Acta Cryst. (2005). E61, m738-m739  [ doi:10.1107/S1600536805008846 ]

(N-Hydroxy-N-phenylbenzamidato-²O,O')oxo[salicylaldehyde (4-nitrobenzoyl)hydrazonato-³O,N,O']vanadium(V)

S. Gao, L.-H. Huo, X.-F. Zhang and S. W. Ng

Online 25 March 2005

Key indicators

• Single-crystal X-ray study
• T = 295 K
• Mean (C-C) = 0.004 Å
• R factor = 0.046
• wR factor = 0.143
• Data-to-parameter ratio = 16.4

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for        C12     

Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.72       
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  V1     -   N1      ..       5.37 su    
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C11     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C13     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C14     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C26     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C27     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         N3     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C9     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C22     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C25     
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist.   C22    -C27           1.37 Ang.  

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
  12 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  13 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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