Acta Cryst. (2005). E61, m1237-m1239  [ doi:10.1107/S1600536805016272 ]

Dichlorotris(triphenylphosphine)ruthenium(II) dichloromethane hemisolvate

A. R. Cowley, J. R. Dilworth and C. A. Maresca von Beckh W.

Online 31 May 2005

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.006 Å
• R factor = 0.039
• wR factor = 0.041
• Data-to-parameter ratio = 10.8

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio 
PLAT141_ALERT_4_C su on a - Axis Small or Missing (x 100000) .....         20 Ang.  
PLAT142_ALERT_4_C su on b - Axis Small or Missing (x 100000) .....         10 Ang.  
PLAT164_ALERT_4_C Nr. of Refined C-H H-Atoms in Heavy-At Struct...          2       
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.86 Ratio 
PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd.  #          2       
              C H2 Cl2                                                          

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion

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