Acta Cryst. (2005). E61, m1301-m1303  [ doi:10.1107/S1600536805017873 ]

Redetermination of catena-poly[[[bis(ethylenediamine)platinum(II)]--chloro-[bis(ethylenediamine)platinum(IV)]--chloro] tetrakis(hexafluorophosphate)]

N. Matsushita

Online 10 June 2005

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (P-F) = 0.007 Å
• Disorder in main residue
• R factor = 0.030
• wR factor = 0.087
• Data-to-parameter ratio = 20.1

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for          P     

Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT061_ALERT_3_C Tmax/Tmin Range Test RR' too Large .............       0.82       
PLAT076_ALERT_1_C Occupancy       0.50 less than 1.0 for Sp.pos  .         CL       
PLAT301_ALERT_3_C Main Residue  Disorder .........................      23.00 Perc. 

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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