# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' y in I 2/a' _shelx_refln_list_code 4 _shelx_F_calc_maximum 625.12 _exptl_crystal_F_000 1880.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 18.5152 _cell_length_b 9.9268 _cell_length_c 20.9475 _cell_angle_alpha 90.000 _cell_angle_beta 94.659 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 106940.53 101813.24 1916.64 o 4 0 0 29023.96 25892.33 687.80 o 6 0 0 14997.20 15601.82 428.64 o 8 0 0 37658.87 39449.07 872.94 o 10 0 0 7158.91 7156.96 329.50 o 12 0 0 3202.63 3029.67 231.69 o 14 0 0 2402.66 2632.50 240.87 o 16 0 0 4251.25 3901.40 312.48 o 18 0 0 2327.01 2243.57 256.75 o 1 1 0 3306.91 3674.18 97.18 o 3 1 0 62.57 85.70 38.81 o 5 1 0 60.99 26.74 22.20 o 7 1 0 5245.77 5970.98 179.19 o 9 1 0 2332.16 2578.36 129.23 o 11 1 0 4228.65 4493.41 191.73 o 13 1 0 18.48 81.59 44.19 o 15 1 0 3091.91 3054.23 189.10 o 17 1 0 1354.05 1377.14 171.63 o 19 1 0 16.62 75.17 88.25 o 21 1 0 173.35 193.20 157.79 o 0 2 0 335.55 326.34 71.27 o 2 2 0 2113.33 2447.11 97.50 o 4 2 0 5268.58 5191.79 174.69 o 6 2 0 1203.27 987.98 83.74 o 8 2 0 8785.33 8105.25 230.14 o 10 2 0 3923.15 3473.32 163.82 o 12 2 0 1269.81 1230.15 108.61 o 14 2 0 2146.93 2160.98 155.07 o 16 2 0 2275.31 2125.08 170.22 o 18 2 0 227.13 193.20 89.07 o 20 2 0 815.63 159.50 137.61 o 1 3 0 23783.62 25914.04 907.40 o 3 3 0 309.05 431.35 67.27 o 5 3 0 10969.84 10023.51 291.76 o 7 3 0 9740.97 10705.25 326.51 o 9 3 0 7672.40 8398.58 378.94 o 11 3 0 1782.78 1898.35 128.45 o 13 3 0 3631.37 3934.54 201.63 o 15 3 0 477.42 533.92 108.27 o 17 3 0 4354.80 4420.11 284.89 o 19 3 0 218.70 226.13 145.23 o 21 3 0 6.42 348.84 285.08 o 0 4 0 6259.75 6034.02 414.66 o 2 4 0 67.86 94.59 54.33 o 4 4 0 1020.06 1123.92 214.66 o 6 4 0 2708.34 2559.58 159.12 o 8 4 0 31129.14 31005.06 682.31 o 10 4 0 4124.55 4112.74 234.79 o 12 4 0 509.09 615.93 119.46 o 14 4 0 1295.01 1290.58 184.19 o 16 4 0 968.92 1214.39 216.36 o 18 4 0 171.04 245.16 147.74 o 20 4 0 83.74 210.06 301.10 o 1 5 0 137.56 98.25 62.19 o 3 5 0 7299.56 7462.38 457.11 o 5 5 0 5297.73 5295.13 249.81 o 7 5 0 2.71 15.58 44.95 o 9 5 0 2560.13 2608.03 364.53 o 11 5 0 7804.43 7316.23 412.75 o 13 5 0 655.44 984.40 182.02 o 15 5 0 12.51 7.61 57.47 o 17 5 0 17.25 79.99 81.61 o 19 5 0 2827.73 2177.87 1742.17 o 0 6 0 743.43 830.68 219.60 o 2 6 0 5596.65 5288.08 345.14 o 4 6 0 582.65 644.52 146.26 o 6 6 0 3771.07 3299.64 213.18 o 8 6 0 904.57 758.54 136.52 o 10 6 0 210.51 219.17 95.73 o 12 6 0 306.11 344.70 119.41 o 14 6 0 58.97 93.43 82.22 o 16 6 0 82.05 142.45 98.11 o 18 6 0 1.00 130.01 103.88 o 1 7 0 7854.61 7804.83 646.88 o 5 7 0 6354.32 6659.86 424.15 o 7 7 0 13.07 74.02 66.18 o 9 7 0 9.79 32.71 63.09 o 11 7 0 2070.46 1789.92 231.25 o 13 7 0 1618.94 1473.04 218.43 o 15 7 0 58.70 104.64 92.10 o 17 7 0 23.79 146.21 138.15 o 0 8 0 311.32 331.11 199.49 o 2 8 0 30.12 38.06 73.48 o 4 8 0 144.54 262.60 123.97 o 6 8 0 1307.72 1380.01 238.11 o 8 8 0 4265.68 3822.88 346.24 o 10 8 0 12.79 -4.74 61.24 o 12 8 0 120.90 125.15 98.70 o 14 8 0 267.77 259.68 124.84 o 16 8 0 9.67 207.11 104.64 o 1 9 0 2004.53 1981.32 274.60 o 3 9 0 705.02 859.44 209.37 o 5 9 0 21.50 86.56 89.78 o 7 9 0 187.47 239.47 130.07 o 9 9 0 2406.14 2330.93 289.09 o 11 9 0 4012.61 3913.63 380.97 o 13 9 0 789.51 809.45 209.05 o 0 10 0 87.47 119.35 176.30 o 2 10 0 148.70 222.83 140.00 o 4 10 0 261.00 312.38 147.07 o 6 10 0 500.80 564.33 192.94 o 8 10 0 283.17 280.75 131.39 o 10 10 0 71.38 235.18 121.77 o 1 11 0 132.83 250.79 151.49 o 3 11 0 1411.75 1627.84 312.53 o 5 11 0 721.62 1073.74 268.49 o 7 11 0 639.51 616.33 203.70 o -20 1 1 1894.60 299.74 257.11 o -18 1 1 159.22 150.03 87.38 o -16 1 1 114.52 97.36 67.43 o -14 1 1 5.33 27.13 41.92 o -12 1 1 4956.23 4938.48 212.67 o -10 1 1 16135.72 15642.23 366.89 o -8 1 1 2638.98 2739.10 127.60 o -6 1 1 3277.68 3063.05 117.98 o -4 1 1 11268.50 10326.70 203.92 o -2 1 1 70333.20 70060.05 1707.73 o 2 1 1 9803.41 10401.08 206.79 o 4 1 1 12601.38 11650.61 218.41 o 6 1 1 20909.98 20400.57 356.45 o 8 1 1 15286.78 16504.51 342.88 o 10 1 1 10389.57 10214.35 284.36 o 12 1 1 12348.42 12298.62 345.37 o 14 1 1 8230.98 8340.81 299.77 o 16 1 1 44.78 100.20 66.24 o 18 1 1 1746.30 2351.09 276.58 o 20 1 1 3635.48 3859.59 366.26 o -21 2 1 492.20 233.20 165.02 o -19 2 1 71.28 156.06 89.30 o -17 2 1 2377.30 2038.16 346.46 o -15 2 1 580.18 848.26 132.55 o -13 2 1 4.11 37.04 42.25 o -11 2 1 0.40 40.95 34.61 o -9 2 1 1258.97 1721.64 110.02 o -7 2 1 5531.62 6313.93 190.29 o -5 2 1 9255.43 8598.86 246.08 o -3 2 1 117.85 131.32 40.86 o -1 2 1 13539.43 14862.66 302.74 o 1 2 1 1356.82 1257.85 94.48 o 3 2 1 4763.38 4718.70 133.52 o 5 2 1 77.74 78.76 34.52 o 7 2 1 33338.82 37593.59 586.17 o 9 2 1 3243.19 3377.60 152.80 o 11 2 1 1124.56 1251.11 103.32 o 13 2 1 387.22 595.97 97.01 o 15 2 1 1972.69 1849.32 150.32 o 17 2 1 516.05 665.05 128.56 o 19 2 1 697.29 1353.20 328.73 o -20 3 1 510.17 435.35 209.89 o -18 3 1 1562.06 1484.38 312.70 o -16 3 1 1695.77 1772.86 317.81 o -14 3 1 251.30 255.60 99.47 o -12 3 1 6244.85 6039.72 241.43 o -10 3 1 20028.84 19748.85 435.08 o -8 3 1 8693.50 7977.91 290.69 o -6 3 1 3975.67 3851.30 223.46 o -4 3 1 1092.31 1110.72 92.95 o -2 3 1 6648.15 6035.23 200.85 o 0 3 1 18723.41 18858.03 511.47 o 2 3 1 6.28 30.55 31.13 o 4 3 1 1384.40 1187.25 94.01 o 6 3 1 4362.07 3991.13 181.34 o 8 3 1 1022.53 1053.12 103.29 o 10 3 1 5449.31 5742.07 218.37 o 12 3 1 5415.44 5810.36 272.22 o 14 3 1 2726.46 2504.06 166.49 o 16 3 1 136.60 229.00 90.16 o 18 3 1 1798.87 1873.78 247.16 o -19 4 1 2459.83 1487.73 1377.99 o -17 4 1 1276.14 1591.39 233.97 o -15 4 1 1242.04 1776.96 342.37 o -13 4 1 3346.50 3417.51 430.00 o -11 4 1 4432.63 4228.07 437.85 o -9 4 1 635.45 629.15 185.16 o -7 4 1 3295.43 2644.49 205.27 o -5 4 1 4145.83 4397.61 249.95 o -3 4 1 138.11 212.49 59.97 o -1 4 1 589.27 701.23 103.36 o 1 4 1 1161.53 1139.07 129.71 o 3 4 1 4394.28 4250.13 166.12 o 5 4 1 755.05 813.12 94.13 o 7 4 1 89.80 246.49 72.73 o 9 4 1 7080.55 6884.36 288.49 o 11 4 1 3183.71 3178.56 210.37 o 13 4 1 340.17 369.27 84.99 o 15 4 1 2078.60 2123.68 199.66 o 17 4 1 6995.13 7671.46 596.58 o -18 5 1 1229.93 1203.84 469.44 o -16 5 1 709.38 404.31 165.20 o -14 5 1 298.99 260.73 111.54 o -12 5 1 1299.36 1280.07 185.39 o -10 5 1 16.06 72.82 56.29 o -8 5 1 727.95 690.27 193.76 o -6 5 1 229.96 208.06 74.76 o -4 5 1 503.88 414.20 89.63 o -2 5 1 3802.09 4146.19 276.32 o 0 5 1 5906.12 5937.21 328.51 o 2 5 1 10.57 -6.42 37.36 o 4 5 1 8943.80 8819.03 412.15 o 6 5 1 7953.37 7638.30 303.67 o 8 5 1 1050.33 968.25 135.90 o 10 5 1 75.06 85.00 53.98 o 12 5 1 148.79 241.02 87.93 o 14 5 1 213.70 248.13 92.20 o 16 5 1 1246.68 1215.22 219.68 o 18 5 1 606.82 402.97 204.09 o -17 6 1 411.94 318.73 127.13 o -15 6 1 492.01 380.01 170.20 o -13 6 1 970.23 735.96 156.63 o -11 6 1 2488.11 2406.57 208.56 o -9 6 1 7172.26 6670.98 331.31 o -7 6 1 4926.27 4889.00 369.14 o -5 6 1 877.40 885.55 120.57 o -3 6 1 727.49 710.21 150.22 o -1 6 1 15996.79 17067.94 645.81 o 1 6 1 44312.35 45964.52 1183.74 o 3 6 1 7771.45 8265.20 434.94 o 5 6 1 52.23 71.61 54.65 o 7 6 1 2571.51 2702.49 248.48 o 9 6 1 8250.43 8010.80 640.40 o 11 6 1 871.20 992.55 181.95 o 13 6 1 4.91 67.59 76.55 o 15 6 1 492.41 521.83 228.48 o 17 6 1 1193.53 773.80 661.37 o -16 7 1 0.16 79.79 86.03 o -14 7 1 487.73 535.04 160.82 o -12 7 1 717.87 592.43 152.53 o -10 7 1 865.06 870.52 162.59 o -8 7 1 961.24 867.85 154.03 o -6 7 1 50.67 61.98 65.69 o -4 7 1 17.64 59.36 68.26 o -2 7 1 656.41 665.25 165.81 o 0 7 1 24.55 23.99 70.64 o 2 7 1 203.59 198.80 102.05 o 4 7 1 8.02 31.19 65.53 o 6 7 1 3.72 64.34 61.38 o 8 7 1 588.36 814.24 151.33 o 10 7 1 28.92 56.20 62.50 o 12 7 1 71.66 138.41 79.74 o 14 7 1 160.49 169.50 100.06 o 16 7 1 0.87 109.02 109.56 o -15 8 1 605.51 791.20 196.20 o -13 8 1 1624.82 1426.59 220.59 o -11 8 1 197.42 145.47 95.37 o -9 8 1 2002.17 1863.04 190.85 o -7 8 1 246.77 335.24 132.01 o -5 8 1 70.67 77.81 81.77 o -3 8 1 218.63 151.73 106.04 o -1 8 1 2059.63 2158.80 264.37 o 1 8 1 5641.46 5788.10 420.61 o 3 8 1 698.98 910.15 198.33 o 5 8 1 220.40 123.12 97.02 o 7 8 1 990.86 1187.62 221.59 o 9 8 1 8108.34 7726.87 387.42 o 11 8 1 766.33 821.93 173.99 o 13 8 1 179.44 179.38 107.80 o 15 8 1 1323.61 1325.56 362.63 o -14 9 1 114.36 200.58 117.30 o -12 9 1 217.90 367.16 144.07 o -10 9 1 70.12 103.05 87.00 o -8 9 1 2902.16 2289.70 287.67 o -6 9 1 115.57 199.00 112.73 o -4 9 1 25.78 47.85 84.67 o -2 9 1 750.43 825.04 213.92 o 0 9 1 25.30 41.44 90.35 o 2 9 1 12.74 51.10 79.22 o 4 9 1 203.68 168.22 109.47 o 6 9 1 691.33 898.74 217.15 o 8 9 1 1833.50 1810.72 258.46 o 10 9 1 133.37 202.98 115.33 o 12 9 1 29.31 42.87 85.31 o 14 9 1 3.72 105.12 98.05 o -11 10 1 202.21 231.45 126.72 o -9 10 1 1079.25 1026.08 239.07 o -7 10 1 3745.54 3844.10 388.92 o -5 10 1 1266.12 1531.26 286.31 o -3 10 1 1439.29 1577.63 291.03 o -1 10 1 109.51 67.18 98.32 o 1 10 1 1040.88 1099.05 258.12 o 3 10 1 599.11 636.80 202.16 o 5 10 1 313.31 437.54 172.26 o 7 10 1 2134.82 2126.30 294.27 o 9 10 1 3337.13 3308.92 361.72 o 11 10 1 806.08 1031.20 242.36 o -6 11 1 0.59 53.67 100.27 o -4 11 1 1580.58 1829.36 307.66 o -2 11 1 1065.15 1353.40 292.96 o 0 11 1 57.12 133.50 126.96 o 2 11 1 28.54 102.96 103.59 o 4 11 1 116.56 269.94 141.92 o 6 11 1 2.35 208.69 128.41 o -22 0 2 661.30 199.49 195.73 o -18 0 2 29.88 73.94 102.75 o -14 0 2 458.93 530.90 375.27 o -12 0 2 11171.60 11527.50 530.09 o -10 0 2 37205.37 41895.89 982.56 o -8 0 2 5974.66 6411.73 286.17 o -4 0 2 124.62 19.12 38.87 o 0 0 2 50896.11 53062.82 982.82 o 2 0 2 1326.93 873.64 104.35 o 4 0 2 23220.29 23276.99 488.82 o 6 0 2 6396.84 5879.55 226.70 o 8 0 2 17683.19 18937.00 519.14 o 10 0 2 10505.03 10509.46 402.01 o 12 0 2 1674.24 1437.43 158.38 o 14 0 2 2237.63 2199.02 213.81 o 16 0 2 234.78 421.22 137.31 o 18 0 2 3974.96 4107.70 516.62 o 20 0 2 1903.64 2512.84 572.88 o -21 1 2 144.54 117.21 83.02 o -19 1 2 0.23 66.41 67.53 o -17 1 2 65.29 75.45 67.62 o -15 1 2 505.87 296.18 141.65 o -13 1 2 1964.61 1965.28 201.25 o -11 1 2 7075.37 7274.60 288.93 o -9 1 2 283.37 309.42 67.61 o -7 1 2 27.33 51.94 35.27 o -5 1 2 79.85 33.86 30.71 o -1 1 2 2941.76 3113.10 180.66 o 1 1 2 75480.06 73689.32 2418.44 o 3 1 2 2384.25 2530.33 73.88 o 5 1 2 7232.15 7031.79 168.96 o 7 1 2 15048.53 16048.44 319.08 o 9 1 2 11.42 50.49 27.74 o 11 1 2 161.45 170.54 51.53 o 13 1 2 0.97 43.01 36.32 o 15 1 2 587.54 707.79 115.20 o 17 1 2 192.93 334.37 177.95 o 19 1 2 98.64 271.86 166.66 o 21 1 2 116.54 234.63 173.34 o -18 2 2 60.50 71.52 68.16 o -12 2 2 8677.58 8901.49 617.55 o -10 2 2 333.98 161.17 117.70 o -8 2 2 19706.93 19254.97 826.93 o -6 2 2 17316.42 16136.51 685.41 o -4 2 2 1668.32 1733.99 176.98 o -2 2 2 628.82 682.21 64.12 o 0 2 2 10961.40 12522.94 343.79 o 2 2 2 2349.94 2097.31 98.57 o 4 2 2 78.21 81.20 41.00 o 6 2 2 1126.89 1017.53 70.93 o 8 2 2 44378.21 49502.53 741.26 o 10 2 2 10940.66 10829.67 296.97 o 12 2 2 556.02 806.69 124.18 o 14 2 2 1622.02 1665.33 142.34 o 16 2 2 8631.13 8152.27 320.54 o 18 2 2 9686.97 9836.19 562.29 o 20 2 2 149.09 590.42 230.02 o -21 3 2 83.80 99.51 90.75 o -19 3 2 28.30 66.23 77.32 o -13 3 2 411.53 175.32 111.73 o -9 3 2 3858.06 3751.01 357.71 o -7 3 2 3579.72 2733.81 281.67 o -5 3 2 138.29 140.43 52.88 o -3 3 2 24250.04 25353.14 1100.80 o -1 3 2 2185.81 2010.43 149.13 o 1 3 2 16197.62 15602.49 450.90 o 3 3 2 224.59 364.88 71.56 o 5 3 2 2223.17 1964.55 123.09 o 7 3 2 2522.05 2285.65 142.20 o 9 3 2 3023.70 3062.06 181.00 o 11 3 2 126.78 155.86 54.14 o 13 3 2 980.30 1188.02 137.96 o 15 3 2 639.59 708.80 118.11 o 17 3 2 12.44 8.02 114.76 o 19 3 2 522.21 861.37 385.67 o 21 3 2 873.06 1537.23 508.77 o -20 4 2 2864.73 1147.22 2523.07 o -18 4 2 1177.97 1414.81 339.64 o -10 4 2 57.77 89.90 64.91 o -8 4 2 3057.54 3055.82 233.90 o -6 4 2 2000.82 1928.73 143.44 o -4 4 2 28103.99 30131.62 627.05 o -2 4 2 313.01 265.62 61.71 o 0 4 2 15694.96 16251.52 647.05 o 2 4 2 911.06 895.44 114.65 o 4 4 2 9473.01 9599.27 356.45 o 6 4 2 11746.69 13063.88 381.51 o 8 4 2 5792.00 5110.16 238.32 o 10 4 2 1344.48 1301.23 131.25 o 12 4 2 601.78 541.06 111.94 o 14 4 2 198.28 462.56 115.36 o 16 4 2 141.17 219.52 122.09 o 18 4 2 99.94 370.67 249.27 o -19 5 2 861.78 1749.01 357.71 o -17 5 2 156.15 239.30 126.29 o -15 5 2 640.48 431.55 263.02 o -13 5 2 667.10 727.94 173.43 o -11 5 2 6675.76 6821.39 585.84 o -9 5 2 5782.30 5808.93 294.50 o -7 5 2 60.16 30.67 41.51 o -5 5 2 1129.51 1149.00 117.85 o -3 5 2 9798.31 8989.08 314.40 o -1 5 2 11171.12 11291.02 470.08 o 1 5 2 2496.41 2632.00 214.43 o 3 5 2 26.90 21.50 43.21 o 5 5 2 644.85 514.47 97.01 o 7 5 2 1224.45 984.31 129.26 o 9 5 2 3389.72 3363.05 214.75 o 11 5 2 179.43 281.30 85.50 o 13 5 2 4576.48 4317.94 266.87 o 15 5 2 3193.57 2856.50 232.71 o 17 5 2 447.54 486.57 176.81 o -18 6 2 4.93 73.97 87.34 o -16 6 2 24.81 101.12 86.19 o -14 6 2 106.55 180.88 93.89 o -12 6 2 4.33 17.68 52.40 o -10 6 2 980.80 766.32 148.55 o -8 6 2 226.44 351.74 107.73 o -6 6 2 1297.84 1358.87 139.06 o -4 6 2 1206.10 1056.03 119.21 o -2 6 2 1029.65 1009.56 170.42 o 0 6 2 3751.06 4389.16 310.42 o 2 6 2 976.78 1014.51 169.75 o 4 6 2 578.24 555.56 134.06 o 6 6 2 112.42 151.42 74.26 o 8 6 2 806.64 856.77 139.39 o 10 6 2 1830.67 1900.76 174.47 o 12 6 2 776.93 759.51 142.17 o 14 6 2 788.23 855.54 163.31 o 16 6 2 215.86 192.32 149.02 o 18 6 2 259.53 292.24 269.39 o -17 7 2 609.02 463.64 163.19 o -15 7 2 563.84 473.90 153.54 o -13 7 2 0.04 12.89 68.61 o -11 7 2 210.69 136.97 90.92 o -9 7 2 1324.09 1232.10 161.94 o -7 7 2 1004.30 911.65 152.49 o -5 7 2 1014.82 1220.19 207.14 o -3 7 2 7167.69 7325.39 619.26 o -1 7 2 10272.36 10583.99 755.32 o 1 7 2 629.19 711.22 163.39 o 3 7 2 1205.21 1219.62 201.47 o 5 7 2 4839.75 4556.95 346.81 o 7 7 2 2837.38 2345.06 352.60 o 9 7 2 3748.30 3859.61 428.30 o 11 7 2 1253.07 970.29 194.35 o 13 7 2 1593.17 1320.26 332.05 o 15 7 2 371.14 376.18 209.89 o 17 7 2 165.31 334.22 169.12 o -16 8 2 23.47 117.89 101.50 o -14 8 2 14.75 68.03 77.81 o -12 8 2 508.19 579.56 157.12 o -10 8 2 191.37 251.65 107.62 o -8 8 2 2.93 30.83 57.44 o -6 8 2 85.01 5.86 62.39 o -4 8 2 708.31 892.23 200.78 o -2 8 2 1489.37 1402.42 239.04 o 0 8 2 53.56 106.32 90.73 o 2 8 2 43.09 45.11 74.15 o 4 8 2 2.43 -0.25 63.11 o 6 8 2 173.96 234.07 119.67 o 8 8 2 2947.50 3068.55 308.51 o 10 8 2 3.56 89.36 73.29 o 12 8 2 54.18 90.51 83.79 o 14 8 2 521.73 487.54 151.85 o -13 9 2 9.74 46.59 70.03 o -11 9 2 1522.72 1595.97 274.29 o -9 9 2 4198.76 3904.77 368.65 o -7 9 2 10.70 35.48 76.32 o -5 9 2 710.39 733.02 202.61 o -3 9 2 1061.58 1273.07 248.06 o -1 9 2 2940.27 3074.60 333.59 o 1 9 2 140.23 205.38 124.47 o 3 9 2 645.82 646.94 191.81 o 5 9 2 2096.69 1968.35 262.84 o 7 9 2 509.78 549.27 178.52 o 9 9 2 70.86 94.72 87.18 o 11 9 2 377.97 415.85 156.97 o 13 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