data_I _shelx_title ' 3b in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 116.11 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7601 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.6363 _cell_length_b 7.2184 _cell_length_c 12.4668 _cell_angle_alpha 90.000 _cell_angle_beta 105.398 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma 2 0 0 3063.08 2923.39 296.78 3 0 0 91.12 69.93 5.73 4 0 0 517.17 504.16 40.44 5 0 0 658.65 651.68 52.32 6 0 0 201.99 211.16 17.16 7 0 0 628.64 596.44 48.66 8 0 0 2.64 3.70 1.88 9 0 0 224.73 252.61 25.43 10 0 0 0.19 4.47 2.53 11 0 0 12.45 13.65 3.61 12 0 0 1.61 1.83 4.47 13 0 0 348.22 360.65 33.04 14 0 0 75.89 77.46 8.08 15 0 0 1.66 15.49 6.09 16 0 0 6.19 7.40 6.06 1 1 0 175.73 193.22 13.00 2 1 0 946.84 875.77 57.47 3 1 0 13480.71 14496.70 1064.84 4 1 0 989.45 985.29 58.91 5 1 0 26.36 20.57 1.67 6 1 0 750.35 706.20 41.65 7 1 0 1552.02 1574.78 92.70 8 1 0 55.33 56.55 3.46 9 1 0 41.80 27.88 2.19 10 1 0 10.36 11.20 1.67 11 1 0 179.92 180.02 15.34 12 1 0 8.93 9.15 2.34 13 1 0 3.24 3.54 2.49 14 1 0 321.99 314.20 29.21 15 1 0 36.49 28.80 4.68 16 1 0 137.05 168.26 16.47 0 2 0 392.75 339.35 46.76 1 2 0 614.18 551.26 34.02 2 2 0 6919.69 7013.75 410.46 3 2 0 266.86 275.87 15.59 4 2 0 1207.03 1242.94 74.18 5 2 0 246.76 271.30 16.24 6 2 0 333.62 331.30 19.86 7 2 0 561.15 532.84 31.83 8 2 0 336.59 320.38 18.46 9 2 0 58.46 54.91 3.67 10 2 0 63.40 68.00 4.55 11 2 0 891.91 859.84 60.51 12 2 0 14.00 15.71 2.84 13 2 0 125.36 106.93 9.54 14 2 0 0.02 0.00 3.50 15 2 0 23.40 27.70 5.97 16 2 0 1.83 1.06 4.37 1 3 0 500.17 482.63 28.57 2 3 0 50.43 52.14 2.98 3 3 0 856.22 866.93 50.66 4 3 0 576.93 604.03 36.87 5 3 0 1062.41 1066.08 66.37 6 3 0 147.59 142.00 9.42 7 3 0 105.48 114.67 7.70 8 3 0 115.28 114.56 7.38 9 3 0 141.16 151.41 9.56 10 3 0 861.17 839.96 58.19 11 3 0 387.30 388.14 27.10 12 3 0 322.20 327.98 23.31 13 3 0 80.89 69.00 7.01 14 3 0 22.24 11.00 3.82 15 3 0 30.39 31.89 5.14 16 3 0 35.51 12.83 8.27 0 4 0 577.68 562.60 56.15 1 4 0 309.78 326.00 19.70 2 4 0 669.07 678.36 41.53 3 4 0 281.30 311.67 19.06 4 4 0 790.90 727.65 50.56 5 4 0 258.67 230.19 15.24 6 4 0 870.50 842.46 55.28 7 4 0 153.83 152.98 10.29 8 4 0 494.65 468.84 29.44 9 4 0 540.05 512.06 33.82 10 4 0 15.13 15.72 2.16 11 4 0 0.13 3.03 1.92 12 4 0 0.80 3.67 2.64 13 4 0 13.31 17.95 4.88 14 4 0 67.55 76.48 9.74 15 4 0 6.28 10.20 9.94 1 5 0 19.85 19.94 1.63 2 5 0 3.39 7.47 1.07 3 5 0 135.36 137.34 11.86 4 5 0 194.33 190.66 16.49 5 5 0 429.83 444.65 38.09 6 5 0 640.10 584.76 50.04 7 5 0 66.86 77.73 6.91 8 5 0 63.39 62.66 5.70 9 5 0 0.14 -1.01 2.13 10 5 0 26.70 26.02 3.15 11 5 0 0.35 0.82 4.22 12 5 0 82.98 78.42 6.64 13 5 0 38.43 35.83 4.52 0 6 0 330.98 335.49 44.19 1 6 0 134.81 138.44 13.12 2 6 0 200.78 189.57 20.37 3 6 0 331.76 352.10 33.41 4 6 0 96.02 89.66 7.95 5 6 0 428.26 430.08 33.40 6 6 0 3.77 0.44 1.65 7 6 0 149.08 144.48 11.53 8 6 0 0.01 -1.66 1.66 9 6 0 12.39 12.31 2.13 10 6 0 47.12 54.34 4.87 11 6 0 17.71 21.74 3.31 12 6 0 7.77 7.98 3.15 13 6 0 94.01 86.47 18.02 1 7 0 29.64 37.12 4.03 2 7 0 30.87 29.42 3.96 3 7 0 154.48 156.42 16.51 4 7 0 169.14 136.06 14.44 5 7 0 63.00 66.23 11.80 6 7 0 0.28 -2.77 2.77 7 7 0 0.79 2.60 3.45 8 7 0 8.78 8.32 2.63 9 7 0 5.15 -0.13 3.43 10 7 0 0.02 -1.35 3.37 11 7 0 1.16 0.20 13.10 0 8 0 41.46 44.57 8.89 1 8 0 89.64 84.73 9.65 2 8 0 88.24 89.51 9.97 3 8 0 207.64 197.99 21.62 4 8 0 6.57 4.16 2.48 5 8 0 2.24 2.01 4.41 6 8 0 9.72 11.64 3.18 7 8 0 34.59 30.09 5.63 1 9 0 47.55 52.11 7.44 2 9 0 31.14 25.60 6.54 3 9 0 3.80 -4.09 4.09 -17 1 1 6.57 14.39 7.36 -16 1 1 30.55 36.66 5.71 -15 1 1 222.76 242.20 22.46 -14 1 1 42.64 37.95 5.14 -13 1 1 43.27 43.08 4.48 -12 1 1 470.16 454.11 35.19 -11 1 1 303.24 301.94 21.87 -10 1 1 320.36 317.76 17.57 -9 1 1 387.72 383.54 22.99 -8 1 1 107.69 118.24 7.18 -7 1 1 533.00 529.60 25.81 -6 1 1 523.08 519.79 29.61 -5 1 1 502.69 506.94 31.71 -4 1 1 43.39 50.07 3.03 -3 1 1 3452.81 3220.58 192.11 -2 1 1 2291.83 2116.34 132.11 -1 1 1 7352.78 8114.19 589.52 0 1 1 1373.41 1304.49 128.88 1 1 1 8718.44 9232.95 603.83 2 1 1 228.58 233.12 15.49 3 1 1 87.25 92.66 5.99 4 1 1 5434.18 5409.45 339.88 5 1 1 78.78 87.23 5.29 6 1 1 3.24 4.45 0.96 7 1 1 38.04 42.03 2.72 8 1 1 8.71 5.94 1.32 9 1 1 177.81 180.92 11.00 10 1 1 16.31 20.08 2.93 11 1 1 0.81 2.79 2.05 12 1 1 822.90 802.94 67.01 13 1 1 25.39 20.50 3.50 14 1 1 617.95 622.45 63.87 15 1 1 0.12 -0.06 3.57 16 1 1 47.86 45.79 9.43 -16 2 1 0.12 -4.16 4.16 -15 2 1 34.16 39.05 7.62 -14 2 1 37.11 31.85 4.44 -13 2 1 13.81 12.55 3.30 -12 2 1 192.61 197.03 20.85 -11 2 1 284.68 288.45 21.85 -10 2 1 84.44 75.51 5.43 -9 2 1 44.59 45.68 3.04 -8 2 1 620.93 575.15 36.04 -7 2 1 262.71 238.12 14.30 -6 2 1 111.19 100.68 6.38 -5 2 1 1649.67 1716.93 107.06 -4 2 1 3805.30 3939.58 245.38 -3 2 1 1065.92 1013.25 58.83 -2 2 1 7646.85 7971.68 443.97 -1 2 1 565.68 482.56 33.09 0 2 1 1745.10 1659.75 131.25 1 2 1 235.69 231.22 16.99 2 2 1 2332.83 2386.26 147.64 3 2 1 92.57 98.83 5.73 4 2 1 563.06 574.46 34.51 5 2 1 1222.24 1159.29 69.36 6 2 1 617.00 616.56 38.52 7 2 1 86.28 97.12 5.86 8 2 1 0.75 0.05 1.24 9 2 1 1453.74 1362.45 85.01 10 2 1 388.17 377.38 24.86 11 2 1 415.13 396.11 26.59 12 2 1 55.11 50.09 5.06 13 2 1 6.81 2.95 2.93 14 2 1 2.30 0.91 3.90 15 2 1 123.34 134.45 15.24 16 2 1 64.48 61.16 9.74 -16 3 1 43.21 40.27 7.36 -15 3 1 1.21 2.54 3.81 -14 3 1 1.85 -1.08 3.31 -13 3 1 81.72 91.05 8.29 -12 3 1 2.87 2.27 2.08 -11 3 1 58.83 56.54 3.90 -10 3 1 27.98 22.10 2.32 -9 3 1 66.12 70.09 4.85 -8 3 1 11.69 8.28 1.86 -7 3 1 339.77 308.70 21.55 -6 3 1 0.20 -1.28 1.28 -5 3 1 28.34 29.33 1.88 -4 3 1 515.68 568.25 34.72 -3 3 1 5.01 7.86 1.01 -2 3 1 1354.20 1348.72 75.18 -1 3 1 256.32 240.82 15.68 0 3 1 164.96 160.58 11.69 1 3 1 208.68 229.59 16.91 2 3 1 124.15 135.89 7.98 3 3 1 1734.60 1782.96 109.69 4 3 1 49.19 46.35 2.91 5 3 1 290.16 286.03 17.91 6 3 1 1270.69 1279.57 83.99 7 3 1 1.10 2.20 1.27 8 3 1 398.11 395.77 25.97 9 3 1 102.77 101.46 6.95 10 3 1 433.53 423.62 28.03 11 3 1 0.52 0.86 1.79 12 3 1 60.90 55.90 4.34 13 3 1 8.25 -1.62 3.28 14 3 1 67.96 68.60 6.85 15 3 1 73.75 60.74 9.12 -15 4 1 0.74 10.53 12.98 -14 4 1 27.36 37.27 5.38 -13 4 1 8.28 10.61 2.95 -12 4 1 30.25 32.75 3.68 -11 4 1 4.20 7.38 1.86 -10 4 1 80.32 71.92 4.77 -9 4 1 51.71 57.62 4.22 -8 4 1 147.81 137.86 9.21 -7 4 1 108.99 105.12 7.15 -6 4 1 45.61 47.43 3.36 -5 4 1 81.29 100.50 6.67 -4 4 1 657.54 656.11 51.98 -3 4 1 606.49 557.61 34.10 -2 4 1 381.63 403.38 27.71 -1 4 1 94.68 105.54 6.89 0 4 1 0.01 1.84 0.98 1 4 1 317.38 311.50 21.59 2 4 1 301.07 312.57 20.03 3 4 1 0.82 1.18 1.19 4 4 1 4.34 6.27 1.17 5 4 1 108.04 103.07 7.28 6 4 1 508.95 517.27 35.95 7 4 1 3.44 6.20 1.86 8 4 1 1095.27 1049.77 68.72 9 4 1 375.60 377.20 27.97 10 4 1 42.86 44.35 5.54 11 4 1 30.87 34.17 3.30 12 4 1 31.94 34.83 3.98 13 4 1 21.53 16.22 3.25 14 4 1 1.83 -4.52 4.52 15 4 1 0.00 13.79 9.02 -13 5 1 20.09 35.48 4.45 -12 5 1 0.30 -0.47 2.89 -11 5 1 50.97 42.17 4.48 -10 5 1 1.55 -2.89 2.89 -9 5 1 17.63 10.99 3.02 -8 5 1 226.12 224.32 19.41 -7 5 1 342.35 320.20 27.65 -6 5 1 279.43 254.94 22.00 -5 5 1 687.20 620.22 59.69 -4 5 1 33.70 41.26 3.84 -3 5 1 41.67 38.05 3.20 -2 5 1 784.56 795.28 56.99 -1 5 1 563.51 560.38 47.22 0 5 1 24.15 25.56 2.47 1 5 1 411.56 396.63 43.91 2 5 1 7.45 8.83 1.10 3 5 1 10.77 13.35 1.73 4 5 1 5.91 5.26 1.68 5 5 1 6.22 3.23 1.47 6 5 1 203.02 189.22 16.36 7 5 1 58.19 54.32 5.08 8 5 1 4.23 3.14 2.68 9 5 1 105.78 86.69 7.74 10 5 1 26.77 23.74 3.07 11 5 1 48.24 43.51 5.19 12 5 1 0.32 0.46 2.63 13 5 1 0.51 -3.28 3.28 -13 6 1 7.61 8.87 6.76 -12 6 1 0.31 -1.33 2.96 -11 6 1 23.33 23.71 3.54 -10 6 1 0.09 -0.05 2.58 -9 6 1 41.72 35.31 3.91 -8 6 1 22.26 19.99 3.60 -7 6 1 15.93 19.04 3.08 -6 6 1 9.12 9.78 1.93 -5 6 1 27.72 27.13 3.02 -4 6 1 111.24 101.28 8.99 -3 6 1 4.39 3.98 1.47 -2 6 1 769.77 697.29 58.98 -1 6 1 8.11 7.90 1.48 0 6 1 70.03 59.11 6.01 1 6 1 6.69 9.47 6.97 2 6 1 35.64 28.60 3.81 3 6 1 0.77 -1.13 3.72 4 6 1 96.29 85.59 8.26 5 6 1 14.07 17.62 2.39 6 6 1 29.25 30.82 3.19 7 6 1 30.99 30.52 3.25 8 6 1 185.65 182.04 15.88 9 6 1 5.63 6.14 2.14 10 6 1 22.79 22.52 4.68 11 6 1 0.78 2.28 2.56 12 6 1 0.90 1.58 4.49 -11 7 1 0.35 2.97 5.36 -10 7 1 0.31 3.32 2.67 -9 7 1 0.12 2.81 2.40 -8 7 1 4.15 3.04 2.11 -7 7 1 1.05 -2.98 2.98 -6 7 1 26.24 26.12 4.07 -5 7 1 1.28 1.42 2.14 -4 7 1 40.30 38.14 4.84 -3 7 1 9.62 10.85 3.07 -2 7 1 285.46 261.19 28.05 -1 7 1 13.62 11.86 3.55 0 7 1 13.15 12.70 4.17 1 7 1 75.64 73.26 8.22 2 7 1 68.07 66.46 7.32 3 7 1 4.36 0.98 1.79 4 7 1 90.36 86.20 9.45 5 7 1 4.39 4.27 1.71 6 7 1 0.00 -1.93 1.93 7 7 1 22.12 19.88 2.99 8 7 1 0.15 1.77 2.62 9 7 1 198.57 206.85 17.69 10 7 1 53.19 60.96 5.47 11 7 1 28.71 33.34 10.64 -7 8 1 49.73 45.03 9.90 -6 8 1 0.65 -1.09 2.67 -5 8 1 8.75 12.80 6.32 -4 8 1 2.18 7.61 2.61 -3 8 1 107.06 94.73 10.88 -2 8 1 10.81 9.02 3.27 -1 8 1 1.94 -0.04 2.21 0 8 1 170.84 175.35 19.09 1 8 1 3.15 0.48 1.95 2 8 1 20.70 22.64 4.64 3 8 1 2.96 8.13 2.47 4 8 1 5.83 3.56 2.28 5 8 1 0.27 -0.33 2.43 6 8 1 1.03 0.32 2.79 7 8 1 0.40 -0.81 3.04 -3 9 1 52.80 60.83 11.82 -2 9 1 42.60 48.87 7.05 -1 9 1 12.29 14.59 3.25 0 9 1 2.01 -2.01 4.50 1 9 1 68.08 76.40 10.50 2 9 1 0.12 -3.45 5.94 3 9 1 138.28 142.88 19.62 -16 0 2 0.57 11.90 11.52 -15 0 2 108.70 142.16 17.70 -14 0 2 425.18 475.32 48.58 -13 0 2 45.14 53.92 6.65 -12 0 2 26.54 22.53 3.99 -11 0 2 291.11 315.89 32.49 -10 0 2 553.70 510.07 51.74 -9 0 2 308.73 378.12 33.49 -8 0 2 635.73 639.25 54.86 -7 0 2 414.07 423.33 31.29 -6 0 2 332.29 332.37 24.61 -5 0 2 506.22 548.94 44.15 -4 0 2 1587.44 1576.38 137.38 -3 0 2 2000.14 1795.71 156.19 -2 0 2 45.73 56.52 5.13 -1 0 2 77.59 72.00 6.55 0 0 2 8881.16 10012.86 892.62 1 0 2 2992.96 3021.78 299.76 2 0 2 935.93 919.84 73.65 3 0 2 5281.78 5506.34 648.33 4 0 2 6337.65 6645.18 592.51 5 0 2 4473.36 4483.76 359.30 6 0 2 65.87 89.24 7.18 7 0 2 528.13 550.12 44.14 8 0 2 1073.56 1085.60 96.39 9 0 2 24.47 24.52 3.63 10 0 2 11.25 7.45 2.68 11 0 2 53.37 58.27 6.07 12 0 2 21.86 35.69 4.55 13 0 2 160.08 207.63 30.84 14 0 2 68.02 67.06 9.69 15 0 2 362.76 447.76 65.32 16 0 2 353.10 363.81 75.48 -17 1 2 90.51 96.83 16.29 -16 1 2 0.37 -2.02 3.72 -15 1 2 17.90 20.02 5.58 -14 1 2 214.77 216.75 18.57 -13 1 2 11.06 7.96 3.02 -12 1 2 138.38 133.06 10.25 -11 1 2 278.51 280.31 21.81 -10 1 2 44.72 49.44 4.16 -9 1 2 0.74 -1.18 1.18 -8 1 2 1108.17 1086.45 67.91 -7 1 2 25.99 35.45 2.16 -6 1 2 448.64 448.79 26.83 -5 1 2 7.94 4.59 0.80 -4 1 2 4253.26 4136.35 257.82 -3 1 2 7728.37 7885.33 551.61 -2 1 2 1319.32 1223.11 81.04 -1 1 2 2674.58 2499.65 163.39 0 1 2 101.51 109.23 6.85 1 1 2 2354.87 2385.23 158.14 2 1 2 356.72 339.59 21.39 3 1 2 1884.76 1825.25 120.65 4 1 2 155.62 165.05 9.92 5 1 2 20.15 21.28 1.73 6 1 2 53.52 56.24 3.53 7 1 2 103.75 120.27 7.30 8 1 2 289.78 319.25 20.16 9 1 2 2.96 5.80 1.72 10 1 2 0.41 -1.24 1.61 11 1 2 0.00 -2.58 2.58 12 1 2 379.90 403.23 33.75 13 1 2 57.82 64.44 5.81 14 1 2 64.47 71.33 7.03 15 1 2 16.57 14.74 5.74 16 1 2 4.15 -10.84 13.68 -16 2 2 12.80 9.40 6.03 -15 2 2 2.60 0.49 5.14 -14 2 2 5.77 3.63 3.21 -13 2 2 0.25 -2.54 2.95 -12 2 2 12.16 4.54 4.16 -11 2 2 125.85 129.21 9.17 -10 2 2 1.28 0.08 2.08 -9 2 2 77.08 79.20 4.93 -8 2 2 72.03 73.04 4.55 -7 2 2 652.11 669.77 40.02 -6 2 2 155.27 157.47 9.53 -5 2 2 157.47 164.95 9.97 -4 2 2 4021.17 4105.74 242.56 -3 2 2 3387.55 3208.42 200.17 -2 2 2 1920.22 1779.78 105.12 -1 2 2 34.67 41.33 3.25 0 2 2 359.49 353.24 31.53 1 2 2 316.86 330.74 20.62 2 2 2 1201.64 1201.81 74.92 3 2 2 1837.93 1875.05 116.85 4 2 2 894.63 927.22 58.39 5 2 2 955.34 922.31 58.08 6 2 2 10.39 13.10 1.72 7 2 2 136.31 125.87 8.08 8 2 2 123.36 131.24 8.07 9 2 2 184.38 188.41 12.58 10 2 2 137.23 150.51 11.49 11 2 2 17.81 15.87 2.53 12 2 2 196.46 199.13 15.73 13 2 2 86.97 84.01 9.50 14 2 2 75.44 77.67 9.06 15 2 2 25.02 25.22 4.35 -16 3 2 4.09 4.91 3.92 -15 3 2 0.02 -4.52 4.52 -14 3 2 6.52 0.54 3.24 -13 3 2 18.97 25.63 4.40 -12 3 2 11.85 6.23 2.52 -11 3 2 7.29 8.59 2.02 -10 3 2 0.18 -1.68 1.68 -9 3 2 300.75 286.83 18.98 -8 3 2 210.54 215.56 14.33 -7 3 2 782.52 798.52 52.57 -6 3 2 2330.94 2339.50 153.22 -5 3 2 587.26 615.34 36.38 -4 3 2 3783.66 3753.83 219.66 -3 3 2 2495.24 2473.49 151.60 -2 3 2 42.75 46.50 2.56 -1 3 2 34.17 37.48 2.75 0 3 2 21.43 29.27 2.52 1 3 2 267.80 283.03 18.59 2 3 2 209.10 215.99 12.21 3 3 2 2031.99 2050.61 121.17 4 3 2 93.24 104.75 6.09 5 3 2 51.45 49.38 3.36 6 3 2 52.06 51.33 3.61 7 3 2 205.69 223.53 15.69 8 3 2 19.20 22.21 2.22 9 3 2 50.62 44.70 3.42 10 3 2 1257.30 1231.37 85.20 11 3 2 74.48 69.66 5.42 12 3 2 45.71 49.84 4.28 13 3 2 30.55 42.91 5.85 14 3 2 39.38 45.90 5.14 15 3 2 3.45 -3.73 4.69 -16 4 2 12.12 12.73 8.35 -15 4 2 5.10 7.57 4.56 -14 4 2 58.82 65.01 7.29 -13 4 2 2.70 1.02 3.53 -12 4 2 24.26 21.42 2.67 -11 4 2 7.42 11.07 2.11 -10 4 2 282.98 286.23 19.08 -9 4 2 49.70 46.19 3.48 -8 4 2 13.60 15.51 1.84 -7 4 2 122.71 127.31 8.58 -6 4 2 973.78 898.54 62.27 -5 4 2 110.58 113.37 8.00 -4 4 2 1.47 0.83 0.90 -3 4 2 59.34 71.55 4.68 -2 4 2 1263.32 1282.84 102.85 -1 4 2 87.41 97.37 7.87 0 4 2 656.67 625.85 49.53 1 4 2 932.30 877.04 69.41 2 4 2 55.63 61.24 4.33 3 4 2 35.96 28.06 2.18 4 4 2 78.41 87.98 6.65 5 4 2 27.24 23.43 2.23 6 4 2 263.41 271.05 20.12 7 4 2 2730.16 2605.09 191.86 8 4 2 43.90 53.28 4.22 9 4 2 4.13 0.31 1.78 10 4 2 131.24 117.01 8.79 11 4 2 5.31 1.54 2.94 12 4 2 9.14 4.01 2.39 13 4 2 109.69 121.81 11.56 14 4 2 0.89 -5.56 5.56 -14 5 2 2.51 8.01 5.71 -13 5 2 144.58 146.10 14.05 -12 5 2 4.98 15.19 3.19 -11 5 2 10.99 1.68 2.45 -10 5 2 107.19 114.31 9.98 -9 5 2 428.55 411.04 35.22 -8 5 2 134.61 139.38 15.84 -7 5 2 0.00 1.88 1.87 -6 5 2 451.99 422.34 40.82 -5 5 2 15.83 18.27 2.11 -4 5 2 16.07 21.14 3.16 -3 5 2 15.64 12.93 1.40 -2 5 2 10.40 10.73 2.02 -1 5 2 226.05 259.21 28.70 0 5 2 132.99 138.37 15.56 1 5 2 29.93 32.94 4.10 2 5 2 255.47 256.50 19.90 3 5 2 28.90 34.81 3.38 4 5 2 131.37 137.54 12.04 5 5 2 60.57 66.16 5.88 6 5 2 50.42 51.50 4.77 7 5 2 602.32 569.44 49.08 8 5 2 821.72 744.68 63.91 9 5 2 6.97 8.71 2.37 10 5 2 181.06 168.76 14.82 11 5 2 72.52 66.58 7.02 12 5 2 34.20 41.19 5.35 13 5 2 4.34 11.53 5.44 -13 6 2 44.95 44.45 6.46 -12 6 2 9.00 10.50 3.17 -11 6 2 2.12 -0.55 3.90 -10 6 2 24.12 25.90 3.32 -9 6 2 209.03 196.00 17.19 -8 6 2 24.09 19.45 2.69 -7 6 2 76.98 68.40 6.47 -6 6 2 16.70 14.42 3.52 -5 6 2 19.99 16.54 2.63 -4 6 2 196.81 196.52 18.73 -3 6 2 519.71 525.04 49.69 -2 6 2 3.88 0.59 1.73 -1 6 2 502.63 498.76 55.01 0 6 2 154.28 147.21 16.61 1 6 2 58.06 69.52 8.28 2 6 2 101.33 95.91 9.25 3 6 2 50.32 51.53 5.45 4 6 2 2.19 2.87 1.82 5 6 2 232.62 243.36 23.21 6 6 2 20.09 24.67 2.95 7 6 2 0.78 3.83 2.70 8 6 2 14.71 11.99 2.43 9 6 2 267.20 259.54 22.62 10 6 2 4.74 3.00 3.01 11 6 2 22.62 23.34 3.45 12 6 2 18.71 12.63 6.78 -11 7 2 106.56 117.64 14.27 -10 7 2 4.35 9.27 2.91 -9 7 2 12.84 7.73 3.81 -8 7 2 7.09 7.34 2.55 -7 7 2 212.59 211.75 20.26 -6 7 2 19.97 28.37 3.59 -5 7 2 30.92 29.20 4.05 -4 7 2 0.42 3.91 2.06 -3 7 2 25.14 23.97 4.39 -2 7 2 46.25 49.38 7.43 -1 7 2 32.48 37.43 8.95 0 7 2 21.61 19.50 4.85 1 7 2 40.27 40.55 6.25 2 7 2 0.22 -1.34 1.89 3 7 2 13.39 19.40 2.66 4 7 2 0.46 -1.32 1.73 5 7 2 117.45 128.82 12.62 6 7 2 14.45 9.46 2.30 7 7 2 0.40 -0.17 3.22 8 7 2 35.14 43.90 5.02 9 7 2 12.48 7.94 2.81 10 7 2 2.94 -1.24 4.06 -7 8 2 49.73 56.31 7.17 -6 8 2 13.94 8.50 5.17 -5 8 2 2.11 1.69 3.60 -4 8 2 135.36 137.36 18.21 -3 8 2 80.39 78.45 10.59 -2 8 2 454.32 440.01 57.20 -1 8 2 1.36 -1.40 3.86 0 8 2 24.09 28.26 5.15 1 8 2 16.30 13.12 4.07 2 8 2 24.84 27.22 3.94 3 8 2 20.07 21.07 3.28 4 8 2 25.69 29.77 4.23 5 8 2 0.00 -0.77 2.63 6 8 2 1.08 -1.59 2.34 8 8 2 32.89 41.76 10.88 -3 9 2 3.59 4.91 3.04 -2 9 2 46.55 56.50 10.76 -1 9 2 9.22 18.48 5.50 2 9 2 2.08 5.08 3.24 3 9 2 24.93 30.22 11.75 -17 1 3 8.12 -5.66 6.78 -16 1 3 7.59 4.39 3.77 -15 1 3 16.72 13.23 3.66 -14 1 3 294.21 312.54 28.96 -13 1 3 39.95 47.08 4.61 -12 1 3 10.98 3.89 2.19 -11 1 3 109.64 103.44 8.49 -10 1 3 26.79 26.72 2.71 -9 1 3 79.40 85.46 5.14 -8 1 3 969.70 989.81 61.78 -7 1 3 551.26 576.20 33.99 -6 1 3 892.95 884.17 52.61 -5 1 3 31.08 33.77 2.18 -4 1 3 2.22 2.32 0.75 -3 1 3 228.68 220.36 13.92 -2 1 3 0.83 1.24 0.85 -1 1 3 2362.19 2359.81 156.53 0 1 3 272.73 261.00 17.39 1 1 3 4684.47 4626.90 275.61 2 1 3 921.93 831.14 52.26 3 1 3 413.43 438.66 26.11 4 1 3 96.59 113.63 6.95 5 1 3 1079.12 1159.57 72.91 6 1 3 449.07 490.45 29.19 7 1 3 2.56 0.31 1.40 8 1 3 0.03 -1.36 1.36 9 1 3 34.35 34.37 2.90 10 1 3 0.29 0.20 2.00 11 1 3 2.88 3.87 2.25 12 1 3 10.71 4.76 2.58 13 1 3 79.64 63.16 7.64 14 1 3 58.94 62.13 6.00 15 1 3 0.00 -4.25 4.66 -17 2 3 6.36 -9.24 9.24 -16 2 3 30.56 31.16 4.99 -15 2 3 7.11 -1.37 3.43 -14 2 3 31.22 27.23 5.12 -13 2 3 120.14 117.75 11.15 -12 2 3 392.15 363.10 33.43 -11 2 3 268.73 269.76 19.20 -10 2 3 315.48 304.33 20.05 -9 2 3 23.15 24.02 2.44 -8 2 3 310.95 344.35 20.67 -7 2 3 40.14 45.05 2.90 -6 2 3 99.54 123.55 7.55 -5 2 3 3295.56 3261.88 213.61 -4 2 3 2542.32 2544.95 158.46 -3 2 3 469.59 465.18 28.91 -2 2 3 1829.27 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175.95 12.53 7 3 3 344.70 321.25 21.29 8 3 3 312.03 317.94 21.03 9 3 3 9.95 5.29 1.91 10 3 3 61.61 67.16 5.25 11 3 3 8.34 7.98 2.47 12 3 3 33.32 38.17 4.19 13 3 3 44.94 43.90 5.49 14 3 3 11.48 8.17 3.81 15 3 3 0.77 6.09 14.44 -16 4 3 17.43 13.92 11.23 -15 4 3 1.83 2.28 4.81 -14 4 3 38.79 41.58 5.43 -13 4 3 4.27 1.53 2.72 -12 4 3 3.21 0.76 2.08 -11 4 3 18.94 15.85 2.54 -10 4 3 3.37 2.12 1.84 -9 4 3 429.60 412.18 30.49 -8 4 3 44.94 47.92 3.70 -7 4 3 15.66 18.54 1.98 -6 4 3 0.21 -1.22 1.22 -5 4 3 69.70 76.57 5.72 -4 4 3 99.93 116.19 7.60 -3 4 3 107.95 117.04 8.12 -2 4 3 80.24 98.04 8.08 -1 4 3 42.35 49.29 4.20 0 4 3 80.40 104.94 9.43 1 4 3 93.25 99.71 6.94 2 4 3 134.95 118.49 8.26 3 4 3 256.55 258.28 19.12 4 4 3 79.83 85.25 6.30 5 4 3 416.12 406.00 29.98 6 4 3 882.06 854.66 63.04 7 4 3 488.18 470.19 34.84 8 4 3 458.11 448.31 33.08 9 4 3 124.42 126.26 9.71 10 4 3 17.50 18.33 2.57 11 4 3 38.01 45.01 4.91 12 4 3 121.68 119.51 10.13 13 4 3 46.26 48.36 5.02 14 4 3 8.67 -2.30 9.74 -14 5 3 29.01 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3 2.57 2.30 3.60 4 8 3 18.10 16.90 3.06 5 8 3 0.61 4.47 2.55 6 8 3 45.74 42.31 4.88 7 8 3 64.51 104.36 22.81 -3 9 3 65.86 60.02 11.47 2 9 3 386.70 417.10 79.60 -16 0 4 8.31 2.67 4.97 -15 0 4 45.04 46.56 8.04 -14 0 4 61.99 64.47 8.66 -13 0 4 4.59 8.07 4.20 -12 0 4 34.18 28.72 4.49 -11 0 4 525.20 568.69 67.03 -10 0 4 1140.18 1143.53 165.42 -9 0 4 535.68 518.34 61.12 -8 0 4 14.61 15.16 3.30 -7 0 4 529.44 531.96 42.79 -6 0 4 174.62 147.59 13.42 -5 0 4 343.32 336.15 27.03 -4 0 4 291.63 293.48 23.59 -3 0 4 3385.71 3348.95 268.00 -2 0 4 631.08 631.41 50.57 -1 0 4 55.91 60.72 6.36 0 0 4 1606.75 1633.73 130.75 1 0 4 1175.34 1307.57 116.50 2 0 4 118.72 109.01 8.94 3 0 4 320.58 349.85 28.02 4 0 4 97.39 111.30 9.24 5 0 4 4074.85 4207.01 335.85 6 0 4 338.41 374.06 33.49 7 0 4 163.12 194.10 17.65 8 0 4 673.54 660.78 67.52 9 0 4 1.46 0.89 2.75 10 0 4 0.07 5.92 4.24 11 0 4 28.67 28.59 4.37 12 0 4 66.06 80.84 10.77 13 0 4 298.96 294.60 35.32 14 0 4 9.68 9.70 6.87 15 0 4 47.92 77.56 19.89 -17 1 4 86.47 82.71 11.32 -16 1 4 40.38 51.00 7.93 -15 1 4 16.81 10.66 3.47 -14 1 4 62.96 57.04 5.66 -13 1 4 9.63 5.77 3.53 -12 1 4 9.14 7.98 2.39 -11 1 4 12.40 15.86 2.27 -10 1 4 14.97 15.75 1.91 -9 1 4 553.42 543.97 36.11 -8 1 4 144.58 139.22 9.46 -7 1 4 26.04 20.25 1.64 -6 1 4 268.75 269.01 16.12 -5 1 4 72.69 93.52 6.06 -4 1 4 497.40 508.35 30.28 -3 1 4 103.19 97.09 5.93 -2 1 4 1.67 -0.18 0.73 -1 1 4 822.10 782.59 48.79 0 1 4 92.35 109.93 7.04 1 1 4 40.21 47.69 2.97 2 1 4 1300.01 1464.82 87.33 3 1 4 668.94 684.17 40.84 4 1 4 1596.93 1590.88 98.82 5 1 4 51.97 56.96 3.60 6 1 4 194.71 193.66 12.38 7 1 4 76.49 74.50 5.31 8 1 4 552.03 520.84 36.99 9 1 4 68.41 83.31 6.30 10 1 4 0.24 -2.02 2.08 11 1 4 37.68 38.07 3.89 12 1 4 1.77 -0.04 2.76 13 1 4 11.72 10.03 3.10 14 1 4 5.33 9.76 4.81 15 1 4 165.93 167.06 36.17 -17 2 4 14.84 6.78 11.11 -16 2 4 0.17 4.07 3.67 -15 2 4 34.43 30.21 6.56 -14 2 4 168.36 150.06 16.06 -13 2 4 27.17 28.77 3.84 -12 2 4 54.93 63.68 5.92 -11 2 4 115.50 101.88 8.71 -10 2 4 16.27 17.23 3.29 -9 2 4 23.38 25.12 2.59 -8 2 4 68.65 75.56 4.99 -7 2 4 252.72 270.51 18.04 -6 2 4 22.95 23.58 1.88 -5 2 4 27.05 27.57 2.06 -4 2 4 128.16 141.37 8.52 -3 2 4 1342.36 1345.48 83.55 -2 2 4 630.95 600.15 37.45 -1 2 4 481.46 473.20 29.44 0 2 4 2115.66 2070.91 128.87 1 2 4 2427.53 2320.76 144.67 2 2 4 83.69 80.70 5.19 3 2 4 242.70 243.62 15.46 4 2 4 330.61 385.68 24.30 5 2 4 73.93 79.70 5.48 6 2 4 8.12 13.11 1.99 7 2 4 25.34 22.26 2.15 8 2 4 129.89 124.41 9.15 9 2 4 140.16 140.99 10.26 10 2 4 6.31 6.98 3.83 11 2 4 204.09 207.35 17.83 12 2 4 36.50 33.13 4.01 13 2 4 6.59 -3.08 4.14 14 2 4 11.91 1.80 6.82 15 2 4 8.36 -8.77 8.77 -16 3 4 5.54 -3.48 3.75 -15 3 4 0.25 -3.87 3.87 -14 3 4 46.30 65.28 11.44 -13 3 4 63.36 52.28 5.22 -12 3 4 55.39 46.78 5.87 -11 3 4 19.35 17.61 2.17 -10 3 4 30.50 32.31 2.74 -9 3 4 159.81 159.56 12.09 -8 3 4 0.02 -1.38 1.38 -7 3 4 734.80 727.00 54.34 -6 3 4 463.44 449.46 29.90 -5 3 4 320.82 331.57 21.99 -4 3 4 0.05 -0.39 1.20 -3 3 4 3.74 7.76 1.38 -2 3 4 249.29 247.96 15.45 -1 3 4 323.13 303.79 18.88 0 3 4 20.14 25.81 1.83 1 3 4 105.17 123.44 7.85 2 3 4 620.09 663.67 41.43 3 3 4 48.31 55.82 3.84 4 3 4 62.17 67.81 4.66 5 3 4 4.72 3.28 1.36 6 3 4 314.52 308.46 21.71 7 3 4 3.57 0.93 1.61 8 3 4 0.11 1.04 1.81 9 3 4 0.44 -2.00 2.00 10 3 4 10.53 12.97 2.45 11 3 4 10.08 2.66 3.17 12 3 4 20.52 20.60 3.56 13 3 4 72.23 61.57 6.50 14 3 4 15.98 19.68 8.55 -16 4 4 6.78 -7.03 7.03 -15 4 4 65.69 69.77 8.44 -14 4 4 56.23 79.33 9.35 -13 4 4 92.82 104.68 12.35 -12 4 4 13.34 15.18 2.97 -11 4 4 32.70 34.48 4.48 -10 4 4 13.89 15.08 2.23 -9 4 4 49.35 38.64 3.51 -8 4 4 1.76 -1.31 1.64 -7 4 4 792.04 797.51 63.80 -6 4 4 321.64 348.87 28.07 -5 4 4 176.43 168.01 13.60 -4 4 4 892.55 857.18 63.34 -3 4 4 72.80 92.49 6.40 -2 4 4 18.82 20.25 1.75 -1 4 4 480.62 480.94 32.94 0 4 4 86.55 103.92 7.25 1 4 4 4.49 4.94 1.02 2 4 4 1.37 2.25 1.19 3 4 4 693.20 700.57 56.10 4 4 4 222.11 211.04 15.75 5 4 4 29.20 33.27 3.29 6 4 4 73.48 69.50 5.58 7 4 4 170.32 175.12 13.08 8 4 4 4.34 0.11 2.11 9 4 4 146.98 147.24 11.24 10 4 4 11.62 7.12 3.36 11 4 4 40.30 41.54 4.50 12 4 4 7.87 4.46 3.03 13 4 4 26.69 29.40 12.09 -14 5 4 1.44 5.36 4.33 -13 5 4 87.42 85.83 9.19 -12 5 4 29.54 23.44 5.35 -11 5 4 10.86 5.29 2.43 -10 5 4 774.95 762.90 65.30 -9 5 4 236.62 233.04 20.19 -8 5 4 0.04 -2.03 2.03 -7 5 4 188.10 187.09 18.39 -6 5 4 421.62 403.23 39.09 -5 5 4 0.21 0.10 2.65 -4 5 4 215.50 210.79 20.51 -3 5 4 93.58 104.43 9.17 -2 5 4 20.19 22.49 2.34 -1 5 4 691.60 722.22 79.22 0 5 4 16.34 19.40 3.18 1 5 4 13.82 13.04 3.09 2 5 4 207.50 215.14 17.18 3 5 4 205.37 198.90 15.94 4 5 4 303.41 306.67 24.32 5 5 4 1.79 1.86 2.48 6 5 4 25.89 30.56 3.17 7 5 4 10.34 9.51 2.90 8 5 4 84.89 90.43 7.46 9 5 4 61.01 54.05 5.11 10 5 4 428.49 435.57 38.36 11 5 4 188.06 183.14 16.61 12 5 4 18.13 13.57 4.23 -13 6 4 15.89 9.12 4.09 -12 6 4 1.15 -0.53 3.16 -11 6 4 5.80 3.43 3.23 -10 6 4 22.18 23.10 3.62 -9 6 4 100.44 106.33 10.79 -8 6 4 103.21 117.77 11.70 -7 6 4 66.64 69.04 7.20 -6 6 4 81.10 78.00 8.99 -5 6 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6 21.67 23.60 2.05 -4 3 6 26.36 25.86 2.23 -3 3 6 6.47 5.72 1.47 -2 3 6 7.45 5.85 1.21 -1 3 6 550.64 541.17 36.01 0 3 6 33.47 39.25 3.58 1 3 6 86.29 83.03 5.70 2 3 6 86.55 89.47 6.15 3 3 6 82.21 85.88 5.95 4 3 6 0.04 0.63 1.59 5 3 6 17.43 19.07 2.26 6 3 6 4.75 0.67 1.82 7 3 6 510.06 471.11 35.83 8 3 6 604.76 581.50 44.38 9 3 6 4.57 1.20 3.34 10 3 6 3.82 5.93 2.98 11 3 6 0.77 1.26 3.72 12 3 6 8.06 0.97 3.82 -15 4 6 11.75 15.58 6.06 -14 4 6 26.28 25.36 5.98 -13 4 6 2.11 -3.02 3.02 -12 4 6 26.77 20.99 4.24 -11 4 6 126.66 131.18 11.14 -10 4 6 4.95 -1.77 2.87 -9 4 6 334.63 334.65 27.04 -8 4 6 0.05 1.52 2.67 -7 4 6 93.53 94.05 7.91 -6 4 6 167.05 165.08 13.36 -5 4 6 876.20 837.56 67.27 -4 4 6 51.18 49.88 4.40 -3 4 6 9.82 9.95 1.73 -2 4 6 251.54 258.96 20.88 -1 4 6 158.30 155.31 12.55 0 4 6 5.19 5.65 1.48 1 4 6 0.57 -0.66 1.46 2 4 6 235.95 215.11 17.49 3 4 6 21.24 21.93 2.69 4 4 6 3.40 1.07 1.77 5 4 6 1.44 2.53 3.20 6 4 6 8.17 8.46 2.75 7 4 6 214.22 208.30 19.09 8 4 6 42.38 52.21 5.75 9 4 6 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5 6 8 65.58 70.76 7.73 6 6 8 4.48 2.33 3.28 7 6 8 53.79 79.08 18.02 -10 7 8 1.45 -2.22 8.54 -9 7 8 12.12 20.00 9.36 -8 7 8 104.95 140.74 17.39 -7 7 8 159.41 191.22 20.96 -6 7 8 2.88 3.66 3.99 -5 7 8 4.79 2.33 3.17 -4 7 8 27.71 23.62 4.22 -3 7 8 4.11 5.67 3.05 -2 7 8 26.95 29.77 4.55 -1 7 8 11.88 20.79 4.98 0 7 8 19.85 19.96 3.64 1 7 8 14.93 12.60 3.20 2 7 8 22.59 32.57 7.61 3 7 8 0.39 -3.35 3.85 4 7 8 11.47 19.16 5.15 5 7 8 37.51 20.70 8.66 -4 8 8 60.50 45.86 12.87 -3 8 8 22.64 29.83 10.88 -2 8 8 18.18 21.05 10.41 -1 8 8 59.49 73.47 18.13 1 8 8 28.52 28.66 10.29 -16 1 9 0.70 -0.55 6.52 -15 1 9 5.24 1.83 4.21 -14 1 9 67.85 76.73 6.86 -13 1 9 56.18 63.61 6.51 -12 1 9 0.00 -1.96 2.49 -11 1 9 160.92 177.13 13.55 -10 1 9 1020.64 1017.74 84.91 -9 1 9 3.92 5.77 2.01 -8 1 9 375.54 363.99 26.10 -7 1 9 165.71 155.97 11.19 -6 1 9 2.52 1.46 1.85 -5 1 9 35.58 30.30 3.70 -4 1 9 8.24 5.00 1.75 -3 1 9 57.81 64.79 4.91 -2 1 9 328.96 339.02 24.27 -1 1 9 142.74 150.65 10.89 0 1 9 9.71 7.62 1.94 1 1 9 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1.09 0.60 4.76 2 6 9 15.69 20.64 7.37 3 6 9 39.43 49.08 6.63 4 6 9 45.02 55.31 10.62 5 6 9 11.46 10.15 4.47 6 6 9 47.69 68.20 15.79 -9 7 9 2.61 10.99 10.29 -8 7 9 53.85 51.36 14.04 -7 7 9 72.14 84.57 13.62 -6 7 9 1.29 2.18 4.54 -5 7 9 17.34 10.44 7.53 -4 7 9 0.11 1.74 6.07 -3 7 9 14.99 16.16 3.68 -2 7 9 71.78 72.94 9.01 -1 7 9 0.22 6.12 3.66 0 7 9 78.36 85.98 9.20 1 7 9 0.01 0.72 3.11 2 7 9 7.03 21.08 6.90 3 7 9 5.38 14.27 8.77 -16 0 10 0.07 -8.89 8.89 -15 0 10 0.39 6.42 5.56 -14 0 10 11.84 11.41 5.14 -13 0 10 469.86 493.71 58.71 -12 0 10 185.10 200.68 24.47 -11 0 10 9.20 11.64 7.10 -10 0 10 100.45 123.43 15.33 -9 0 10 154.43 175.58 21.15 -8 0 10 1.30 -2.71 5.18 -7 0 10 47.13 47.34 8.66 -6 0 10 309.07 301.86 31.22 -5 0 10 4.10 5.85 2.90 -4 0 10 92.60 94.47 10.32 -3 0 10 88.22 90.60 8.40 -2 0 10 16.14 6.73 2.37 -1 0 10 22.39 18.53 3.23 0 0 10 225.36 223.58 23.20 1 0 10 2053.46 1966.87 231.66 2 0 10 1639.60 1552.08 183.13 3 0 10 135.40 149.75 18.11 4 0 10 1590.62 1564.41 184.41 5 0 10 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