Acta Cryst. (2005). E61, m582-m584  [ doi:10.1107/S1600536804032891 ]

Acetato[1-(oxazolin-2-ylmethyl-N)-1H-indolyl-C²](triphenylphosphine)palladium(II) dichloromethane solvate

A. R. Cowley, R. I. Cooper, E. Capito, J. M. Brown and A. Ricci

Online 26 February 2005

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.005 Å
• R factor = 0.036
• wR factor = 0.040
• Data-to-parameter ratio = 12.9

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT380_ALERT_4_C Check Incorrectly? Oriented X(sp2)-Methyl Moiety        C14     
PLAT431_ALERT_2_C Short Inter HL..A Contact  Cl1    ..  O1      ..       3.03 Ang.  
PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd.  #          2       
              C H2 Cl2                                                          

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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