 782.31 17.78 o -1 6 1 319.41 323.62 9.21 o 0 6 1 58.83 59.57 1.85 o 1 6 1 57.68 53.59 2.26 o 2 6 1 238.05 256.68 3.64 o 3 6 1 44.09 44.25 1.87 o 4 6 1 251.63 257.36 2.77 o 5 6 1 2.43 4.02 0.84 o 6 6 1 67.56 64.64 1.88 o 7 6 1 52.75 49.96 1.23 o 8 6 1 1.87 2.13 1.17 o -8 7 1 9.76 12.81 1.32 o -7 7 1 50.63 49.26 1.16 o -6 7 1 19.04 18.78 1.13 o -5 7 1 11.26 12.30 0.88 o -4 7 1 0.53 1.10 0.99 o -3 7 1 110.11 111.16 2.34 o -2 7 1 7.27 5.25 1.14 o -1 7 1 407.12 419.66 5.90 o 0 7 1 0.48 1.50 1.01 o 1 7 1 578.01 588.96 10.29 o 2 7 1 21.48 22.34 0.99 o 3 7 1 43.70 51.46 2.31 o 4 7 1 81.05 75.11 2.54 o 5 7 1 248.13 243.93 1.60 o 6 7 1 1.69 1.86 0.96 o 7 7 1 319.55 327.32 8.62 o 8 7 1 69.50 69.54 3.36 o -7 8 1 67.64 68.12 1.18 o -6 8 1 45.06 48.32 1.06 o -5 8 1 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0.31 -1.51 1.66 o 1 0 11 295.39 274.20 2.25 o 2 0 11 92.89 95.65 1.93 o 3 0 11 29.58 24.84 1.44 o 4 0 11 126.62 121.86 1.91 o 5 0 11 93.32 97.21 1.78 o 6 0 11 46.47 50.24 1.34 o -4 1 11 121.12 119.49 2.15 o -3 1 11 16.80 15.97 1.71 o -2 1 11 390.60 384.47 3.21 o -1 1 11 56.47 53.79 1.80 o 0 1 11 510.04 489.78 3.95 o 1 1 11 4.41 2.52 2.28 o 2 1 11 284.68 264.54 2.31 o 3 1 11 112.88 117.89 1.90 o 4 1 11 39.15 35.70 1.26 o 5 1 11 121.58 126.20 1.41 o 6 1 11 60.51 64.68 1.31 o -4 2 11 223.49 212.86 2.37 o -3 2 11 24.07 23.96 1.60 o -2 2 11 179.26 178.92 1.87 o -1 2 11 115.03 113.04 1.67 o 0 2 11 53.62 53.67 1.35 o 1 2 11 107.87 105.20 1.46 o 2 2 11 16.49 19.15 1.33 o 3 2 11 82.41 85.00 1.70 o 4 2 11 2.89 3.86 1.27 o 5 2 11 25.06 24.64 1.15 o 6 2 11 55.73 56.99 1.44 o -4 3 11 238.96 225.76 3.91 o -3 3 11 16.04 18.83 1.39 o -2 3 11 75.62 75.37 1.55 o -1 3 11 122.25 121.14 1.50 o 0 3 11 5.66 5.76 1.25 o 1 3 11 196.68 187.09 3.14 o 2 3 11 68.14 69.69 1.24 o 3 3 11 7.59 6.30 1.25 o 4 3 11 19.10 19.06 1.30 o 5 3 11 173.13 174.28 1.90 o 6 3 11 5.42 5.26 1.20 o -4 4 11 135.53 120.65 4.69 o -3 4 11 143.29 138.36 3.05 o -2 4 11 0.30 1.08 1.30 o -1 4 11 107.67 110.02 2.13 o 0 4 11 107.59 116.86 1.57 o 1 4 11 94.92 94.28 1.40 o 2 4 11 89.21 92.05 1.95 o 3 4 11 746.93 744.49 15.21 o 4 4 11 31.95 35.76 1.37 o 5 4 11 537.54 560.79 3.72 o 6 4 11 23.15 25.01 1.42 o -3 5 11 28.03 26.80 1.55 o -2 5 11 52.59 53.60 1.46 o -1 5 11 47.03 44.90 1.35 o 0 5 11 1.33 2.52 1.25 o 1 5 11 186.18 184.02 2.57 o 2 5 11 0.23 1.06 1.36 o 3 5 11 85.85 94.81 2.52 o 4 5 11 1.04 1.94 1.71 o 5 5 11 0.24 0.99 1.25 o 6 5 11 45.76 47.75 1.34 o -3 6 11 55.78 56.57 1.70 o -2 6 11 19.46 19.40 1.33 o -1 6 11 0.57 -0.27 1.23 o 0 6 11 60.71 59.17 1.70 o 1 6 11 33.48 33.16 1.19 o 2 6 11 88.26 79.88 3.77 o 3 6 11 67.16 69.99 1.40 o 4 6 11 103.22 102.99 2.34 o 5 6 11 71.73 71.46 1.42 o -2 7 11 81.12 76.82 1.37 o -1 7 11 1.61 1.09 1.05 o 0 7 11 170.35 169.77 3.12 o 1 7 11 67.86 66.89 1.27 o 2 7 11 25.28 24.04 1.22 o 3 7 11 204.80 201.14 4.51 o 4 7 11 45.83 49.28 1.57 o 5 7 11 53.09 50.01 1.33 o -1 8 11 50.94 48.29 1.30 o 0 8 11 43.28 47.92 1.30 o 1 8 11 175.80 171.12 3.51 o 2 8 11 202.02 201.61 3.00 o 3 8 11 47.99 44.97 1.82 o 4 8 11 103.84 102.54 3.99 o 0 9 11 36.16 34.07 1.21 o 1 9 11 28.42 31.22 1.59 o 2 9 11 0.82 0.31 1.14 o 1 -5 12 22.05 23.12 1.78 o 2 -5 12 1.92 1.16 2.23 o -1 -4 12 4.31 6.81 1.62 o 0 -4 12 1.10 3.56 1.63 o 1 -4 12 272.17 292.22 2.95 o 2 -4 12 21.08 31.42 2.70 o 3 -4 12 901.48 1001.87 12.52 o 4 -4 12 39.09 41.51 1.48 o -1 -3 12 10.12 9.75 1.60 o 0 -3 12 15.74 17.23 1.63 o 1 -3 12 189.62 185.54 3.55 o 2 -3 12 17.70 18.40 4.39 o 3 -3 12 120.37 123.57 2.15 o 4 -3 12 0.30 0.27 1.51 o -2 -2 12 14.74 13.95 1.60 o -1 -2 12 17.74 16.44 1.60 o 0 -2 12 13.19 11.97 1.65 o 1 -2 12 6.75 6.54 1.50 o 2 -2 12 50.52 50.09 3.06 o 3 -2 12 23.88 33.04 2.82 o 4 -2 12 63.65 67.67 1.96 o 5 -2 12 14.06 13.80 1.22 o -2 -1 12 68.11 71.43 2.06 o -1 -1 12 31.81 30.98 1.88 o 0 -1 12 59.35 65.19 2.70 o 1 -1 12 58.85 61.81 3.31 o 2 -1 12 0.05 3.56 1.39 o 3 -1 12 57.26 59.65 1.63 o 4 -1 12 14.36 12.83 1.93 o 5 -1 12 29.57 28.51 1.65 o -3 0 12 65.93 65.48 3.17 o -2 0 12 46.25 42.62 2.85 o -1 0 12 39.58 38.07 1.89 o 0 0 12 0.01 1.56 1.73 o 1 0 12 48.90 57.71 1.41 o 2 0 12 32.53 33.83 1.50 o 3 0 12 139.38 148.17 1.89 o 4 0 12 44.04 42.90 1.59 o 5 0 12 6.90 7.57 1.21 o -3 1 12 13.45 12.59 2.23 o -2 1 12 39.92 46.16 2.01 o -1 1 12 87.33 85.11 4.55 o 0 1 12 126.08 136.86 1.69 o 1 1 12 27.41 29.63 1.53 o 2 1 12 135.26 138.76 1.79 o 3 1 12 33.83 32.62 1.55 o 4 1 12 103.53 111.75 1.63 o 5 1 12 88.34 88.54 3.20 o -3 2 12 261.22 259.89 3.12 o -2 2 12 105.94 108.72 1.96 o -1 2 12 22.72 24.11 1.83 o 0 2 12 4.52 3.87 2.31 o 1 2 12 26.45 27.13 1.41 o 2 2 12 43.31 42.20 1.51 o 3 2 12 40.21 41.96 1.69 o 4 2 12 71.92 66.98 1.35 o 5 2 12 45.63 52.77 2.01 o -3 3 12 0.26 0.81 1.88 o -2 3 12 23.48 23.02 1.54 o -1 3 12 4.59 6.04 1.44 o 0 3 12 15.92 15.18 1.43 o 1 3 12 17.82 19.95 1.49 o 2 3 12 111.79 108.83 2.14 o 3 3 12 21.87 23.30 1.46 o 4 3 12 103.44 104.84 1.82 o 5 3 12 0.49 0.86 1.19 o -2 4 12 89.32 85.53 1.60 o -1 4 12 1.89 2.19 1.41 o 0 4 12 119.13 112.67 1.66 o 1 4 12 27.65 30.53 1.39 o 2 4 12 37.54 34.85 1.52 o 3 4 12 10.11 8.87 1.32 o 4 4 12 6.26 11.65 1.39 o 5 4 12 65.37 53.41 1.44 o -2 5 12 268.28 260.53 2.45 o -1 5 12 19.43 16.75 1.35 o 0 5 12 57.99 60.96 1.52 o 1 5 12 2.40 3.53 1.18 o 2 5 12 0.03 0.79 1.33 o 3 5 12 31.67 36.64 1.57 o 4 5 12 0.98 3.99 1.12 o 5 5 12 178.79 190.04 1.68 o -1 6 12 130.58 124.70 4.38 o 0 6 12 117.44 117.14 1.70 o 1 6 12 2.20 2.29 1.26 o 2 6 12 84.87 86.03 1.48 o 3 6 12 101.44 103.63 3.61 o 4 6 12 37.58 36.67 1.30 o 0 7 12 17.47 17.48 1.44 o 1 7 12 4.87 7.34 1.22 o 2 7 12 14.51 13.11 1.34 o 3 7 12 85.95 89.12 1.41 o 0 -2 13 20.15 21.12 2.13 o 1 -2 13 10.84 9.50 1.57 o 2 -2 13 5.27 5.89 1.55 o 3 -2 13 273.64 282.34 6.30 o 0 -1 13 80.78 85.48 2.20 o 1 -1 13 52.99 54.14 1.68 o 2 -1 13 0.04 3.49 1.83 o 3 -1 13 84.88 89.48 2.13 o -1 0 13 8.33 4.73 1.62 o 0 0 13 14.01 13.33 2.00 o 1 0 13 0.13 -1.30 1.82 o 2 0 13 67.64 70.64 2.10 o 3 0 13 0.61 3.53 1.89 o 4 0 13 58.72 59.73 3.61 o -1 1 13 0.02 -0.32 1.91 o 0 1 13 85.35 87.12 2.13 o 1 1 13 0.06 1.75 1.82 o 2 1 13 4.73 5.29 1.86 o 3 1 13 35.28 33.14 1.63 o 4 1 13 164.50 178.40 2.12 o -1 2 13 3.16 5.78 1.88 o 0 2 13 75.98 80.94 2.11 o 1 2 13 10.27 11.52 2.64 o 2 2 13 1.58 0.93 1.96 o 3 2 13 0.23 0.90 1.31 o 4 2 13 46.69 46.24 3.37 o -1 3 13 8.49 8.77 1.74 o 0 3 13 18.56 20.93 1.45 o 1 3 13 10.28 9.79 1.58 o 2 3 13 60.67 60.64 1.67 o 3 3 13 65.38 61.63 1.89 o 4 3 13 40.20 40.66 1.83 o 0 4 13 236.34 235.00 2.07 o 1 4 13 133.05 139.20 2.33 o 2 4 13 102.58 107.33 1.70 o 3 4 13 63.92 72.62 2.81 o 0 5 13 6.40 7.17 1.61 o 1 5 13 38.29 41.81 1.39 o 2 5 13 106.51 108.04 1.75 o 3 5 13 56.40 61.22 2.19 o 0 0 00 END