Acta Cryst. (2005). E61, m695-m696  [ doi:10.1107/S1600536805007737 ]

[4-Bromo-2-(pyridin-2-ylmethyliminomethyl)phenolato-³O,N,N']methoxocobalt(III) perchlorate

J.-Y. Ma, T.-X. Wu, X.-G. She and X.-F. Pan

Online 18 March 2005

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.007 Å
• Disorder in solvent or counterion
• R factor = 0.047
• wR factor = 0.134
• Data-to-parameter ratio = 15.9

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT430_ALERT_2_B Short Inter D...A Contact  O1     ..  O6      ..       2.66 Ang.  
PLAT430_ALERT_2_B Short Inter D...A Contact  O6     ..  O5'     ..       2.73 Ang.  
PLAT430_ALERT_2_B Short Inter D...A Contact  N1     ..  O2'     ..       2.85 Ang.  
PLAT432_ALERT_2_B Short Inter X...Y Contact  O2     ..  C14     ..       2.91 Ang.  

Alert level C
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......       0.97       
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        Cl1     
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      44.00 Perc. 
PLAT341_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...          7       

   0 ALERT level A = In general: serious problem
   4 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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