# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 040525A in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 321.94 _exptl_crystal_F_000 1184.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.7290 _cell_length_b 12.1160 _cell_length_c 19.5520 _cell_angle_alpha 89.721 _cell_angle_beta 85.328 _cell_angle_gamma 66.677 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2661.75 2385.26 62.16 o 2 0 0 33458.34 30829.95 668.13 o 3 0 0 17926.45 16785.13 414.45 o 4 0 0 19642.54 18605.45 694.03 o 5 0 0 4146.09 3776.63 255.39 o 6 0 0 8751.60 7414.05 478.96 o 7 0 0 2630.09 2275.60 162.73 o 8 0 0 1458.54 1622.03 165.47 o 9 0 0 3022.17 2816.77 215.61 o 10 0 0 551.85 554.46 148.66 o 11 0 0 1014.80 988.90 177.39 o -11 1 0 83.52 348.92 186.77 o -10 1 0 993.19 762.05 156.57 o -9 1 0 620.42 591.21 142.99 o -8 1 0 1743.09 1625.46 169.48 o -7 1 0 1366.15 1057.51 127.06 o -6 1 0 3678.36 3450.26 153.45 o -5 1 0 2476.37 2560.59 77.32 o -4 1 0 1403.91 1239.76 50.33 o -3 1 0 20665.94 20621.40 342.76 o -2 1 0 30425.77 33406.15 525.11 o -1 1 0 5757.70 6707.07 156.48 o 0 1 0 40.16 -0.49 8.99 o 1 1 0 31456.03 26534.09 564.04 o 2 1 0 427.27 409.40 64.99 o 3 1 0 16199.61 16980.59 500.95 o 4 1 0 218.04 274.75 21.80 o 5 1 0 1650.23 1480.81 110.44 o 6 1 0 2123.35 2218.13 150.22 o 7 1 0 6243.87 5841.61 263.99 o 8 1 0 2135.47 2002.33 165.17 o 9 1 0 47.55 31.08 107.12 o 10 1 0 1498.68 1268.13 169.18 o 11 1 0 36.29 78.78 154.13 o -10 2 0 180.25 476.56 172.99 o -9 2 0 778.85 575.86 154.52 o -8 2 0 94.81 29.61 119.53 o -7 2 0 1099.80 1059.76 129.99 o -6 2 0 1111.12 936.91 62.44 o -5 2 0 3575.10 3380.33 208.23 o -4 2 0 5459.42 5051.58 120.93 o -3 2 0 13344.98 14753.37 264.47 o -2 2 0 13447.96 14229.06 327.32 o -1 2 0 2756.54 2773.66 89.43 o 0 2 0 5469.40 4893.57 129.01 o 1 2 0 51.64 45.94 18.18 o 2 2 0 632.53 713.47 30.08 o 3 2 0 4482.28 4952.77 249.18 o 4 2 0 6564.05 6927.35 135.12 o 5 2 0 2935.98 2722.50 96.07 o 6 2 0 1709.09 1583.33 126.67 o 7 2 0 5224.73 5458.49 255.09 o 8 2 0 2159.36 1896.38 167.03 o 9 2 0 1825.31 1570.72 169.18 o 10 2 0 64.58 200.75 139.18 o 11 2 0 1024.31 831.44 170.26 o 12 2 0 45.90 -181.11 148.56 o -10 3 0 477.71 530.42 186.48 o -9 3 0 52.37 7.92 138.00 o -8 3 0 2032.80 1790.24 190.98 o -7 3 0 1545.02 1343.09 159.90 o -6 3 0 1753.40 1758.17 85.52 o -5 3 0 2189.79 2339.92 89.81 o -4 3 0 1068.42 1197.82 90.11 o -3 3 0 1482.63 1530.29 139.08 o -2 3 0 3479.18 4078.45 132.63 o -1 3 0 12360.10 14112.08 337.00 o 0 3 0 146.33 39.26 21.40 o 1 3 0 24891.26 26780.45 440.89 o 2 3 0 9951.85 9930.48 180.66 o 3 3 0 25970.96 27076.03 440.76 o 4 3 0 5926.91 5828.52 124.79 o 5 3 0 22384.20 21780.05 426.67 o 6 3 0 3473.21 3223.01 85.81 o 7 3 0 5243.05 4995.51 239.55 o 8 3 0 2193.10 1939.68 170.06 o 9 3 0 2019.32 1620.08 165.17 o 10 3 0 1682.69 1497.32 187.65 o 11 3 0 154.25 9.58 149.63 o 12 3 0 990.47 1042.07 201.63 o -9 4 0 393.98 478.91 158.53 o -8 4 0 686.10 402.58 152.66 o -7 4 0 1556.98 1605.62 181.99 o -6 4 0 2565.33 2403.15 192.44 o -5 4 0 1441.18 1492.22 81.59 o -4 4 0 2334.75 2556.04 100.01 o -3 4 0 2457.74 2430.71 114.25 o -2 4 0 8675.93 8800.39 244.83 o -1 4 0 2780.08 2274.13 103.01 o 0 4 0 14740.35 14941.44 314.47 o 1 4 0 292.98 317.66 106.24 o 2 4 0 9500.46 10479.07 198.50 o 3 4 0 464.23 474.67 38.33 o 4 4 0 12204.66 13225.72 246.11 o 5 4 0 1748.43 1978.20 143.33 o 6 4 0 6368.04 7662.12 167.16 o 7 4 0 397.70 339.26 45.22 o 8 4 0 2388.55 2503.81 188.83 o 9 4 0 1120.63 1008.64 142.21 o 10 4 0 366.34 328.49 129.60 o 11 4 0 976.16 1011.38 170.06 o 12 4 0 36.65 219.03 174.56 o -9 5 0 313.99 124.91 181.50 o -8 5 0 255.53 278.84 166.45 o -7 5 0 1265.05 1220.83 180.52 o -6 5 0 426.00 522.01 136.93 o -5 5 0 3219.34 3253.00 127.71 o -4 5 0 2679.69 2595.05 109.12 o -3 5 0 8525.72 8589.96 261.15 o -2 5 0 274.87 72.03 62.84 o -1 5 0 16798.65 15338.28 391.92 o 0 5 0 3456.02 2832.45 112.01 o 1 5 0 12935.60 12548.39 193.33 o 2 5 0 139.19 111.31 47.60 o 3 5 0 6187.23 6416.68 146.61 o 4 5 0 369.56 434.99 71.59 o 5 5 0 9982.79 11004.96 296.04 o 6 5 0 2186.51 2454.94 87.96 o 7 5 0 1154.90 1409.94 144.01 o 8 5 0 5401.33 5623.76 280.99 o 9 5 0 114.36 162.93 108.19 o 10 5 0 1093.14 1151.34 163.71 o 11 5 0 86.58 41.44 128.03 o 12 5 0 433.08 542.34 165.47 o -8 6 0 333.00 271.71 180.52 o -7 6 0 1072.03 949.71 184.72 o -6 6 0 773.44 624.15 157.36 o -5 6 0 1558.66 1528.94 117.48 o -4 6 0 3735.25 3749.95 149.83 o -3 6 0 1240.60 1218.58 110.15 o -2 6 0 15780.01 15374.24 412.94 o -1 6 0 205.88 217.86 45.33 o 0 6 0 7810.01 8318.42 174.52 o 1 6 0 26.80 -6.77 35.55 o 2 6 0 24549.54 25272.79 445.83 o 3 6 0 754.35 813.75 58.78 o 4 6 0 945.89 869.83 61.57 o 5 6 0 1895.46 1656.01 79.83 o 6 6 0 5285.20 5768.96 152.64 o 7 6 0 4043.91 4209.00 130.42 o 8 6 0 1205.04 1126.80 143.67 o 9 6 0 2326.20 2148.93 193.03 o 10 6 0 70.38 323.80 146.51 o 11 6 0 377.29 306.40 147.19 o 12 6 0 340.13 221.67 164.00 o -7 7 0 206.44 269.58 117.37 o -6 7 0 773.63 874.84 172.99 o -5 7 0 754.61 720.15 99.31 o -4 7 0 431.36 552.34 120.51 o -3 7 0 2080.83 2208.38 106.19 o -2 7 0 659.61 588.43 63.41 o -1 7 0 1608.03 1653.97 79.86 o 0 7 0 2626.12 2598.15 91.43 o 1 7 0 6241.28 6561.76 149.64 o 2 7 0 633.86 565.24 73.13 o 3 7 0 8441.71 8912.85 206.07 o 4 7 0 499.15 515.82 60.83 o 5 7 0 4397.86 4694.34 140.22 o 6 7 0 1468.74 1567.82 112.54 o 7 7 0 388.32 269.72 62.80 o 8 7 0 917.67 744.86 80.05 o 9 7 0 1338.27 1595.84 182.38 o 10 7 0 596.28 713.67 153.45 o 11 7 0 155.14 59.91 167.32 o 12 7 0 539.20 835.74 186.09 o -6 8 0 342.68 228.27 111.14 o -5 8 0 268.24 313.54 127.89 o -4 8 0 527.78 585.30 75.24 o -3 8 0 160.87 145.66 75.33 o -2 8 0 3292.14 3087.13 151.00 o -1 8 0 1073.53 908.94 72.99 o 0 8 0 5492.47 5210.63 140.03 o 1 8 0 897.82 873.07 155.40 o 2 8 0 5507.41 5371.29 349.02 o 3 8 0 686.10 746.70 83.37 o 4 8 0 4273.02 4341.18 140.38 o 5 8 0 1971.35 2250.17 105.02 o 6 8 0 2896.71 2619.49 112.30 o 7 8 0 1235.85 1227.18 92.25 o 8 8 0 1788.94 2104.72 111.19 o 9 8 0 1154.82 1330.00 171.33 o 10 8 0 873.95 980.20 172.99 o 11 8 0 722.89 519.47 185.41 o 12 8 0 29.85 0.59 189.71 o -5 9 0 411.55 674.68 143.09 o -4 9 0 346.43 323.07 80.88 o -3 9 0 985.32 1131.35 147.83 o -2 9 0 582.48 440.42 80.48 o -1 9 0 2847.29 2888.02 172.21 o 0 9 0 701.83 573.52 103.21 o 1 9 0 7685.16 7168.87 269.07 o 2 9 0 495.29 378.92 91.48 o 3 9 0 5309.50 5553.84 290.47 o 4 9 0 10.54 17.56 68.91 o 5 9 0 8689.87 8994.72 285.15 o 6 9 0 25.95 137.30 71.81 o 7 9 0 3728.90 4163.29 154.37 o 8 9 0 1895.52 1899.53 117.51 o 9 9 0 1528.68 1861.88 193.71 o 10 9 0 504.12 600.00 159.21 o 11 9 0 279.83 364.26 167.23 o 12 9 0 480.11 220.69 181.30 o -4 10 0 500.26 688.16 163.02 o -3 10 0 445.18 340.90 144.06 o -2 10 0 1336.96 1458.72 165.27 o -1 10 0 156.30 162.14 102.33 o 0 10 0 712.31 655.23 125.00 o 1 10 0 96.05 -62.75 103.01 o 2 10 0 1931.56 1739.91 144.36 o 3 10 0 2.55 50.84 79.49 o 4 10 0 1834.32 1912.19 142.11 o 5 10 0 125.55 131.29 80.63 o 6 10 0 2959.25 2925.56 137.53 o 7 10 0 46.17 46.49 118.60 o 8 10 0 439.58 353.46 93.58 o 9 10 0 425.82 510.28 160.97 o 10 10 0 80.46 108.98 148.27 o 11 10 0 282.97 241.41 196.35 o -3 11 0 542.16 616.03 163.71 o -2 11 0 176.51 222.06 148.95 o -1 11 0 1084.25 1109.70 162.05 o 0 11 0 56.07 -23.16 122.07 o 1 11 0 819.94 809.55 127.84 o 2 11 0 0.44 115.92 115.13 o 3 11 0 2105.43 1973.59 158.04 o 4 11 0 352.83 342.82 201.09 o 5 11 0 1082.59 986.91 133.56 o 6 11 0 1017.92 955.50 105.70 o 7 11 0 195.80 196.04 91.89 o 8 11 0 527.45 654.84 120.66 o 9 11 0 513.99 601.18 175.73 o 10 11 0 324.06 603.03 177.98 o 11 11 0 184.04 70.37 167.13 o -2 12 0 714.94 867.31 186.87 o -1 12 0 163.34 121.49 155.99 o 0 12 0 1332.98 1234.31 157.65 o 1 12 0 28.10 125.49 119.73 o 2 12 0 1300.33 1308.20 155.30 o 3 12 0 0.73 144.45 130.09 o 4 12 0 1187.46 1211.71 131.47 o 5 12 0 79.73 131.78 92.58 o 6 12 0 1054.74 1300.79 189.07 o 7 12 0 408.42 283.82 103.62 o 8 12 0 798.04 1115.55 122.65 o 9 12 0 235.96 218.34 177.68 o 10 12 0 629.46 580.46 193.42 o 0 13 0 110.93 222.74 170.94 o 1 13 0 981.04 1045.10 177.98 o 2 13 0 6.86 70.57 146.02 o 3 13 0 942.53 996.91 152.18 o 4 13 0 1.79 126.86 124.42 o 5 13 0 981.03 1135.26 145.30 o 6 13 0 11.10 116.77 101.24 o 7 13 0 943.54 924.31 122.96 o 8 13 0 331.41 440.17 114.10 o 9 13 0 391.33 315.68 122.02 o 3 14 0 0.81 20.52 160.09 o 4 14 0 729.91 709.76 171.14 o 5 14 0 55.83 116.60 136.83 o 6 14 0 890.13 736.25 171.82 o 7 14 0 519.54 652.56 138.37 o -7 -14 1 374.05 142.50 156.09 o -6 -14 1 93.31 167.13 142.01 o -5 -14 1 257.00 158.82 143.28 o -4 -14 1 55.61 -72.33 152.08 o -3 -14 1 634.53 575.57 171.82 o -9 -13 1 217.51 364.20 130.14 o -8 -13 1 556.98 705.79 154.42 o -7 -13 1 292.57 139.59 114.71 o -6 -13 1 735.70 550.49 139.23 o -5 -13 1 297.00 217.37 128.91 o -4 -13 1 727.94 601.18 155.40 o -3 -13 1 68.74 73.69 145.33 o -2 -13 1 1099.30 1109.60 157.84 o -1 -13 1 29.95 -23.95 155.40 o 0 -13 1 798.77 779.84 177.29 o -10 -12 1 276.17 402.67 173.97 o -9 -12 1 158.52 193.97 129.65 o -8 -12 1 769.43 708.42 116.69 o -7 -12 1 552.72 377.75 106.99 o -6 -12 1 576.52 691.09 118.95 o -5 -12 1 1653.97 1715.59 131.13 o -4 -12 1 16.68 12.52 182.08 o -3 -12 1 2034.34 1859.44 180.91 o -2 -12 1 21.10 74.67 112.59 o -1 -12 1 702.58 626.10 149.83 o 0 -12 1 10.54 -0.20 140.55 o 1 -12 1 930.55 1010.69 156.28 o 2 -12 1 15.31 222.16 173.29 o -11 -11 1 248.13 419.88 202.51 o -10 -11 1 95.45 206.81 174.17 o -9 -11 1 309.43 420.46 172.11 o -8 -11 1 613.35 631.85 103.84 o -7 -11 1 676.04 815.35 104.59 o -6 -11 1 1511.26 1497.52 118.12 o -5 -11 1 103.26 175.36 83.95 o -4 -11 1 466.62 578.25 204.17 o -3 -11 1 66.46 -46.91 114.55 o -2 -11 1 1155.14 1059.07 134.29 o -1 -11 1 349.50 139.86 120.90 o 0 -11 1 1365.82 1340.26 158.53 o 1 -11 1 24.91 19.84 135.27 o 2 -11 1 646.84 741.33 161.36 o 3 -11 1 334.17 351.85 159.51 o -11 -10 1 30.60 37.14 165.76 o -10 -10 1 1120.47 970.82 196.35 o -9 -10 1 628.20 535.60 151.88 o -8 -10 1 749.27 870.53 98.77 o -7 -10 1 2631.43 3010.99 141.47 o -6 -10 1 302.18 232.72 79.55 o -5 -10 1 3567.75 3664.78 146.15 o -4 -10 1 877.72 895.33 91.00 o -3 -10 1 2602.10 2815.51 142.84 o -2 -10 1 27.75 -8.70 91.87 o -1 -10 1 1716.90 1570.82 151.39 o 0 -10 1 258.43 148.07 95.39 o 1 -10 1 1425.54 1306.54 137.91 o 2 -10 1 283.72 160.39 129.31 o 3 -10 1 465.58 690.02 149.15 o 4 -10 1 250.95 172.11 151.20 o -12 -9 1 13.65 109.17 201.34 o -11 -9 1 1104.61 948.14 205.83 o -10 -9 1 344.31 291.55 147.68 o -9 -9 1 979.56 867.31 160.97 o -8 -9 1 158.31 245.93 78.80 o -7 -9 1 685.35 827.76 90.29 o -6 -9 1 1537.42 1512.54 100.10 o -5 -9 1 943.95 1135.66 89.03 o -4 -9 1 2285.21 2215.83 112.67 o -3 -9 1 707.28 687.93 174.17 o -2 -9 1 5399.26 5219.71 224.01 o -1 -9 1 35.94 -86.89 91.58 o 0 -9 1 5057.46 4771.30 218.83 o 1 -9 1 16.16 -5.86 102.23 o 2 -9 1 1454.54 1488.32 92.31 o 3 -9 1 474.93 403.55 138.25 o 4 -9 1 734.80 798.34 112.54 o 5 -9 1 312.11 -35.58 161.75 o -12 -8 1 468.29 754.72 190.68 o -11 -8 1 128.52 12.80 145.73 o -10 -8 1 301.15 315.69 148.07 o -9 -8 1 797.36 1025.16 160.39 o -8 -8 1 1119.61 1163.74 94.90 o -7 -8 1 1906.92 1770.41 117.14 o -6 -8 1 598.11 594.91 88.30 o -5 -8 1 6506.64 7052.47 187.59 o -4 -8 1 29.92 75.72 54.45 o -3 -8 1 4060.91 4072.37 136.93 o -2 -8 1 5.04 121.44 55.76 o -1 -8 1 2651.99 2795.82 101.75 o 0 -8 1 125.24 166.07 56.84 o 1 -8 1 4137.28 3815.08 126.60 o 2 -8 1 388.96 291.83 69.93 o 3 -8 1 4091.38 4299.93 149.47 o 4 -8 1 140.27 226.50 67.55 o 5 -8 1 779.88 844.88 111.68 o 6 -8 1 667.74 616.03 157.45 o -12 -7 1 75.77 8.01 172.99 o -11 -7 1 694.23 721.88 165.66 o -10 -7 1 384.39 349.02 143.57 o -9 -7 1 1307.54 1311.23 170.06 o -8 -7 1 1113.77 1242.25 86.26 o -7 -7 1 3871.48 4054.00 135.45 o -6 -7 1 5468.20 6154.06 168.70 o -5 -7 1 3938.19 3614.84 122.36 o -4 -7 1 4458.52 4543.13 134.43 o -3 -7 1 112.22 85.68 47.33 o -2 -7 1 16214.13 15871.53 647.03 o -1 -7 1 1162.50 1209.64 120.12 o 0 -7 1 13986.59 13038.00 255.81 o 1 -7 1 116.07 136.87 53.15 o 2 -7 1 9506.93 9610.82 217.00 o 3 -7 1 1205.77 1170.54 84.66 o 4 -7 1 2345.23 2283.49 153.04 o 5 -7 1 355.73 510.93 94.30 o 6 -7 1 981.94 1252.71 123.44 o 7 -7 1 464.51 442.92 163.32 o -12 -6 1 539.96 420.85 158.14 o -11 -6 1 15.73 -60.30 134.00 o -10 -6 1 3552.25 3594.06 250.89 o -9 -6 1 1152.83 1358.54 175.34 o -8 -6 1 3494.49 3598.56 225.87 o -7 -6 1 809.27 1086.46 198.16 o -6 -6 1 2585.74 2562.63 129.01 o -5 -6 1 1231.53 1118.45 68.29 o -4 -6 1 6083.98 7096.08 167.01 o -3 -6 1 867.46 1031.27 96.17 o -2 -6 1 236.26 194.76 52.73 o -1 -6 1 12271.56 11757.45 194.21 o 0 -6 1 501.88 435.97 74.77 o 1 -6 1 9257.57 9601.88 202.17 o 2 -6 1 3477.13 3273.15 109.74 o 3 -6 1 4129.69 3832.08 123.59 o 4 -6 1 476.95 571.13 77.06 o 5 -6 1 1176.14 1105.80 92.33 o 6 -6 1 515.34 745.92 151.78 o 7 -6 1 411.67 656.59 162.93 o 8 -6 1 466.84 266.45 170.16 o -12 -5 1 13.75 313.93 177.88 o -11 -5 1 729.03 491.52 165.37 o -10 -5 1 203.61 364.65 127.25 o -9 -5 1 2470.33 2210.02 187.85 o -8 -5 1 2420.37 2615.33 197.04 o -7 -5 1 697.04 600.43 103.16 o -6 -5 1 2070.08 2204.37 87.05 o -5 -5 1 528.64 515.36 123.69 o -4 -5 1 5545.19 5740.49 234.96 o -3 -5 1 2105.74 2330.55 79.75 o -2 -5 1 8681.49 8781.01 182.16 o -1 -5 1 253.37 361.95 33.16 o 0 -5 1 13626.85 14730.37 264.34 o 1 -5 1 1448.12 1359.57 63.19 o 2 -5 1 4095.10 4524.98 122.29 o 3 -5 1 966.61 1029.56 92.65 o 4 -5 1 3022.25 2988.12 149.83 o 5 -5 1 1057.89 1006.49 85.05 o 6 -5 1 3563.64 3537.38 232.32 o 7 -5 1 1103.70 1348.18 171.72 o 8 -5 1 224.91 104.68 151.10 o 9 -5 1 691.38 739.38 191.76 o -12 -4 1 1189.22 950.59 188.34 o -11 -4 1 359.76 520.25 152.08 o -10 -4 1 990.43 672.23 140.35 o -9 -4 1 171.12 293.80 110.83 o -8 -4 1 2689.37 2544.37 190.10 o -7 -4 1 3613.59 3594.71 107.24 o -6 -4 1 5297.06 5340.55 353.90 o -5 -4 1 12463.46 12914.39 247.09 o -4 -4 1 1332.60 1321.55 59.74 o -3 -4 1 3984.41 4113.73 103.05 o -2 -4 1 6958.96 7505.31 152.66 o -1 -4 1 27661.85 28251.10 379.83 o 0 -4 1 95.43 154.85 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