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Acta Cryst. (2005). E61, i18-i19 [ doi:10.1107/S1600536805001960 ]
Tetratellurium bis[heptachlorodigallate(III)], Te4[Ga2Cl7]2
Online 29 January 2005
Key indicators
- Single-crystal X-ray study
- T = 296 K
- Mean
(e-Te) = 0.001 Å
- R factor = 0.032
- wR factor = 0.060
- Data-to-parameter ratio = 30.1
checkCIF/PLATON results
No syntax errors found
Alert level A
PLAT432_ALERT_2_A Short Inter X...Y Contact Te1 .. Cl2 .. 3.28 Ang.
| Author Response: This is not a particularly short Te-X contact considering
other structures containing tellurium polycations.
|
Alert level B
PLAT432_ALERT_2_B Short Inter X...Y Contact Te1 .. Cl5 .. 3.38 Ang.
| Author Response: This is not a particularly short Te-X contact considering
other structures containing tellurium polycations.
|
PLAT432_ALERT_2_B Short Inter X...Y Contact Te2 .. Cl2 .. 3.37 Ang.
| Author Response: This is not a particularly short Te-X contact considering
other structures containing tellurium polycations.
|
Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings Differ .... ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ .... ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............ 2.00 Ratio
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Ga1
PLAT431_ALERT_2_C Short Inter HL..A Contact Cl5 .. Cl6 .. 3.44 Ang.
PLAT432_ALERT_2_C Short Inter X...Y Contact Te2 .. Cl5 .. 3.51 Ang.
| Author Response: This is not a particularly short Te-X contact considering
other structures containing tellurium polycations.
|
1 ALERT level A = In general: serious problem
2 ALERT level B = Potentially serious problem
6 ALERT level C = Check and explain
0 ALERT level G = General alerts; check
3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
6 ALERT type 2 Indicator that the structure model may be wrong or deficient
0 ALERT type 3 Indicator that the structure quality may be low
0 ALERT type 4 Improvement, methodology, query or suggestion
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