Acta Cryst. (2005). E61, m3-m5  [ doi:10.1107/S1600536804030983 ]

(2,2'-Bipyridine-²N,N')(3-oxidonaphthalene-2-carboxylato-²O:O')palladium(II) hemihydrate

Y. Wang and N. Okabe

Online 4 December 2004

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.006 Å
• R factor = 0.031
• wR factor = 0.044
• Data-to-parameter ratio = 15.9

checkCIF/PLATON results

No syntax errors found




Alert level C
GOODF01_ALERT_2_C  The least squares goodness of fit parameter lies
            outside the range 0.80 <> 2.00
            Goodness of fit given =      0.658
PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low ....         43 Perc. 
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio 
PLAT230_ALERT_2_C Hirshfeld Test Diff for    N12    -   C126    ..       5.16 su    
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Pd2    -   O21     ..       5.82 su    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   7 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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