(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2005). E61, m699-m701 [ doi:10.1107/S1600536805005738 ]

trans-Carbonylchlorobis(tri-m-tolylphosphino)rhodium(I) dichloromethane solvate

R. Meijboom, A. Muller and A. Roodt

Online 18 March 2005

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.010 Å
Disorder in solvent or counterion
R factor = 0.062
wR factor = 0.151
Data-to-parameter ratio = 19.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT202_ALERT_3_C Isotropic non-H Atoms in Anion/Solvent .........          3       
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.75 Ratio 
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.18 Ratio 
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C65     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C13     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        C1A     
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      50.00 Perc. 
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         10       
PLAT720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........          4       

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   9 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion