# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 041008d in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 220.41 _exptl_crystal_F_000 930.00 _reflns_d_resolution_high 0.8400 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.7497 _cell_length_b 13.5118 _cell_length_c 14.0681 _cell_angle_alpha 65.430 _cell_angle_beta 86.264 _cell_angle_gamma 81.663 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 35721.12 32510.83 1157.58 o 2 0 0 5114.36 4846.92 252.09 o 3 0 0 17173.37 15493.82 313.33 o 4 0 0 10319.64 9178.48 193.33 o 5 0 0 12296.64 12586.01 263.36 o 6 0 0 18.77 11.86 16.14 o 7 0 0 56.20 -6.93 21.14 o 8 0 0 8.06 -45.60 45.60 o 9 0 0 354.44 342.26 80.98 o 10 0 0 523.89 500.12 103.28 o 11 0 0 287.29 172.52 96.39 o 12 0 0 451.59 600.37 123.54 o 13 0 0 526.08 603.11 138.75 o -13 1 0 117.82 143.31 105.59 o -12 1 0 4.60 -19.03 85.53 o -11 1 0 62.60 -42.62 76.04 o -10 1 0 111.81 41.40 77.60 o -9 1 0 1021.19 966.77 116.79 o -8 1 0 757.81 882.77 108.08 o -7 1 0 4287.95 3854.42 449.77 o -6 1 0 3392.02 2676.54 96.72 o -5 1 0 5938.82 5524.06 243.92 o -4 1 0 9880.26 10024.09 606.41 o -3 1 0 4849.31 4392.08 157.20 o -2 1 0 48580.09 47218.08 1761.91 o -1 1 0 3374.42 4073.35 155.05 o 1 1 0 319.64 393.83 21.92 o 2 1 0 102.04 94.98 12.94 o 3 1 0 6668.16 6165.20 160.31 o 4 1 0 65.68 54.61 22.14 o 5 1 0 15.80 110.04 25.05 o 6 1 0 249.90 211.54 34.00 o 7 1 0 2912.30 2861.40 179.24 o 8 1 0 683.52 654.21 67.66 o 9 1 0 1438.19 1330.31 74.00 o 10 1 0 494.00 515.97 104.36 o 11 1 0 90.90 52.45 80.24 o 12 1 0 486.19 660.74 124.71 o 13 1 0 268.69 271.31 111.80 o -13 2 0 326.02 255.50 120.27 o -12 2 0 441.99 557.80 123.10 o -11 2 0 1581.80 1810.59 153.28 o -10 2 0 2276.00 2472.36 173.20 o -9 2 0 3827.39 3730.58 212.83 o -8 2 0 3364.77 3143.94 323.42 o -7 2 0 378.52 286.99 101.89 o -6 2 0 38.00 -23.25 23.25 o -5 2 0 2092.47 1828.65 141.20 o -4 2 0 5515.15 5378.89 235.45 o -3 2 0 85.05 68.49 19.27 o -2 2 0 0.09 -8.33 13.63 o -1 2 0 228.01 232.18 19.23 o 0 2 0 1587.31 1803.06 80.24 o 1 2 0 6235.01 7310.79 190.80 o 2 2 0 3737.75 4023.93 87.68 o 3 2 0 6113.21 5877.52 154.21 o 4 2 0 1908.87 1933.12 123.54 o 5 2 0 9864.76 10340.03 475.70 o 6 2 0 768.48 608.20 58.47 o 7 2 0 4469.07 4449.51 141.48 o 8 2 0 1807.36 1711.65 79.88 o 9 2 0 19.44 53.39 43.22 o 10 2 0 437.53 544.06 67.50 o 11 2 0 1062.09 1070.35 84.14 o 12 2 0 104.44 -15.12 88.71 o 13 2 0 58.42 -49.37 100.79 o -13 3 0 519.76 577.27 136.60 o -12 3 0 258.11 340.11 111.60 o -11 3 0 423.81 366.62 104.22 o -10 3 0 1237.08 1047.64 114.78 o -9 3 0 197.05 167.63 80.44 o -8 3 0 202.21 60.20 42.79 o -7 3 0 63.67 5.89 33.27 o -6 3 0 20.96 -39.93 44.69 o -5 3 0 148.02 52.99 29.18 o -4 3 0 2758.23 2828.32 99.44 o -3 3 0 210.06 194.55 36.06 o -2 3 0 1576.31 1684.10 76.81 o -1 3 0 18413.76 22497.06 575.14 o 0 3 0 13728.50 16534.63 424.69 o 1 3 0 249.15 239.37 36.53 o 2 3 0 6269.34 7473.36 198.85 o 3 3 0 7660.72 8202.51 172.79 o 4 3 0 8846.69 9639.34 248.24 o 5 3 0 5149.61 5598.91 158.88 o 6 3 0 1363.57 1306.51 103.31 o 7 3 0 1390.06 1353.48 67.97 o 8 3 0 83.92 64.40 38.29 o 9 3 0 224.70 232.51 49.89 o 10 3 0 400.99 383.94 81.74 o 11 3 0 405.56 382.15 68.80 o 12 3 0 1175.73 1207.17 89.06 o 13 3 0 528.48 683.99 86.95 o -12 4 0 29.38 -94.92 94.92 o -11 4 0 27.91 -82.93 82.93 o -10 4 0 37.39 -53.08 74.95 o -9 4 0 791.43 848.61 123.98 o -8 4 0 950.24 876.26 71.00 o -7 4 0 1278.46 1233.45 137.75 o -6 4 0 2744.70 2696.20 109.23 o -5 4 0 4641.51 4786.28 271.88 o -4 4 0 4330.53 4292.15 151.47 o -3 4 0 4397.74 4566.91 310.60 o -2 4 0 6052.08 7019.09 318.26 o -1 4 0 3159.78 3373.88 103.71 o 0 4 0 13850.13 16032.46 415.63 o 1 4 0 9.74 0.33 11.02 o 2 4 0 4908.96 5905.36 162.78 o 3 4 0 4446.70 4995.08 113.07 o 4 4 0 1200.08 1271.58 51.64 o 5 4 0 1336.21 1281.75 77.45 o 6 4 0 489.47 462.10 44.65 o 7 4 0 317.39 285.11 81.83 o 8 4 0 1922.01 1788.58 84.01 o 9 4 0 2063.92 2094.93 122.78 o 10 4 0 1052.35 1091.54 77.43 o 11 4 0 557.91 755.10 79.05 o 12 4 0 251.60 225.57 67.46 o 13 4 0 347.95 504.54 82.97 o -12 5 0 326.07 474.75 128.78 o -11 5 0 791.82 878.70 143.60 o -10 5 0 1044.61 1115.65 128.87 o -9 5 0 1880.07 1929.33 152.35 o -8 5 0 2013.18 2039.24 111.26 o -7 5 0 1190.85 1083.37 75.64 o -6 5 0 2409.15 2411.06 106.07 o -5 5 0 3421.51 3459.34 127.99 o -4 5 0 2379.34 2583.51 100.85 o -3 5 0 1620.41 1837.45 76.79 o -2 5 0 2.78 -14.68 18.25 o -1 5 0 2690.62 3248.41 104.63 o 0 5 0 3556.66 4053.38 121.56 o 1 5 0 839.55 827.04 64.78 o 2 5 0 1814.28 1968.93 119.72 o 3 5 0 3056.70 3153.50 98.81 o 4 5 0 10838.33 11956.01 253.28 o 5 5 0 6501.52 7040.12 159.19 o 6 5 0 2758.05 2890.66 169.80 o 7 5 0 5824.65 6048.51 182.59 o 8 5 0 1401.83 1295.70 72.85 o 9 5 0 1270.40 1208.85 111.80 o 10 5 0 818.69 854.18 82.58 o 11 5 0 614.73 613.06 79.96 o 12 5 0 85.73 -38.07 61.67 o 13 5 0 15.45 -68.53 68.53 o -11 6 0 704.54 764.41 139.24 o -10 6 0 780.01 893.87 138.41 o -9 6 0 1284.77 1075.37 130.04 o -8 6 0 951.13 1160.38 97.73 o -7 6 0 38.61 -44.25 44.25 o -6 6 0 0.36 11.08 38.81 o -5 6 0 28.34 -25.62 33.94 o -4 6 0 896.64 807.71 58.02 o -3 6 0 1087.80 1065.33 61.10 o -2 6 0 4665.30 5521.36 169.05 o -1 6 0 3684.91 4123.50 130.66 o 0 6 0 3851.45 4088.55 126.12 o 1 6 0 763.06 774.88 32.45 o 2 6 0 3997.35 4042.28 123.75 o 3 6 0 13696.42 15987.15 421.66 o 4 6 0 8138.81 8903.57 196.76 o 5 6 0 9112.53 9885.56 217.36 o 6 6 0 1361.71 1296.21 65.94 o 7 6 0 1317.57 1315.02 70.34 o 8 6 0 278.40 225.21 47.53 o 9 6 0 21.73 -85.88 101.84 o 10 6 0 0.14 -15.57 49.35 o 11 6 0 95.46 50.18 62.12 o 12 6 0 261.57 227.03 75.27 o 13 6 0 258.71 139.58 77.96 o -11 7 0 27.84 -3.38 104.41 o -10 7 0 9.81 0.05 96.93 o -9 7 0 177.77 69.40 65.28 o -8 7 0 56.40 7.19 55.40 o -7 7 0 136.76 54.34 71.93 o -6 7 0 1497.81 1478.61 97.78 o -5 7 0 2509.86 2590.14 115.60 o -4 7 0 5251.34 5495.03 182.96 o -3 7 0 2336.23 2394.71 99.34 o -2 7 0 6549.74 7255.32 216.92 o -1 7 0 7286.96 7855.22 227.66 o 0 7 0 2730.16 2928.22 102.29 o 1 7 0 6728.59 7628.24 218.17 o 2 7 0 3603.41 3935.04 124.24 o 3 7 0 1373.89 1458.98 138.21 o 4 7 0 189.50 151.26 68.60 o 5 7 0 25.30 -13.90 21.50 o 6 7 0 58.76 -21.68 31.42 o 7 7 0 256.79 212.20 45.34 o 8 7 0 668.84 717.35 63.39 o 9 7 0 1298.14 1081.14 77.66 o 10 7 0 1965.82 2063.78 117.01 o 11 7 0 1886.79 2053.82 111.22 o 12 7 0 976.44 1135.72 104.57 o 13 7 0 556.54 648.18 97.31 o -10 8 0 202.24 108.52 113.57 o -9 8 0 470.42 592.10 176.71 o -8 8 0 458.24 511.21 86.90 o -7 8 0 1012.59 1116.72 101.49 o -6 8 0 8296.53 9439.69 300.45 o -5 8 0 4824.30 5258.59 187.74 o -4 8 0 2144.27 2155.27 102.54 o -3 8 0 1249.34 1430.75 78.33 o -2 8 0 532.13 649.57 86.75 o -1 8 0 1363.46 1359.21 67.96 o 0 8 0 2.95 -19.17 25.19 o 1 8 0 30.53 13.91 23.62 o 2 8 0 4.68 -4.98 24.28 o 3 8 0 1303.66 1229.93 59.53 o 4 8 0 3792.33 3837.23 126.92 o 5 8 0 1616.24 1649.21 62.18 o 6 8 0 1272.90 1171.85 66.46 o 7 8 0 2822.07 2790.87 109.64 o 8 8 0 3065.52 3084.51 157.05 o 9 8 0 1271.87 1397.05 204.36 o 10 8 0 1109.99 995.88 94.43 o 11 8 0 1157.47 1412.09 103.93 o 12 8 0 155.31 216.27 102.85 o -9 9 0 332.34 190.58 119.54 o -8 9 0 562.11 429.65 130.49 o -7 9 0 62.12 112.34 98.00 o -6 9 0 146.22 90.91 83.03 o -5 9 0 18.08 16.34 72.90 o -4 9 0 839.66 770.53 109.89 o -3 9 0 44.03 96.83 65.08 o -2 9 0 1234.02 1180.62 112.09 o -1 9 0 746.94 696.06 97.12 o 0 9 0 1646.71 1535.14 119.23 o 1 9 0 6475.99 6444.92 295.90 o 2 9 0 7457.19 7732.16 337.49 o 3 9 0 3003.14 2958.29 165.27 o 4 9 0 1278.59 1276.76 104.90 o 5 9 0 612.02 635.63 62.11 o 6 9 0 1845.21 1657.70 123.15 o 7 9 0 1241.61 1143.78 108.61 o 8 9 0 15.21 -61.11 61.11 o 9 9 0 67.11 47.17 74.96 o 10 9 0 9.65 -76.67 76.67 o 11 9 0 13.65 -88.80 88.80 o 12 9 0 28.38 -101.96 101.96 o -8 10 0 9.23 -59.30 108.13 o -7 10 0 128.03 502.76 127.60 o -6 10 0 833.79 966.97 146.73 o -5 10 0 321.63 370.34 106.86 o -4 10 0 1228.43 1254.80 139.34 o -3 10 0 1986.09 2239.42 170.36 o -2 10 0 2102.56 2292.75 164.10 o -1 10 0 4264.06 4079.76 227.11 o 0 10 0 4951.24 4774.36 247.81 o 1 10 0 3888.94 3862.78 210.92 o 2 10 0 1898.13 1847.92 137.77 o 3 10 0 794.89 751.01 96.92 o 4 10 0 721.61 707.90 95.50 o 5 10 0 1199.22 1134.19 107.59 o 6 10 0 445.21 486.01 91.74 o 7 10 0 19.32 -22.26 59.25 o 8 10 0 426.43 404.49 91.45 o 9 10 0 389.66 365.45 98.20 o 10 10 0 541.83 538.43 110.38 o 11 10 0 524.73 518.66 122.80 o -7 11 0 890.23 1089.57 170.60 o -6 11 0 1124.09 1213.45 166.20 o -5 11 0 566.60 546.74 132.64 o -4 11 0 474.21 525.71 124.76 o -3 11 0 1548.88 1541.50 153.97 o -2 11 0 633.04 585.40 113.56 o -1 11 0 6.26 -56.02 67.42 o 0 11 0 1.43 -44.63 62.04 o 1 11 0 36.23 -3.03 60.87 o 2 11 0 0.90 57.54 60.53 o 3 11 0 1423.10 1299.17 116.79 o 4 11 0 1917.25 1700.46 131.61 o 5 11 0 865.47 1097.16 103.38 o 6 11 0 2305.78 2101.21 148.59 o 7 11 0 1813.09 1619.10 133.57 o 8 11 0 739.99 789.46 117.52 o 9 11 0 930.79 914.52 125.64 o 10 11 0 804.87 840.88 127.35 o -6 12 0 348.04 85.09 122.13 o -5 12 0 155.37 -4.89 104.02 o -4 12 0 28.71 -84.79 97.31 o -3 12 0 73.81 -71.97 83.56 o -2 12 0 500.41 420.99 109.50 o -1 12 0 1003.52 932.86 136.80 o 0 12 0 1803.25 1324.12 132.59 o 1 12 0 2232.37 1962.02 151.47 o 2 12 0 2663.97 2423.53 166.98 o 3 12 0 1557.44 1383.67 129.07 o 4 12 0 2369.69 2160.26 160.87 o 6 12 0 1038.45 1145.25 128.28 o 7 12 0 601.96 573.80 110.67 o 8 12 0 557.24 406.69 106.22 o 9 12 0 452.29 515.14 116.35 o -4 13 0 774.87 790.05 159.94 o -3 13 0 703.62 756.59 149.03 o -2 13 0 1712.82 1786.03 167.37 o -1 13 0 2614.69 2058.30 179.36 o 0 13 0 2583.51 2093.19 170.75 o 1 13 0 1968.31 1637.93 149.61 o 2 13 0 2047.57 1793.27 154.21 o 3 13 0 989.53 1164.43 140.81 o 4 13 0 1111.33 1205.33 132.05 o 6 13 0 127.71 27.35 92.33 o 7 13 0 38.37 14.04 95.36 o -2 14 0 917.32 814.95 156.02 o -1 14 0 952.41 1047.84 159.35 o 0 14 0 496.26 453.08 121.25 o 1 14 0 234.45 116.01 96.05 o 2 14 0 97.75 58.72 90.42 o 3 14 0 5.67 -60.33 80.34 o -3 -14 1 649.14 804.24 140.32 o -2 -14 1 111.73 129.37 94.72 o -1 -14 1 5.18 -13.50 87.24 o 0 -14 1 6.40 -93.15 93.15 o -7 -13 1 234.00 402.83 116.65 o -6 -13 1 118.48 55.98 100.11 o -5 -13 1 17.07 3.87 90.27 o -3 -13 1 369.29 267.74 96.98 o -2 -13 1 551.38 373.87 104.27 o -1 -13 1 1285.97 1355.58 159.06 o 0 -13 1 1424.09 1195.11 157.69 o 1 -13 1 2052.11 1513.61 156.32 o 2 -13 1 1919.89 1696.06 171.14 o 3 -13 1 1449.38 1320.60 176.77 o -8 -12 1 126.36 105.88 98.44 o -7 -12 1 425.05 250.81 105.24 o -6 -12 1 634.75 564.11 107.24 o -5 -12 1 1473.61 1254.45 129.75 o -4 -12 1 2691.74 2604.31 182.88 o -3 -12 1 1725.02 1638.32 143.94 o -2 -12 1 861.83 786.87 119.33 o -1 -12 1 477.91 542.73 108.91 o 0 -12 1 1724.43 1669.10 147.12 o 1 -12 1 1525.03 1298.88 137.24 o 2 -12 1 481.63 414.63 111.11 o 3 -12 1 8.49 -83.71 83.71 o 4 -12 1 60.94 -36.16 98.49 o 5 -12 1 19.54 -100.25 100.25 o -9 -11 1 1172.20 1179.45 144.62 o -8 -11 1 1226.97 1256.75 142.18 o -7 -11 1 1442.42 1363.75 130.53 o -6 -11 1 2217.63 1990.73 148.83 o -5 -11 1 1995.89 1983.25 143.01 o -4 -11 1 1869.14 1671.30 135.48 o -3 -11 1 673.20 763.97 106.66 o -2 -11 1 652.19 784.42 108.86 o -1 -11 1 402.53 508.83 95.65 o 0 -11 1 40.03 -32.10 63.27 o 1 -11 1 0.24 -64.92 64.92 o 2 -11 1 94.01 29.75 76.48 o 3 -11 1 467.58 489.19 114.50 o 4 -11 1 582.57 502.32 120.06 o 5 -11 1 497.68 566.27 137.92 o 6 -11 1 561.63 567.98 138.41 o 7 -11 1 709.28 762.85 160.87 o -10 -10 1 599.31 639.85 121.78 o -9 -10 1 1145.65 1173.33 138.36 o -8 -10 1 1503.81 1319.43 126.13 o -7 -10 1 431.28 533.83 97.80 o -6 -10 1 79.63 74.71 65.96 o -5 -10 1 109.75 44.82 67.42 o -4 -10 1 137.22 244.50 72.71 o -3 -10 1 31.28 -16.49 54.90 o -2 -10 1 1083.85 1044.17 105.83 o -1 -10 1 2141.56 2025.52 144.48 o 0 -10 1 2431.03 2063.05 149.61 o 1 -10 1 2849.13 2419.13 166.05 o 2 -10 1 1383.49 1204.21 123.64 o 3 -10 1 3031.70 2844.78 190.08 o 4 -10 1 1604.62 1523.69 145.99 o 5 -10 1 1126.88 1257.29 151.23 o 6 -10 1 1383.00 1406.56 165.71 o 7 -10 1 738.21 833.15 143.45 o 8 -10 1 567.84 490.77 136.75 o -11 -9 1 203.99 -4.79 106.03 o -10 -9 1 104.67 -12.87 91.40 o -9 -9 1 101.10 -80.58 80.58 o -8 -9 1 6.45 -59.88 67.03 o -7 -9 1 204.03 170.96 76.04 o -6 -9 1 223.10 247.53 72.71 o -5 -9 1 824.29 872.55 71.94 o -4 -9 1 2150.17 2114.13 137.87 o -3 -9 1 2379.34 2435.42 151.42 o -2 -9 1 2202.50 2121.76 139.78 o -1 -9 1 7256.49 6935.94 313.61 o 0 -9 1 6027.63 5578.50 269.58 o 1 -9 1 3875.59 3602.83 201.77 o 2 -9 1 1765.02 1838.14 142.91 o 3 -9 1 1162.20 1066.58 114.63 o 4 -9 1 2558.49 2436.10 172.46 o 5 -9 1 406.53 360.07 96.93 o 6 -9 1 163.19 111.16 86.11 o 7 -9 1 1.44 -45.11 88.56 o 8 -9 1 89.70 20.26 100.60 o 9 -9 1 49.16 -110.18 110.18 o -12 -8 1 165.54 37.43 100.35 o -11 -8 1 16.74 -48.20 91.01 o -10 -8 1 771.42 780.80 121.68 o -9 -8 1 375.09 409.53 92.23 o -8 -8 1 204.88 279.83 79.95 o -7 -8 1 1003.31 973.47 104.11 o -6 -8 1 3102.89 2878.44 156.61 o -5 -8 1 4288.60 4434.85 147.99 o -4 -8 1 1048.40 1142.12 95.70 o -3 -8 1 2137.42 2184.97 133.71 o -2 -8 1 2905.03 3069.50 165.66 o -1 -8 1 1833.81 2028.41 130.53 o 0 -8 1 306.11 388.69 68.94 o 1 -8 1 45.44 41.15 49.08 o 2 -8 1 7.06 12.82 50.64 o 3 -8 1 581.51 716.52 98.78 o 4 -8 1 40.89 -3.08 57.49 o 5 -8 1 1026.13 1134.19 135.28 o 6 -8 1 2863.06 2747.71 195.90 o 7 -8 1 374.95 246.94 103.29 o 8 -8 1 865.51 931.79 141.10 o 9 -8 1 496.86 544.74 129.36 o -12 -7 1 880.09 960.21 112.04 o -11 -7 1 615.32 652.01 87.74 o -10 -7 1 1793.23 1824.15 103.01 o -9 -7 1 2359.99 2394.74 111.02 o -8 -7 1 1781.64 1771.59 89.00 o -7 -7 1 1658.47 1580.74 105.88 o -6 -7 1 278.82 188.17 39.96 o -5 -7 1 2297.09 2264.77 71.90 o -4 -7 1 244.96 238.67 32.27 o -3 -7 1 12.40 17.22 22.08 o -2 -7 1 417.87 483.46 64.20 o -1 -7 1 6217.73 7044.52 201.72 o 0 -7 1 8468.43 9196.57 257.83 o 1 -7 1 5247.32 5593.93 170.79 o 2 -7 1 3570.96 3903.15 133.41 o 3 -7 1 2845.42 2963.28 113.70 o 4 -7 1 5041.23 5436.71 181.83 o 5 -7 1 2953.45 3020.45 127.20 o 6 -7 1 2796.08 2528.54 198.32 o 7 -7 1 1756.23 1869.92 105.97 o 8 -7 1 455.92 507.68 75.61 o 9 -7 1 373.35 378.49 93.55 o 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