Acta Cryst. (2005). E61, m1295-m1297  [ doi:10.1107/S1600536805017599 ]

Diaquadiperchlorato[-11,23-dimethyl-3,7,15,19-tetraazatricyclo[19.3.1.1^9,13]hexacosa-1(25),2,7,9,11,13(26),14,19,21,23-decaene-25,26-diolato-1²N,N';2²N'',N''';1:2²O:O']dicadmium(II) diaqua[-11,23-dimethyl-3,7,15,19-tetraazatricyclo[19.3.1.1^9,13]hexacosa-1(25),2,7,9,11,13(26),14,19,21,23-decaene-25,26-diolato-1²N,N';2²N'',N''';1:2²O:O']dicadmium(II) diperchlorate

B. Liu, H. Zhou, Z.-Q. Pan, X.-L. Hu and L. Chen

Online 10 June 2005

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.009 Å
• R factor = 0.050
• wR factor = 0.119
• Data-to-parameter ratio = 14.4

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT199_ALERT_1_C Check the Reported _cell_measurement_temperature        293 K     
PLAT200_ALERT_1_C Check the Reported _diffrn_ambient_temperature .        293 K     
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...          9       

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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