(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2005). E61, m649-m651 [ doi:10.1107/S1600536805006446 ]

Triphenyl[(2-oxidobenzylideneamino)acetato]antimony(V) dichloromethane solvate

G.-C. Wang, Y.-N. Lu, L. Yu, H.-B. Song and J.-S. Li

Online 11 March 2005

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.010 Å
Disorder in solvent or counterion
R factor = 0.042
wR factor = 0.097
Data-to-parameter ratio = 13.2

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.86 Ratio 
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.02 Ratio 
PLAT221_ALERT_4_C Large Solvent/Anion  C     Ueq(max)/Ueq(min) ...       3.79 Ratio 
PLAT223_ALERT_4_C Large Solvent/Anion  H     Ueq(max)/Ueq(min) ...       3.74 Ratio 
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C40     
PLAT243_ALERT_4_C High  'Solvent' Ueq as Compared to Neighbors for        C56     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for       C56'     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for       C56"     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for       C55'     
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      40.00 Perc. 
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         10       
PLAT431_ALERT_2_C Short Inter HL..A Contact  Cl4    ..  Cl4     ..       3.25 Ang.  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
  12 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   7 ALERT type 4 Improvement, methodology, query or suggestion