Acta Cryst. (2005). E61, m226-m228  [ doi:10.1107/S1600536804032209 ]

{N-[Bis(2-pyridyl)methyl]-N,N-bis(2-pyridylmethyl)amine-⁵N}chlororuthenium(II) perchlorate methanol solvate

T. Kojima, D. M. Weber and C. T. Choma

Online 8 January 2005

Key indicators

• Single-crystal X-ray study
• T = 113 K
• Mean (C-C) = 0.006 Å
• R factor = 0.044
• wR factor = 0.119
• Data-to-parameter ratio = 17.2

checkCIF/PLATON results

No syntax errors found




Alert level B
ABSTM02_ALERT_3_B  The ratio of expected to reported Tmax/Tmin(RR') is < 0.75
            Tmin and Tmax reported:      0.444     0.841
            Tmin' and Tmax expected:      0.652     0.841
            RR' =      0.681
            Please check that your absorption correction is appropriate.
PLAT061_ALERT_3_B Tmax/Tmin Range Test RR' too Large .............       0.67       

Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT152_ALERT_1_C Supplied and Calc Volume s.u. Inconsistent .....          ?
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        Cl2     

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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